TG-DTA and FTIR analyses of roman and later historic mortars from Drobeta-Turnu Severin region

Journal of Thermal Analysis and Calorimetry - Tập 138 Số 3 - Trang 2159-2166 - 2019
Moşoiu, Codruţa1, Vlase, Dan2,3, Vlase, Gabriela1, Lazău, Radu4, Vlase, Titus1
1Research Center for Thermal Analysis in Environmental Problems, West University of Timisoara, Timişoara, Romania
2Department of Scientific Research and Academic Creation, West University of Timisoara, Timişoara, Romania
3County Directorate for Culture Timiş, Timişoara, Romania
4Faculty of Industrial Chemistry and Environmental Engineering, Politehnica University Timisoara, Timisoara, Romania

Tóm tắt

The study shows the analysis of the various Roman mortars in the survival structure of the Danube Bridge in Drobeta-Turnu Severin, Romania, which is particularly relevant, and the results provided will help clarify the technology used for its construction through spectral, XRD and thermoanalytic techniques. It is intended to establish similarities or differences between the studied subjects. This paper highlights the complementary nature of the various techniques: XRD for the identification of major crystalline phases, FTIR for a more detailed evaluation of the composition comprising non-crystalline and TGA phase for the quantitative determination of volatile phases (especially CO2 and H2O).

Tài liệu tham khảo

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