Evaluation of multistep derivatization methods for identification and quantification of oxygenated species in organic aerosol

Journal of Chromatography A - Tập 1418 - Trang 1-11 - 2015
Rosa M. Flores1, Paul V. Doskey1,2,3
1Department of Civil and Environmental Engineering, Michigan Technological University, Houghton, MI 49931, USA
2School of Forest Resources and Environmental Science, Michigan Technological University, Houghton, MI 49931, USA
3Atmospheric Sciences Program, Michigan Technological University, Houghton, MI 49931, USA

Tài liệu tham khảo

Seinfeld, 2006 Hallquist, 2009, The formation, properties and impact of secondary organic aerosol: current and emerging issues, Atmos. Chem. Phys., 9, 5155, 10.5194/acp-9-5155-2009 Liao, 2007, Biogenic secondary organic aerosol over the United States: comparison of climatological simulations with observations, J. Geophys. Res., 112, D06201, 10.1029/2006JD007813 Flores, 2014, Using multidimensional gas chromatography to group secondary organic aerosol species by functionality, Atmos. Environ., 96, 310, 10.1016/j.atmosenv.2014.07.046 Hamilton, 2010, Using comprehensive two-dimensional gas chromatography to study the atmosphere, J. Chromatogr. Sci., 48, 274, 10.1093/chromsci/48.4.274 Kallio, 2006, Comprehensive two-dimensional gas chromatography coupled to time-of-flight mass spectrometry in the identification of organic compounds in atmospheric aerosols from coniferous forest, J. Chromatogr. A, 1125, 234, 10.1016/j.chroma.2006.05.050 Hamilton, 2004, Partially oxidised organic components in urban aerosol using GCXGC-TOF/MS, Atmos. Chem. Phys., 4, 1279, 10.5194/acp-4-1279-2004 Jennings, 1980 Jaoui, 2012, SOA formation from the atmospheric oxidation of 2-methyl-3-buten-2-ol and its implications for PM2.5, Atmos. Chem. Phys., 12, 2173, 10.5194/acp-12-2173-2012 Surratt, 2010, Reactive intermediates revealed in secondary organic aerosol formation from isoprene, P. Natl. Acad. Sci. U.S.A., 107, 6640, 10.1073/pnas.0911114107 Szmigielski, 2007, Characterization of 2-methylglyceric acid oligomers in secondary organic aerosol formed from the photooxidation of isoprene using trimethylsilylation and gas chromatography/ion trap mass spectrometry, J. Mass Spectrom., 42, 101, 10.1002/jms.1146 Connelly, 2012, Heterogeneous glyoxal oxidation: a potential source of secondary organic aerosol, J. Phys. Chem. A, 116, 6180, 10.1021/jp211502e Edney, 2003, Polar organic oxygenates in PM2.5 at a southeastern site in the United States, Atmos. Environ., 37, 3947, 10.1016/S1352-2310(03)00461-8 Fu, 2009, Isoprene, monoterpene, and sesquiterpene oxidation products in the high Arctic aerosols during late winter to early summer, Environ. Sci. Technol., 43, 4022, 10.1021/es803669a Fu, 2009, Summertime contributions of isoprene, monoterpenes, and sesquiterpene oxidation to the formation of secondary organic aerosol in the troposphere over Mt. Tai, Central East China during MTX2006, Atmos. Chem. Phys. Discuss., 9, 16941 Kundu, 2010, Seasonal variations of diacids, ketoacids, and α-dicarbonyls in aerosols at Gosan, Jeju Island, South Korea: Implications for sources, formation, and degradation during long-range transport, J. Geophys. Res., 115, D19307, 10.1029/2010JD013973 Jaoui, 2010, Formation of organic tracers for isoprene SOA under acidic conditions, Atmos. Environ., 44, 1798, 10.1016/j.atmosenv.2010.01.018 Chiappini, 2012, Secondary organic aerosols formation in indoor environment: the role of housecleaning products, Pollut. Atmosphérique, 99, 213 Pietrogrande, 2010, GC–MS analysis of low-molecular-weight dicarboxylic acids in atmospheric aerosol: comparison between silylation and esterification derivatization procedures, Anal. Bioanal. Chem., 396, 877, 10.1007/s00216-009-3212-z Hyder, 2012, Yearly trend of dicarboxylic acids in organic aerosols from south of Sweden and source attribution, Atmos. Environ., 57, 197, 10.1016/j.atmosenv.2012.04.027 Kawamura, 2012, Low molecular weight (C1-C10) monocarboxylic acids, dissolved organic carbon and major inorganic ions in alpine snow pit sequence from a high mountain site, central Japan, Atmos. Environ., 62, 272, 10.1016/j.atmosenv.2012.08.018 Šťávová, 2011, Limits of detection for the determination of mono- and dicarboxylic acids using gas and liquid chromatographic methods coupled with mass spectrometry, J. Chromatogr. B, 879, 1429, 10.1016/j.jchromb.2010.11.027 Temime, 2007, A denuder-filter sampling technique for the detection of gas and particle phase carbonyl compounds, Environ. Sci. Technol., 41, 6514, 10.1021/es070802v Yu, 1997, Atmospheric photooxidation of alkylbenzenes – I. Carbonyl product analyses, Atmos. Environ., 31, 2261, 10.1016/S1352-2310(97)00011-3 Rossignol, 2012, Development of parallel sampling and analysis for the elucidation of gas/particle partitioning of oxygenated semi-volatile organics: a limonene ozonolysis study, Atmos. Meas. Tech., 5, 1459, 10.5194/amt-5-1459-2012 Healy, 2008, Gas/particle partitioning of carbonyls in the photooxidation of isoprene and 1,3,5-trimethylbenzene, Atmos. Chem. Phys., 8, 3215, 10.5194/acp-8-3215-2008 Forester, 2009, Yields of carbonyl products from gas-phase reactions of fragrance compounds with OH radical and ozone, Environ. Sci. Technol., 43, 3561, 10.1021/es803465v Pashynska, 2002, Development of a gas chromatographic/ion trap mass spectrometric method for the determination of levoglucosan and saccharidic compounds in atmospheric aerosols. Application to urban aerosols, J. Mass Spectrom., 37, 1249, 10.1002/jms.391 Wang, 2005, Characterization of oxygenated derivatives of isoprene related to 2-methyltetrols in Amazonian aerosols using trimethylsilylation and gas chromatography/ion trap mass spectrometry, Rapid Commun. Mass Spectrom., 19, 1343, 10.1002/rcm.1940 Chan, 2010, Characterization and quantification of isoprene-derived epoxydiols in ambient aerosol in the Southeastern United States, Environ. Sci. Technol., 44, 4590, 10.1021/es100596b Chiappini, 2006, Development of a supercritical fluid extraction–gas chromatography–mass spectrometry method for the identification of highly polar compounds in secondary organic aerosols formed from biogenic hydrocarbons in smog chamber experiments, Anal. Bioanal. Chem., 386, 1749, 10.1007/s00216-006-0744-3 Pietrogrande, 2011, GC–MS analysis of water-soluble organics in atmospheric aerosol: response surface methodology for optimizing silyl-derivatization for simultaneous analysis of carboxylic acids and sugars, Anal. Chim. Acta, 689, 257, 10.1016/j.aca.2011.01.047 Kourtchev, 2005, Observation of 2-methyltetrols and related photo-oxidation products of isoprene in boreal forest aerosols from Hyytiälä, Finland, Atmos. Chem. Phys., 5, 2761, 10.5194/acp-5-2761-2005 Borrás, 2012, Determination of oxygenated compounds in secondary organic aerosol from isoprene and toluene smog chamber experiments, Int. J. Environ. Anal. Chem., 92, 110, 10.1080/03067319.2011.572164 Yu, 1998, Identification of products containing –COOH, –OH, and –CO in atmospheric oxidation of hydrocarbons, Environ. Sci. Technol., 32, 2357, 10.1021/es980129x Lewandowski, 2007, Composition of PM2.5 during the summer of 2003 in Research Triangle Park, North Carolina, Atmos. Environ., 41, 4073, 10.1016/j.atmosenv.2007.01.012 Cocker, 2001, The effect of water on gas–particle partitioning of secondary organic aerosol: II. m-xylene and 1,3,5-trimethylbenzene photooxidation systems, Atmos. Environ., 35, 6073, 10.1016/S1352-2310(01)00405-8 Kubátová, 2000, Carbonaceous aerosol characterization in the Amazon Basin, Brazil: novel dicarboxylic acids and related compounds, Atmos. Environ., 34, 5037, 10.1016/S1352-2310(00)00320-4 Jaoui, 2004, Identification and quantification of aerosol polar oxygenated compounds bearing carboxylic or hydroxyl Groups. 1. Method development, Anal. Chem., 76, 4765, 10.1021/ac049919h Kowalewski, 2011, Multistep derivatization method for the determination of multifunctional oxidation products from the reaction of α-pinene with ozone, J. Chromatogr. A, 1218, 7264, 10.1016/j.chroma.2011.08.061 Le Lacheur, 1993, Identification of carbonyl compounds in environmental samples, Environ. Sci. Technol., 27, 2745, 10.1021/es00049a013 Jaoui, 2006, Analysis of secondary organic aerosol compounds from the photooxidation of d-limonene in the presence of NOX and their detection in ambient PM2.5, Environ. Sci. Technol., 40, 3819, 10.1021/es052566z Jaoui, 2005, Identification and quantification of aerosol polar oxygenated compounds bearing carboxylic or hydroxyl groups. 2. Organic tracer compounds from monoterpenes, Environ. Sci. Technol., 39, 5661, 10.1021/es048111b Kawamura, 1993, Identification of C2-C10 .omega.-oxocarboxylic acids, pyruvic acid, and C2-C3 .alpha.-dicarbonyls in wet precipitation and aerosol samples by capillary GC and GC/MS, Anal. Chem., 65, 3505, 10.1021/ac00071a030 Li, 2005, Simultaneous determination of mono- and dicarboxylic acids, ω-oxo-carboxylic acids, midchain ketocarboxylic acids, and aldehydes in atmospheric aerosol samples, Environ. Sci. Technol., 39, 7616, 10.1021/es050896d Hsu, 2009, Determination of low-molecular-weight dicarboxylic acids in atmospheric aerosols by injection-port derivatization and gas chromatography–mass spectrometry, Talanta, 80, 1025, 10.1016/j.talanta.2009.07.047 Limbeck, 2001, Semivolatile behavior of dicarboxylic acids and other polar organic species at a rural background site (Nylsvley, RSA), Atmos. Environ., 35, 1853, 10.1016/S1352-2310(00)00497-0 Ray, 2005, Dicarboxylic acid concentration trends and sampling artifacts, Atmos. Environ., 39, 7906, 10.1016/j.atmosenv.2005.09.024 Lewandowski, 2008, Primary and secondary contributions to ambient PM in the Midwestern United States, Environ. Sci. Technol., 42, 3303, 10.1021/es0720412 Moretti, 2008, NMR determination of total carbonyls and carboxyls: a tool for tracing the evolution of atmospheric oxidized organic aerosols, Environ. Sci. Technol., 42, 4844, 10.1021/es703166v Lamoureux, 2009, A comparison of several modern alkylating agents, ARKIVOC i, 251, 10.3998/ark.5550190.0010.108 Hodnet, 2003, Trimethylsilyldiazomethane, Synlett, 2003, 2095, 10.1055/s-2003-42031 Little, 1999, Artifacts in trimethylsilyl derivatization reactions and ways to avoid them, J. Chromatogr. A, 844, 1, 10.1016/S0021-9673(99)00267-8 Flores, 2013 Doskey, 1986, High-volume sampling of airborne polychlorobiphenyls with amberlite XAD-2 resin, Anal. Chim. Acta, 110, 129, 10.1016/S0003-2670(01)83538-8 Middleditch, 1972, The mass spectra of some o-methyloximes of aliphatic aldehydes and ketones, Org. Mass Spectrom., 6, 179, 10.1002/oms.1210060208 Lebedev, 2012 Castillo, 2011, Data analysis tool for comprehensive two-dimensional gas chromatography/time-of-flight mass spectrometry, Anal. Chem., 83, 3058, 10.1021/ac103308x