Development and validation of a HILIC-ELSD method for simultaneous analysis of non-substituted and acetylated xylo-oligosaccharides

Journal of Pharmaceutical and Biomedical Analysis - Tập 139 - Trang 232-237 - 2017
Jianghua Pu1,2, Xia Zhao1,2, Lin Xiao3,4, Haitao Zhao3,5
1Key Laboratory of Marine Drugs, Ministry of Education, School of Medicine and Pharmacy, Ocean University of China, Shandong Provincial Key laboratory of Glycoscience and Glycoengineering, Qingdao 266003, China
2Laboratory for Marine Drugs and Bioproducts of Qingdao National Laboratory for Marine Science and Technology, Qingdao 266237, China
3Shandong Long Live Bio-Technology Co.,Ltd. Yucheng 251200, China
4Shandong Key Laboratory of Straw and Stover Biorefinement Technologies, High-technology Development Zone, Yucheng, Shandong 251200, China
5Shandong Functional Sugar Engineering Research Center, Yucheng, Shandong 251200, China

Tài liệu tham khảo

Carvalho, 2013, Xylo-oligosaccharides from lignocellulosic materials: chemical structure, health benefits and production by chemical and enzymatic hydrolysis, Food Res. Int., 51, 75, 10.1016/j.foodres.2012.11.021 Pandey, 2015, Probiotics, prebiotics and synbiotics-a review, J. Food Sci. Technol., 52, 7577, 10.1007/s13197-015-1921-1 Singh, 2015, Prebiotic potential of oligosaccharides: a focus on xylan derived oligosaccharides, Bioact. Carbohyd. Diet. Fibre, 5, 19, 10.1016/j.bcdf.2014.11.003 Moure, 2006, Advances in the manufacture, purification and applications of xylo-oligosaccharides as food additives and nutraceuticals, Process Biochem., 41, 1913, 10.1016/j.procbio.2006.05.011 Courtois, 2009, Oligosaccharides from land plants and algae: production and applications in therapeutics and biotechnology, Cur. Opin. Microbiol., 12, 261, 10.1016/j.mib.2009.04.007 Patel, 2011, Functional oligosaccharides: production, properties and applications, World J. Microb. Biot., 27, 1119, 10.1007/s11274-010-0558-5 Moniz, 2014, Hydrothermal production and gel filtration purification of xylo-oligosaccharides from rice straw, Ind. Crops Prod., 62, 460, 10.1016/j.indcrop.2014.09.020 Gullón, 2011, Structural features and properties of soluble products derived from eucalyptus globules hemicelluloses, Food Chem., 127, 1798, 10.1016/j.foodchem.2011.02.066 Kumar, 2014, Generation of xylooligosaccharides from microwave irradiated agroresidues using recombinant thermo-alkali-stable endoxylanase of the polyextremophilic bacterium bacillus halodurans, expressed in pichia pastoris, Bioresour. Technol., 179, 382, 10.1016/j.biortech.2014.12.049 Moniz, 2016, Assessment of the bifidogenic effect of substituted xylo-oligosaccharides obtained from corn straw, Carbohyd. Polym., 136, 466, 10.1016/j.carbpol.2015.09.046 Samala, 2014, Comparison of xylo-oligosaccharides production by autohydrolysis of fibers separated from ground corn flour and DDGS, Food Bioprod. Process., 94, 354, 10.1016/j.fbp.2014.04.004 Otieno, 2012, A thermochemical pretreatment process to produce xylooligosaccharides (XOS), arabinooligosaccharides (AOS) and mannooligosaccharides (MOS) from lignocellulosic biomasses, Bioresour. Technol., 112, 285, 10.1016/j.biortech.2012.01.162 Chen, 2014, Autohydrolysis of miscanthus x giganteus for the production of xylooligosaccharides (XOS): kinetics, characterization and recovery, Bioresour. Technol., 155, 359, 10.1016/j.biortech.2013.12.050 Wang, 2006, Progress in precolumn derivatization for HPLC analysis of glycans, Chin. J. Org. Chem., 26, 592 Sheng, 2014, A dextran-bonded stationary phase for saccharide separation, J. Chromatogr. A, 1345, 57, 10.1016/j.chroma.2014.03.076 Ma, 2014, Simultaneous separation and determination of fructose sorbitol, glucose and sucrose in fruits by HPLC-ELSD, Food Chem., 145, 784, 10.1016/j.foodchem.2013.08.135 Sastre, 2016, MALDI-TOF mass spectrometry and reversed-phase HPLC-ELSD chromatography for structural and quantitative studies of major steroid saponins in commercial extracts of Yucca schidigera Roezl, J. Pharm. Biomed. Anal., 120, 270, 10.1016/j.jpba.2015.12.043 ICH, 2005, Q2 (R1) validation of analytical procedures Guo, 2014, Hydrophilic interaction chromatography for selective separation of isomeric saponins, J. Chromatogr. A, 1325, 121, 10.1016/j.chroma.2013.12.006 Fu, 2013, Separation of carbohydrates using hydrophilic interaction liquid chromatography, Carbohyd. Res., 379, 13, 10.1016/j.carres.2013.06.006 Naran, 2009, Extraction and characterization of native heteroxylans from delignified corn stover and aspen, Cellulose, 16, 661, 10.1007/s10570-009-9324-y Pu, 2016, Development and validation of a HPLC method for determination of degree of polymerization of xylo-oligosaccharides, Food Chem., 213, 654, 10.1016/j.foodchem.2016.07.014