Synthesis of N-(oxyran-2-ylmethyl)triazoles and -tetrazoles

Pleiades Publishing Ltd - Tập 51 - Trang 1308-1312 - 2015
T. V. Golobokova1, A. G. Proidakov1, L. I. Vereshchagin1, V. N. Kizhnyaev1
1Irkutsk State University, Irkutsk, Russia

Tóm tắt

The alkylation of 5-phenyl-1H-tetrazole and 4-nitro-2H-1,2,3-triazole with 1-chloro-2,3-epoxypropane and cycloaddition of 1-azido-3-chloropropan-2-ol to acetylenic dipolarophiles gave the corresponding N-(3-chloro-2-hydroxypropyl)azoles as intermediate products in the synthesis of N-(oxiran-2-ylmethyl)azoles.

Tài liệu tham khảo

Buzilova, S.R., Kuznetsova, N.I., Shul’gina, V.M., Gareev, G.A., and Vereshchagin, L.I., Chem. Heterocycl. Compd., 1983, vol. 19, p. 107. Licht, H.H. and Ritter, H., J. Energ. Mater., 1994, vol. 12, p. 223. Kagitani, T., Minagawa, M., Nakakata, Y., Kimura, R., Tsubakimoto, T., Oshiumi, R., and Sakano, K., JPN Patent no. 6 239 525, 1987; Chem. Abstr., 1987, vol. 107, no. 59 040. Novikov, S.S., Shveikhgeimer, G.A., and Sevost’yanova, V.A., Khimiya alifaticheskikh i alitsiklicheskikh nitrosoedinenii (Chemistry of Aliphatic and Alicyclic Nitro Compounds), Moscow: Khimiya, 1974, p. 153. Livi, O., Biagi, G., Ferretti, M., Lucacchini, A., and Berili, L., Eur. J. Med. Chem., 1983, vol. 18, p. 171. Eages, T., Khan, M.A., and Lynch, B.M., Org. Prep. Proced. Int., 1970, vol. 2, p. 117. Maksikova, A.V., Serebryakova, E.S., Shcherbakov, V.V., Gareev, G.A., and Vereshchagin, L.I., Zh. Org. Khim., 1989, vol. 25, p. 1519. Khan, M.A. and Lynch, B.M., J. Heterocycl. Chem., 1970, vol. 7, p. 1237. Vereshchagin, L.I., Kuznetsova, N.I., Kirillova, L.P., Shcherbakov, V.V., Sukhanov, G.T., and Gareev, G.A., Chem. Heterocycl. Compd., 1986, vol. 22, p. 745.