On flame retardancy in polycaprolactam composites by aluminium diethylphosphinate and melamine polyphosphate in conjunction with organically modified montmorillonite nanoclay

Shonaike, 2003 Mark, 2007 Walters, 2000, Heats of combustion of high temperature polymers, Fire Mater, 24, 245, 10.1002/1099-1018(200009/10)24:5<245::AID-FAM744>3.0.CO;2-7 Pesetskii, 2005, Influence of a cooling rate on a structure of PA6, Eur Polym J, 41, 1380, 10.1016/j.eurpolymj.2004.12.009 Wang, 2006, Crystallisation behaviour of PA6/SiO2 organic–inorganic hybrid material, Mater Res Bull, 41, 298, 10.1016/j.materresbull.2005.08.023 Killaris, 2012, Study on the properties of polyamide 6 blended with melamine polyphosphate and layered silicates, Polym Degrad Stab, 97, 1114 Rodriguez, 2009, Thermo-XRD and differential scanning calorimetry to trace epitaxial crystallisation in PA6/montmorillonite nanocomposites, Mater Lett, 63, 1159, 10.1016/j.matlet.2009.02.027 Bakirtzis, 2009, Structure of the condensed phase and char of fire-retarded PBT nanocomposites in N2, Fire Saf J, 44, 1023, 10.1016/j.firesaf.2009.07.002 Ramani, 2010, Interaction of a phosphorous based FR, a nanoclay and PA6. Part 2 Interaction of the complete PA6 polymer nanocomposites, Fire Mater, 34, 77 Businger, 1971, Linear least squares solutions by householder transformations, vol. 2, 111 Pramoda, 2003, Thermal degradation behaviour of polyamide 6/clay nanocomposite, Polym Degrad Stab, 81, 4756, 10.1016/S0141-3910(03)00061-2 Jang, 2005, The effect of clay on the thermal degradation of polyamide 6 in polyamide 6/clay nanocomposites, Polymer, 46, 32643274, 10.1016/j.polymer.2005.02.078 Smith, 2007 Uc, 2007, Thermal degradation of commercially available organoclays studied by TGA-FTIR, Thermochim Acta, 457, 92, 10.1016/j.tca.2007.03.008 Ramani, 2009, Interaction of a phosphorus based FR, a nanoclay and PA6. Part 1. Interaction of FR and nanoclay, Fire Mater, 33, 273, 10.1002/fam.1004 Siow, 2004, Flame inhibition activity of phosphorous-containing compounds using laser-induced fluorescence measurements of hydroxyl, Combust Flame, 136, 16, 10.1016/j.combustflame.2003.08.010 Korobeinichev, 1999, The destruction chemistry of organophosphorous compounds in flames—I: quantitative determination of final phosphorous-containing species in hydrogen–oxygen flames, Combust Flame, 118, 718, 10.1016/S0010-2180(99)00030-9 Korobeinichev, 2000, The chemistry of the destruction of organophosphorous compounds in flames—III: the destruction of DMMP and TMP in a flame of hydrogen and oxygen, Combust Flame, 121, 593, 10.1016/S0010-2180(99)00171-6 Schartel, 2010, Phosphorous-based flame retardancy mechanism—old hat or a starting point for future development?, Materials, 3, 4710, 10.3390/ma3104710 Twarowski, 1995, Reduction of a phosphorous oxide and acid reaction set, Combust Flame, 102, 41, 10.1016/0010-2180(94)00230-P Twarowski, 1993, The influence of phosphorous oxides and acids on the rate of H + OH recombination, Combust Flame, 94, 91, 10.1016/0010-2180(93)90022-U Jeffrey, 1997 Braun, 2005, The effect of red phosphorous and melamine polyphosphate on fire behaviour of HIPS, J Fire Sci, 23, 5 Braun, 2007, Flame retardancy mechanisms of aluminium phosphinate in combination with melamine polyphosphate and zinc borate in glass-fibre reinforced polyamide 6,6, Polym Degrad Stab, 92, 1528, 10.1016/j.polymdegradstab.2007.05.007 Levchik, 1999, Thermal decomposition of aliphatic nylons, Polym Int, 48, 532, 10.1002/(SICI)1097-0126(199907)48:7<532::AID-PI214>3.0.CO;2-R Balabanovich, 2004, 1,2-methyl-1,2-oxaphospholan-5-one 2-oxide fire retardance in HIPS: the effect of melamine and novalac, J Fire Sci, 22, 163 Zhaoqi, 1996, Catalytic hydrolysis of s-triazine compound over Al2O3, Catal Today, 27, 167, 10.1016/0920-5861(95)00185-9 Lu, 2002, Recent developments in the chemistry of halogen-free flame retardant polymers, Prog Polym Sci, 27, 1661, 10.1016/S0079-6700(02)00018-7 Reddy, 2009, Brønsted and Lewis acidity of modified montmorillonite clay catalysts determined by FT-IR spectroscopy, Catal Today, 141, 157, 10.1016/j.cattod.2008.04.004 Harrick, 1987, Internal reflection spectroscopy Delichatsios, 2010, Micro- and mesoscale testing and modeling for nanocomposite polymers in fires, 509 Davis, 2003, Processing degradation of polyamide 6/montmorillonite clay nanocomposites and clay organic modifier, Polym Degrad Stab, 79, 111, 10.1016/S0141-3910(02)00263-X 1956, vol. 3 Braun, 2010, Fire retardancy effect of aluminium phosphinate and melamine polyphosphate in glass fibre reinforced polyamide 6, e-Polymers, 10.1515/epoly.2010.10.1.443 Herrera, 2001, Main products and kinetics of the thermal degradation of polyamides, Chemosphere, 42, 601, 10.1016/S0045-6535(00)00233-2 Mlaga, 2007, A rising bubble in a polymer solution, J Non-Newtonian Mech, 141, 59, 10.1016/j.jnnfm.2006.07.012 Xie, 2001, Thermal characterization of organically modified montmorillonite, Thermochim Acta, 367-368, 339, 10.1016/S0040-6031(00)00690-0 Dahiya, 2012, The combined effect of organic phoshphinate/ammonium polyphosphate and pentaerythritol on thermal and fire properties of polyamide 6-clay nanocomposites, Polym Degrad Stab, 97, 1458, 10.1016/j.polymdegradstab.2012.05.012 Scaffaro, 2009, Effect of heating of organo-montmorillonites under different atmospheres, Appl Clay Sci, 45, 185, 10.1016/j.clay.2009.06.002 Samyn, 2008, Characterisation of the dispersion in polymer flame retarded nanocomposites, Eur Polym J, 44, 1631, 10.1016/j.eurpolymj.2008.03.018 Albalak, 1996 Frank, 2007, Bubble nucleation and growth in fluids, Chem Eng Sci, 62, 7090, 10.1016/j.ces.2007.08.030 Chrissafis, 2011, Can nanoparticles really enhance thermal stability of polymers? Part I: An overview on thermal decomposition of addition polymers, Thermochim Acta, 20, 1, 10.1016/j.tca.2011.06.010 Bikiaris, 2011, Can nanoparticles really enhance thermal stability of polymers? Part I: An overview on thermal decomposition of polycondensation polymers, Thermochim Acta, 20, 25, 10.1016/j.tca.2011.06.012 Kaynak, 2009, Mechanical properties, flammability and char morphology of epoxy resin/montmorillonite nanocomposites, Appl Clay Sci, 46, 319, 10.1016/j.clay.2009.08.033 Wallis, 1946, vol. 3 Lehn, 1995 Chen, 1998, Thermal decomposition of urea and urea derivatives by simultaneous TG/(DTA)/MS, J Mass Spectrom Soc Jpn, 46, 299, 10.5702/massspec.46.299 Levchik, 1997, Effect of melamine and its salts on combustion and thermal decomposition of polyamide 6, Fire Mater, 21, 75, 10.1002/(SICI)1099-1018(199703)21:2<75::AID-FAM597>3.0.CO;2-P Pankratov, 1989, Polycyclotrimerization of cyanamides, Russ Chem Rev, 58, 879, 10.1070/RC1989v058n09ABEH003484 Jahromi, 2003, Effect of melamine polyphosphate on thermal degradation of polyamides: a combined X-ray diffraction and solid-state NMR study, Polymer, 44, 25, 10.1016/S0032-3861(02)00686-9 Jastrzebski, 2011, Infrared spectroscopy of different phosphates structures, Spectrochim Acta Part A; Mol Biomol Spectrosc, 79, 722, 10.1016/j.saa.2010.08.044 Gallo, 2011, Flame retardant biocomposites: synergism between phosphinate and nanometric metal oxides, Eur Polym J, 47, 1390, 10.1016/j.eurpolymj.2011.04.001 Frankel, 1974, Surface acidity of montmorillonites, Clays Clay Miner, 22, 435, 10.1346/CCMN.1974.0220510