Octadecanuclear Cluster or 1D Polymer with [{ML}₂Nb(CN)₈]_nMotifs as a Function of {ML} (M = Ni(II),n= 6; M = Mn(II),n= ∞; L = Macrocycle)

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Preparation, 40 mL), a solution of [K4Nb(CN)8·2H2O]15 (37 mg, 0.075 mmol) was allowed to slowly diffuse into a H2O solution of {MnL}Cl2 16 (77 mg, 0.15 mmol) yielding 1 (50 mg, yield = 31%) as light-orange needles