Synthesis of Hydroxyapatite Coatings with Hexagonal Crystal Structure on Etched Titanium by Hydrothermal Method

Duong Thanh Tung1, Nguyen Thi Lan1, Bui Thi Hue1, Hoang Van Vuong2, Hoang Nhu Van3, Nguyen Viet Tung1, Pham Hung Vuong4, Nguyen Huu Thong1, Le Thai Hung2, Cao Xuan Thang1, Le Quynh Duong5, Le Van Toan6
1International Training Institute for Materials Science (ITIMS), Hanoi University of Science and Technology (HUST), No 01, Dai Co Viet Road, Hanoi, Vietnam
2School of Materials Science and Engineering, Hanoi University of Science and Technology (HUST), No 01, Dai Co Viet Road, Hanoi, Vietnam
3Faculty of Materials Science and Engineering, Phenikaa University, Yen Nghia, Ha-Dong District, Hanoi 1000, Viet Nam
4HUST
5International Training Institute for Materials Science (ITIMS), Hanoi University of Science and Technology (HUST)

Tóm tắt

Hydroxyapatite (HAp) has been successfully coated on etched titanium substrates by hydrothermal method using solutions of Ca(NO3)2.4H2O, NH4H2PO4 at 200 oC for 12 h. Results obtained from measurements on the modern physical methods of FE-SEM and XRD showedhat the structure of HAp has a regular hexagonal morphology belonging to the space group P63/m. The degree of HAp nucleation and nucleation development on the un-etched titanium plates was lower than that on the etched titanium plates. In vitro bioactivity of HAp-coated titanium testing using SBF solution showed prospective results. Keywords: Hydroxyapatite (HAp), Hydrothermal method, etched, titanium.