Comparison of methods for the detection of 10Be with AMS and a new approach based on a silicon nitride foil stack

International Journal of Mass Spectrometry - Tập 444 - Trang 116175 - 2019
Peter Steier1, Martin Martschini1, Josef Buchriegler1,2, Jenny Feige1,3, Johannes Lachner1, Silke Merchel1,2, Leonard Michlmayr1, Alfred Priller1, Georg Rugel2, Edith Schmidt1, Anton Wallner1,4, Eva Maria Wild1, Robin Golser1
1Universität Wien, Fakultät für Physik, Währinger Straße 17, A-1090, Vienna, Austria
2Helmholtz-Zentrum Dresden-Rossendorf (HZDR), Bautzner Landstr. 400, 01328, Dresden, Germany
3Technische Universität Berlin, Zentrum für Astronomie und Astrophysik, Hardenbergstraße 36, 10623 Berlin, Germany
4Department of Nuclear Physics, Australian National University, Canberra, ACT, 2601, Australia

Tài liệu tham khảo

Korschinek, 2010, A new value for the half-life of 10Be by Heavy-Ion Elastic Recoil Detection and liquid scintillation counting, Nucl. Instrum. Methods Phys. Res. B, 268, 187, 10.1016/j.nimb.2009.09.020 Chmeleff, 2010, Determination of the 10Be half-life by multicollector ICP-MS and liquid scintillation counting, Nucl. Instrum. Methods Phys. Res. B, 268, 192, 10.1016/j.nimb.2009.09.012 Raisbeck, 2006, 10Be evidence for the Matuyama-Brunhes geomagnetic reversal in the EPICA Dome C ice core, Nature, 444, 82, 10.1038/nature05266 Beer, 1990, Use of 10Be in polar ice to trace the 11-year cycle of solar activity, Nature, 347, 164, 10.1038/347164a0 Gosse, 2001, Terrestrial in situ cosmogenic nuclides: theory and application, Quat. Sci. Rev., 20, 1475, 10.1016/S0277-3791(00)00171-2 Willenbring, 2010, Long-term stability of global erosion rates and weathering during late-Cenozoic cooling, Nature, 465, 211, 10.1038/nature09044 Herzog, 2014, Cosmic-ray exposure ages of meteorites, vol 1, 419 Ehmann, 1958, Cosmic-ray-induced radioactivities in meteorites - II Al26, Be10 and Co60, aerolites, siderites and tektites, Geochem. Cosmochim. Acta, 14, 364, 10.1016/0016-7037(58)90075-9 von Blanckenburg, 1996, Separation of 9Be and cosmogenic 10Be from environmental materials and SIMS isotope dilution analysis, Chem. Geol., 129, 93, 10.1016/0009-2541(95)00157-3 Raisbeck, 1978, Beryllium-10 mass spectrometry with a cyclotron, Science, 202, 215, 10.1126/science.202.4364.215 Raisbeck, 1978, Measurement of 10Be in 1,000- and 5,0000- year-old Antarctic ice, Nature, 275, 731, 10.1038/275731a0 Fifield, 1990, Accelerator mass spectrometry at the Australian National University's 14UD accelerator: experience and developments, Nucl. Instrum. Methods Phys. Res. B, 852, 233, 10.1016/0168-583X(90)90412-N Matsuzaki, 2000, Development of a gas counter for AMS measurement of 10Be and 26Al of cosmic spherules, Nucl. Instrum. Methods Phys. Res. B, 172, 218, 10.1016/S0168-583X(00)00122-1 Kumar, 2011, 10Be measurements at IUAC-AMS facility, J. Radioanal. Nucl. Chem., 290, 179, 10.1007/s10967-011-1184-x Lawson, 2000, AMS at ANTARES - the first 10 years, Nucl. Instrum. Methods Phys. Res. B, 172, 95, 10.1016/S0168-583X(00)00276-7 Klein, 2008, Performance of the HVE 5 MV AMS system at CEREGE using an absorber foil for isobar suppression, Nucl. Instrum. Methods Phys. Res. B, 266, 1828, 10.1016/j.nimb.2007.11.077 Müller, 2010, Competitive 10Be measurements below 1 MeV with the upgraded ETH–TANDY AMS facility, Nucl. Instrum. Methods Phys. Res. B, 268, 2801, 10.1016/j.nimb.2010.05.104 Kubik, 2010, 10Be and 26Al measurements at the Zurich 6 MV Tandem AMS facility, Nucl. Instrum. Methods Phys. Res. B, 268, 880, 10.1016/j.nimb.2009.10.054 Middleton, 1989 Ziegler, 1985, vol 1 Fulbright, 1979, Ionization chambers, Nucl. Instrum. Methods, 162, 21, 10.1016/0029-554X(79)90704-3 2013 Lachner, 2014, 10Be and 26Al low-energy AMS using He-stripping and background suppression via an absorber, Nucl. Instrum. Methods Phys. Res. B, 331, 209, 10.1016/j.nimb.2013.11.034 Hofmann, 1987, Charge state distributions and isotopic fractionation, Nucl. Instrum. Methods Phys. Res. B, 29, 100, 10.1016/0168-583X(87)90214-X K.M. Wilcken, T. Fujioka, D. Fink, R.H. Fulop, A.T. Codilean, K. Simon, C. Mifsud, S. Kotevski. SIRIUS Performance: 10Be, 26Al and 36Cl measurements at ANSTO. Nucl. Instr. and Meth. in Phys. Res. B, https://doi.org/10.1016/j.nimb.2019.02.009, article in press L.K. Fifield, S.G. Tims, T. Fujioka, W.T. Hoo, S.E. Everett. Accelerator mass spectrometry with the 14UD accelerator at the Australian National University. Nucl. Instrum. Methods Phys. Res. B 201, 268, 858. Nottoli, 2013, The physics behind the isobar separation of 36Cl and 10Be at the French AMS national facility ASTER, Nucl. Instrum. Methods Phys. Res. B, 294, 397, 10.1016/j.nimb.2012.01.052 Kilius, 1997, Molecular fragment problems in heavy element AMS, Nucl. Instrum. Methods Phys. Res. B, 127, 10, 10.1016/S0168-583X(96)00421-1 Ziegler, 2010, SRIM – the stopping and range of ions in matter, Nucl. Instrum. Methods Phys. Res. B, 268, 1818, 10.1016/j.nimb.2010.02.091 Stocker, 2005, A universal and competitive compact AMS facility, Nucl. Instrum. Methods Phys. Res. B, 240, 483, 10.1016/j.nimb.2005.06.224 Zhao, 2004, The potential for AMS analysis of 10Be using BeF-, Nucl. Instrum. Methods Phys. Res. B, 223, 199, 10.1016/j.nimb.2004.04.041 Zhao, 2007, Measurement of Be-10 in air filters using BeF-ions from BaBeF4, Nucl. Instrum. Methods Phys. Res. B, 259, 345, 10.1016/j.nimb.2007.01.178 Ruiz-Gómez, 2010, On the measurement of 10Be on the 1 MV compact AMS system at the Centro Nacional de Aceleradores (Spain), Nucl. Instrum. Methods Phys. Res. B, 268, 733, 10.1016/j.nimb.2009.10.017 Synal, 1997, Status report of the PSI/ETH AMS facility, Nucl. Instrum. Methods Phys. Res. B, 123, 62, 10.1016/S0168-583X(96)00608-8 Woodruff, 2017, Improvements in measurement with the PRIME lab gas-filled magnet system Raisbeck, 1984, Measurement of 10Be with a tandetron accelerator operating at 2 MV, Nucl. Instrum. Methods Phys. Res. B, 5, 175, 10.1016/0168-583X(84)90505-6 Merchel, 2008, Towards more precise 10Be and 36Cl data from measurements at the 10-14 level: influence of sample preparation, Nucl. Instrum. Methods Phys. Res. B, 266, 4921, 10.1016/j.nimb.2008.07.031 Arnold, 2010, The French accelerator mass spectrometry facility ASTER: improved performance and developments, Nucl. Instrum. Methods Phys. Res. B, 268, 1954, 10.1016/j.nimb.2010.02.107 Akhmadaliev, 2013, The new 6 MV AMS-facility DREAMS at Dresden, Nucl. Instrum. Methods Phys. Res. B, 294, 5, 10.1016/j.nimb.2012.01.053 Heinemeier, 2015, The new extended HVE 1MV multi-element AMS system for low background installed at the Aarhus AMS Dating Center, Nucl. Instrum. Methods Phys. Res. B, 361, 143, 10.1016/j.nimb.2015.05.039 Maxeiner, 2019, Proof-of-principle of a compact 300 kV multi-isotope AMS facility, Nucl. Instrum. Methods Phys. Res. B, 439, 84, 10.1016/j.nimb.2018.11.028 Rom, 1998, Systematic investigations of 14C measurements at the Vienna enviromental research accelerator, Radiocarbon, 40, 255, 10.1017/S0033822200018129 Forstner, 2008, Applications of a compact ionization chamber in AMS at energies below 1 MeV/amu, Nucl. Instrum. Methods Phys. Res. B, 266, 2213, 10.1016/j.nimb.2008.02.060 Martschini, 2008 Wallner, 2010, Nuclear astrophysics and AMS – probing nucleosynthesis in the lab, Nucl. Instrum. Methods Phys. Res. B, 268, 1277, 10.1016/j.nimb.2009.10.152 Elsässer, 2011, Continuous 25-years aerosol records at coastal Antarctica: II. Variability and climate implications of 7Be, 10Be and 210Pb, Tellus, B63, 920, 10.1111/j.1600-0889.2011.00543.x Merchel, 2012, Quality assurance in accelerator mass spectrometry: results from an international round-robin exercise for 10Be, Nucl. Instrum. Methods Phys. Res. B, 289, 68, 10.1016/j.nimb.2012.07.038 Łosiak, 2012, 10Be content in suevite breccia clasts from the bosumtwi crater fill as a proxy for the content of surface components, Meteorit. Planet. Sci., 47/SI/1, A253 Elsässer, 2015, Simulating ice core 10Be on the glacial-interglacial timescale, Clim. Past, 11, 115, 10.5194/cp-11-115-2015 Klein, 1982, Modifications of an FN tandem for quantitative 10Be measurements, Nucl. Instrum. Methods, 193, 601, 10.1016/0029-554X(82)90258-0 Priller, 2004, Accelerator mass spectrometry of particle-bound 10Be, Nucl. Instrum. Methods Phys. Res. B, 223–224, 601, 10.1016/j.nimb.2004.04.111 Fischer, 1998 Schmelmer, 1998, Energy straggling of 60 MeV 58Niq+ ions in thin carbon foils and gases, Nucl. Instrum. Methods Phys. Res. B, 145, 261, 10.1016/S0168-583X(98)00526-6 Southon, 1983, The measurement of 10Be concentrations with a tandem accelerator, Nucl. Instrum. Methods, 205, 251, 10.1016/0167-5087(83)90195-3 Xu, 2010, Improved 10Be and 26Al-AMS with a 5 MV spectrometer, Nucl. Instrum. Methods Phys. Res. B, 268, 736, 10.1016/j.nimb.2009.10.018 Rood, 2010, Challenges and opportunities in high-precision Be-10 measurements at CAMS, Nucl. Instrum. Methods Phys. Res. B, 268, 730, 10.1016/j.nimb.2009.10.016 Goncz, 1992, An environmental sample chamber for X-ray microscopy, J. Microsc. (Oxf.), 168, 101, 10.1111/j.1365-2818.1992.tb03254.x Dran, 2004, Ion-beam analysis of Art works: 14 years of use in the Louvre, Nucl. Instrum. Methods Phys. Res. B, 219–220, 7, 10.1016/j.nimb.2004.01.019 Döbeli, 2004, Gas ionization chambers with silicon nitride windows for the detection and identification of low energy ions, Nucl. Instrum. Methods Phys. Res. B, 219–220, 415, 10.1016/j.nimb.2004.01.093 Klein, 2006, A compact 1 MV multi-element AMS system, Nucl. Instrum. Methods Phys. Res. B, 249, 764, 10.1016/j.nimb.2006.03.135 Andersen, 2005, Annealing and deposition effects of the chemical composition of silicon-rich nitride, Appl. Surf. Sci., 243, 401, 10.1016/j.apsusc.2004.09.096 Vockenhuber, 2005, The DTOF detector for isobar separation at ion energies below 1 MeV/amu, Nucl. Instrum. Methods Phys. Res. B, 240, 490, 10.1016/j.nimb.2005.06.169 Steier, 2000, Developments towards a fully automated AMS system, Nucl. Instrum. Methods Phys. Res. B, 161–163, 250, 10.1016/S0168-583X(99)00918-0 Nishiizumi, 2007, Absolute calibration of Be-10 AMS standards, Nucl. Instrum. Methods Phys. Res. B, 258, 403, 10.1016/j.nimb.2007.01.297 Christl, 2013, The ETH Zurich AMS facilities: performance parameters and reference materials, Nucl. Instrum. Methods Phys. Res. B, 294, 29, 10.1016/j.nimb.2012.03.004 Pavetich, 2014, Interlaboratory study of the ion source memory effect in Cl-36 accelerator mass spectrometry, Nucl. Instrum. Methods Phys. Res. B, 329, 22, 10.1016/j.nimb.2014.02.130 Rugel, 2016, The first four years of the AMS-facility DREAMS: status and developments for more accurate radionuclide data, Nucl. Instrum. Methods Phys. Res. B, 370, 94, 10.1016/j.nimb.2016.01.012 Auer, 2009, Cosmogenic 26Al in the atmosphere and the prospect of a 26Al/10Be chronometer to date old ice, Earth Planet. Sci. Lett., 287, 453, 10.1016/j.epsl.2009.08.030 Zanis, 2003, An estimate of the impact of stratosphere-to-troposphere transport (STT) on the lower free tropospheric ozone over the Alps using Be-10 and Be-7 measurements, J. Geophys. Res., 108, 8520, 10.1029/2002JD002604 Feige, 2014 Feige, 2018, Limits on supernova-associated 60Fe/26Al nucleosynthesis ratios from accelerator mass spectrometry measurements of deep-sea sediments, Phys. Rev. Lett., 121, 221103, 10.1103/PhysRevLett.121.221103 Wallner, 2016, Recent near-Earth supernovae probed by global deposition of interstellar radioactive 60Fe, Nature, 532, 69, 10.1038/nature17196 Feige, 2013, AMS measurements of cosmogenic and supernova-ejected radionuclides in deep-sea sediment cores, EPJ Web Conf., 63, 10.1051/epjconf/20136303003 Evaluated Nucleard Data File (ENDF) Riisager, 2014, 11Be(βp) - a quasi-free neutron decay?, Phys. Lett. B, 732, 305, 10.1016/j.physletb.2014.03.062 J. Lachner, M. Ploner, P. Steier, A. Sakaguchi, A. Usui. Accumulation of ferromanganese crusts derived from carrier-free 10Be/9Be. Manuscript submitted to Nucl. Instrum. Methods Phys. Res. B Jeskovsky, 2015, Preliminary AMS measurements of Be-10 at the CENTA facility, Nucl. Instrum. Methods Phys. Res. B, 361, 139, 10.1016/j.nimb.2015.04.072 S.R. Winkler, V. Mbele, S. Mullins. 10-Be at iThembaLABS using a silicon nitride membrane stack as absorber for isobar suppression. Presentation at the AMS-14 Conference in Ottawa, Canada, 2017. Manuscript in Preparation. Scognamiglio, 2019, 10Be low-energy AMS with the passive absorber technique, Nucl. Instrum. Methods Phys. Res. B, 438, 113, 10.1016/j.nimb.2018.07.005