Gas chromatography-mass spectrometry method for determination of phospholipid peroxides; II. Transesterification to form pentafluorobenzyl esters and detection with picogram sensitivity

Journal of Free Radicals in Biology & Medicine - Tập 1 - Trang 387-393 - 1985
Frederik J.G.M. van Kuijk1, David W. Thomas2,1, Robert J. Stephens2,1, Edward A. Dratz
1Chemistry Board of Studies, Division of Natural Sciences, University of California, Santa Cruz CA 95064, U.S.A.
2Life Sciences Division, Cell Biology Program, SRI International, Menlo Park CA 94025, U.S.A.

Tài liệu tham khảo

1984, 1 Cerutti, 1985, Prooxidant states and tumor promotion, Science, 227, 375, 10.1126/science.2981433 van Kuijk, 1985, Chromatography-Mass Spectrometry method for determination of phospholipid peroxides: I. Transesterification to form methyl esters, J. Free Rad. Biol. Med., 1, 215, 10.1016/0748-5514(85)90121-7 Kawahara, 1968, Microdetermination of derivatives of phenols and mercaptans by means of electron capture gas chromatography, Anal. Chem., 40, 1009, 10.1021/ac60262a044 Kawahara, 1968, Microdetermination of pentafluorobenzyl ester derivatives of organic acids by means of electron capture gas chromatography, Anal. Chem., 40, 2073, 10.1021/ac60269a044 Strife, 1984, Preparation of pentafluorobenzyl esters of arachidonic acid lipoxygenase metabolites. Analysis by gas chromatography and negative-ion chemical ionization mass spectrometry, J. Chromatogr., 305, 3, 10.1016/S0378-4347(00)83309-5 Strife, 1984, Stable isotope labelled 5-lipoxygenase metabolites of arachidonic acid: analysis by negative ion chemical ionization mass spectrometry, Prostaglandines, Leukotrienes and Medicine, 13, 1, 10.1016/0262-1746(84)90095-7 Turk, 1985, Arachinodonic acid metabolism in isolated pancreatic islets. III. Effects of exogenous lipoxygenasw products and inhibitors on insuline secretion, Biochim. Biophys. Acta, 834, 23, 10.1016/0005-2760(85)90172-9 1967, Volume 1, 911 van Kuijk, 1986, Transesterification of phospholipids or triglycerides to fatty acid benzyl esters with simultaneous methylation of free fatty acids for gas chromatographic analysis, J. Lipid Res., 27, 452, 10.1016/S0022-2275(20)38826-X Bligh, 1959, A rapid method of total lipid extraction and purification, Can J. Biochem. Physiol., 37, 911, 10.1139/o59-099 van Kuijk, 1985, Consecutive action of phospholipase A2 and glutathione peroxidase is required for reduction of phospholipid hydroperoxides and provides a convenient method to determine peroxide values in membranes, J. Free Rad. Biol. Med., 1, 421, 10.1016/0748-5514(85)90156-4 Chan, 1977, Autooxidation of methyl linoleate. Separation and analysis of iosmeric mixtures of methyl linoleate hydroperoxides and methyl hydroxylinoleates, Lipids, 12, 99, 10.1007/BF02532979 Slater, 1984, Overview of methods used for detecting lipid peroxidation, Volume 105, 283 Bird, 1984, Comparative studys on different methods of malonaldehyde determination, Volume 105, 299 Hughes, 1983, High performance liquid chromatography and gas chromatography-mass spectrometry determination of specific lipid peroxidation products in vivo, Anal. Biochem., 130, 431, 10.1016/0003-2697(83)90612-7 McCreary, 1978, A novel and rapid method for the preparation of methyl esters for gas chromatography: Application to the determination of the fatty acids of edible fats and oils, J. Chromatogr. Sci., 16, 329, 10.1093/chromsci/16.8.329 Farnsworth, 1979, Effects of vitamin E and selenium deficiency on the fatty acid composition of retinal tissues, Biochim. Biophys. Acta, 552, 281, 10.1016/0005-2736(79)90283-9 Deese, 1981, Interaction of rhodopsin with two unsaturated phosphatidylcholines: A deuterium nuclear magnetic resonance study, Biochemistry, 20, 6420, 10.1021/bi00525a021 Netting, 1984, High performance liquid chromatographic separation of fatty acids as pentafluorobenzyl esters, J. Chromatogr., 336, 115, 10.1016/S0378-4347(00)85135-X