Nitrogen-doped graphene-like carbon from bio-waste as efficient low-cost electrocatalyst for fuel cell application

Bulletin of Materials Science - Tập 44 - Trang 1-7 - 2021
Dasari Bosubabu1,2, V Parthiban1,2, A K Sahu1,2, K Ramesha1,2
1CSIR-Central Electrochemical Research Institute-Madras Unit, CSIR-Madras Complex, Chennai, India
2Academy of Scientific and Innovative Research (AcSIR), Ghaziabad, India

Tóm tắt

The development of metal-free carbon-based catalysts for alkaline fuel cells has been the subject of current interest, because of the low cost and improving fuel cell efficiency. Particularly, nitrogen-doped carbon shows prominent results. Here, we show an oxygen reduction reaction (ORR) activity of nitrogen-doped graphene-like carbon materials (N-GLC) prepared by heating bagasse-derived carbon and melamine in a 1:15 ratio. The N-GLC catalyst displays excellent electro-catalytic activity towards the ORR with an onset potential of 0.92 V vs. reversible hydrogen electrode (RHE) in alkaline media (0.1 M KOH). Moreover, the half-wave (E1/2) potential 0.83 V is almost the same compared to Pt-C (40 wt%) catalyst and the diffusion limiting current of 4 mA cm–2. The rotating ring disc experiment showed a four-electron pathway (n = 3.65) with the moderate peroxide ( $${{\rm HO}}^{-}_{2}$$ ) yield. Due to its promising ORR activity and long-term electrochemical stability, N-GLC catalyst is used in alkaline anion exchange membrane fuel cell (AEMFC) as a single cell, about 6 mW cm–2 peak power density was achieved at the load current density of ~20 mA cm–2. So the N-GLC can be a cheap alternative ORR catalyst for AEMFC applications.

Tài liệu tham khảo

Takanabe K 2017 ACS Catal. 7 8006 Strasser P 2016 Acc. Chem. Res. 49 2658 Yadegari H, Norouzi Banis M, Lushington A, Sun Q, Li R, Sham T K et al 2017 Energy Environ. Sci. 10 286 Dresp S, Luo F, Schmack R, Kühl S and Gliech M 2016 Energy Environ. Sci. 9 2020 Wang Z L, Xu D, Xu J J and Zhang X B 2014 Chem. Soc. Rev. 43 774 Angamuthu G, Bosu D, Ramesha K and Rangarajan V 2019 J. Electroanal. Chem. 843 37 Masthanaiah P, Babu D B, Roy M L and Ramesha K 2019 J. Power Sources 436 226850 Bosubabu D, Sivaraj J, Sampathkumar R and Ramesha K 2019 ACS Appl. Energy Mater. 2 4118 Bosubabu D, Ette P M, Nanda Kumar A K, Arulraj A and Ramesha K 2020 ACS Appl. Energy Mater. 3 8716 Bosu D, Ramesha R N, Masthanaiah P, Kaitheri A, Kumar N, Arulraj A et al 2019 J. Power Sources 436 226870 Ramesha R N, Bosu D, Masthanaiah P and Ramesha K 2020 ChemElectroChem 7 328 Srinu A, Peera S G, Parthiban V, Bhuvaneshwari B and Sahu A K 2018 Chem. Select. 3 690 Ramaswamy N and Mukerjee S 2012 Adv. Phys. Chem. 2012 1 Spendelow J S and Wieckowski A 2007 Phys. Chem. Chem. Phys. 9 2654 Ge X, Sumboja A, Wuu D, An T, Li B, Thomas Goh F W et al 2015 ACS Catal. 5 4643 Mahata A, Nair A S and Pathak B 2019 Catal. Sci. Technol. 9 4835 Zhao X, Yin M, Ma L, Liang L, Liu C, Liao J et al 2011 Energy Environ. Sci. 4 2736 Song W, Chen Z, Yang C, Yang Z, Tai J, Nan Y et al 2015 J. Mater. Chem. A 3 1049 Li H, Chen C, Yan D, Wang Y, Chen R, Zou Y et al 2019 J. Mater. Chem. A 7 23432 Xue Y, Sun S, Wang Q, Dong Z and Liu Z 2018 J. Mater. Chem. A 6 10596 Peera S G, Lee T G and Sahu A K 2019 Sustain. Energy Fuels 3 1866 Hu C and Dai L 2016 Angew. Chemie Int. Ed. 55 11736 Ma R, Lin G, Zhou Y, Liu Q, Zhang T, Shan G et al 2019 NPJ Comput. Mater. 5 1 Hu C, Xiao Y, Zou Y and Dai L 2018 Electrochem. Energy Rev. 1 84 Sarapuu A, Kibena-Põldsepp E, Borghei M and Tammeveski K 2018 J. Mater. Chem. A 6 776 Cui H, Guo Y, Guo L, Wang L, Zhou Z and Peng Z 2018 J. Mater. Chem. A 6 18782 Xiong D, Li X, Fan L and Bai Z 2018 Catalysts 8 301 Guo Z, Ren G, Jiang C, Lu X, Zhu Y, Jiang L et al 2015 Sci. Rep. 5 1 Bosu Babu D and Ramesha K 2016 Electrochem. Acta 219 290 Naumov O, Naumov S, Abel B and Varga A 2018 Nanoscale 10 6724 Wong W Y, Daud W R W, Mohamad A B, Kadhum A A H, Loh K S and Majlan E H 2013 Int. J. Hydrogen Energy 38 9370 Quílez-Bermejo J, Melle-Franco M, San-Fabián E, Morallón E and Cazorla-Amorós D 2019 J. Mater. Chem. A 7 24239 Wang H, Maiyalagan T and Wang X 2012 ACS Catal. 2 781 Bosu D and Ramesha K 2019 Carbon 144 582 Liu Y, Shi Z, Gao Y, An W, Cao Z and Liu J 2016 ACS Appl. Mater. Interface 8 28283 Zou B X, Gao Y, Liu B, Yu Y and Lu Y 2016 RSC Adv. 6 4483 Li H, Yuan D, Tang C, Wang S, Sun J, Li Z et al 2016 Carbon 100 151 Zhu S, Taberna P L, Zhao N and Simon P 2018 Electrochem. Commun. 96 6 Zhang X, Zhao J, He X, Li Q, Ao C, Xia T et al 2018 Carbon 127 236 Parthiban V, Bhuvaneshwari B, Karthikeyan J, Murugan P and Sahu A K 2019 Nanoscale Adv. 1 4926