13-halo derivatives of ent-kauranoic acid. Synthesis and structure

Russian Journal of General Chemistry - Tập 81 - Trang 927-930 - 2011
R. N. Khaibullin1, M. G. Kurochkina1, I. Yu. Strobykina1, A. B. Dobrynin1, V. E. Kataev1
1Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan, Tatarstan, Russia

Tóm tắt

The ent-kauranoic acid 13-chloro-, bromo- and iodo-derivatives were synthesized in quantitative yield. Their molecular structure was established by the X-ray diffraction analysis.

Tài liệu tham khảo

Garcia, P.A., de Oliveira, A.B., and Batista, R., Molecules, 2007, vol. 12, no. 3, p. 455. Ghisalberti, E.L., Fitoterapia, 1997, no. 68, p. 303. Avent, A.G., Hanson, J.R., Hitchcock, P.B., and Oliveira, B.H., J. Chem. Soc. Perkin Trans 1, 1990, p. 2661. Khaibullin, R.N., Strobykina, I.Yu., Kataev, V.E., Lodochnikova, O.A., Gubaidullin, A.T., and Musin, R.Z., Zh. Obshch. Khim., 2009, no. 79, p. 795. Olah, G.A., Narang, S.C., Balaram, Gupta, B.G., and Malhotra, R., J. Org. Chem., 1979, vol. 44, p. 1247. Altomare, A., Cascarano, G., Giacovazzo, C., and Viterbo, D., Acta Crystallogr. Sec. A, 1991, vol. 47, no. 6, p. 744. Sheldrick, G.M., SHELXL-97 A Computer Program for Crystal Structure Determination, University for Gottingen, 1997 Farrugia, L.J., J. Appl. Crystallogr., 1999, vol. 32, p. 837.