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Three macroinitiators with different chain lengths were extended with poly(butyl acrylate) (PBA) to form ABA triblock copolymers. The structure and dynamics of the ABA triblock copolymers with PSU central segments and various molecular weight PBA side chains were investigated by small‐angle X‐ray scattering and rheology. The block copolymers form micelles with a PSU core and PBA corona. The length of each block has an important effect on the structure and resulting dynamics of the copolymers. Dynamic mechanical measurements indicate three relaxation modes: (i) PBA segmental relaxation at high frequency; (ii) PBA relaxation of the corona block at intermediate frequency; (iii) an additional relaxation process related to structural rearrangement of the micelles at low frequency. 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DSC results showed that the binary blends of epoxy with PEO (and\u002For PCL) are fully miscible in the entire composition in the amorphous state. FTIR indicates that there were interchain specific interactions between the crosslinked epoxy and the linear polymers in the binary blends and the hydrogen bonding interactions between epoxy and PCL are much weaker than those between epoxy and PEO. The difference in the strength of interchain specific interactions gives rise to the competitive hydrogen bonding interactions in the ternary blends of epoxy, PEO and PCL, which were evidenced by the results of FTIR. The results of optical microscopy and DSC showed that in the ternary blends PCL component separated out with inclusion of PEO. The formation of the specific phase structures is ascribed to the competitive interchain specific interactions among the crosslinked epoxy, PEO and PCL.\u003C\u002Fjats:p>\u003Cjats:p>\u003Cjats:boxed-text content-type=\"graphic\" position=\"anchor\">\u003Cjats:caption>\u003Cjats:p>Phase boundary diagram of epoxy, PEO and PCL ternary blends.\u003C\u002Fjats:p>\u003C\u002Fjats:caption>\u003Cjats:graphic xmlns:xlink=\"http:\u002F\u002Fwww.w3.org\u002F1999\u002Fxlink\" position=\"anchor\" xlink:href=\"urn:x-wiley:10221352:media:MACP200400512:gra001\">\u003Cjats:alt-text>image\u003C\u002Fjats:alt-text>\u003Cjats:caption>\u003Cjats:p>Phase boundary diagram of epoxy, PEO and PCL ternary blends.\u003C\u002Fjats:p>\u003C\u002Fjats:caption>\u003C\u002Fjats:graphic>\u003C\u002Fjats:boxed-text>\u003C\u002Fjats:p>",{"EN":520},"Ternary Thermosetting Blends of Epoxy Resin, Poly(ethylene oxide) and Poly(\u003Ci>ε\u003C\u002Fi>‐caprolactone)",{"VOID":522},"10.1002\u002Fmacp.200400512",[158],"https:\u002F\u002Fonlinelibrary.wiley.com\u002Fdoi\u002F10.1002\u002Fmacp.200400512",[526,546],{"id":527,"sortIndex":25,"researcher":24,"roles":528,"affiliations":529,"properties":541},"996e0396-3c0e-4efd-a085-078fc5d5586b",[],[530],{"id":531,"sortIndex":25,"affiliation":532,"properties":24},"69ca7fb7-024e-4126-8366-e70a2602731f",{"id":533,"createTime":534,"updateTime":535,"relativeEntities":536,"slug":537,"properties":538,"entityType":77,"verifyStatus":23,"verifyTime":24,"verifyNote":24,"syncStatus":23,"languages":24,"translateLanguages":24,"viewCount":25},"0c1964c4-4811-45ab-9a7b-dabf5de599df","2024-10-04T22:28:07.917+00:00","2025-06-12T00:56:14.985+00:00",[],"Department-of-Polymer-Science-and-Engineering-Shanghai-Jiao-Tong-University-Shanghai-200240-P-R-China",{"title":539},{"EN":540},"Department of Polymer Science and Engineering, Shanghai Jiao Tong University, Shanghai 200240, P. 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The POSS macromer is used to synthesize PEO‐\u003Cjats:italic>b\u003C\u002Fjats:italic>‐P(MA‐POSS)‐\u003Cjats:italic>b\u003C\u002Fjats:italic>‐PNIPAAm triblock copolymers via sequential atom transfer radical polymerization (ATRP). The organic‐inorganic, amphiphilic and thermoresponsive ABC triblock copolymers are characterized by means of nuclear magnetic resonance spectroscopy (NMR) and gel permeation chromatography (GPC). Differential scanning calorimetry (DSC) and atomic force microscopy (AFM) show that the hybrid ABC triblock copolymers are microphase‐separated in bulk. Cloud point measurements show that the effect of the hydrophiphilic block (i.e. PEO) on the LCSTs is more pronounced than the hydrophobic block (i.e. P(MA‐POSS)). Both transmission electron microscopy (TEM) and dynamic light scattering (DLS) show that all the triblock copolymers can be self‐organized into micellar aggregates in aqueous solutions. The sizes of the micellar aggregates can be modulated by changing the temperature. The temperature‐tunable self‐assembly behavior is interpreted using a combination of the highly hydrophobicity of P(MA‐POSS), the water‐solubility of PEO and the thermoresponsive property of PNIPAAm in the triblock copolymers.\u003C\u002Fjats:p>",{"EN":769},"Synthesis and Self‐Assembly Behavior of Organic–Inorganic Poly(ethylene oxide)‐\u003Ci>block\u003C\u002Fi>‐Poly(MA POSS)‐\u003Ci>block\u003C\u002Fi>‐Poly(\u003Ci>N\u003C\u002Fi>‐isopropylacrylamide) Triblock Copolymers",{"VOID":771},"10.1002\u002Fmacp.201100506",[158],"https:\u002F\u002Fonlinelibrary.wiley.com\u002Fdoi\u002F10.1002\u002Fmacp.201100506",[775,794,811,828],{"id":776,"sortIndex":252,"researcher":24,"roles":777,"affiliations":778,"properties":790},"89b32725-7a0f-46aa-b11e-762e09826c85",[],[779],{"id":780,"sortIndex":25,"affiliation":781,"properties":24},"6e60d778-b36e-4de1-839c-725923f096d7",{"id":782,"createTime":783,"updateTime":784,"relativeEntities":785,"slug":786,"properties":787,"entityType":77,"verifyStatus":23,"verifyTime":24,"verifyNote":24,"syncStatus":23,"languages":24,"translateLanguages":24,"viewCount":25},"080af9ef-a7f1-4273-bacf-57ac5ec715ff","2024-08-31T14:56:19.021+00:00","2025-06-11T21:03:26.705+00:00",[],"Department-of-Polymer-Science-and-Engineering-and-State-Key-Laboratory-of-Metal-Matrix-Composites-Shanghai-Jiao-Tong-University-Shanghai-200240-P-R-China",{"title":788},{"EN":789},"Department of Polymer Science and Engineering and State Key Laboratory of Metal Matrix Composites, Shanghai Jiao Tong University, Shanghai 200240, P. 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Analysis of these novel ethylene–propylene–POSS polymers using wide‐angle X‐ray diffraction reveals that pendant POSS groups off the polymer backbones aggregate with a phenyl periphery, and the polymers crystallize as anisotropically shaped nanocrystals. POSS particle aggregation is strongly dependent on the nature of the POSS peripheral group. X‐Ray studies suggest that aggregation of POSS in the EP elastomers did not occur with isobutyl and ethyl peripheries, as they disperse within the polymer matrix. The formation of POSS nanocrystals increases the mechanical properties of these thermoplastic elastomers. The tensile storage modulus increases significantly with the addition of POSS, as does the length of the rubbery plateau region. Tensile studies reveal an elongation at break of 720% for one EP‐phenyl POSS polymer sample, with the others between 400 and 500%.\u003C\u002Fjats:p>\u003Cjats:p>\u003Cjats:boxed-text content-type=\"graphic\" position=\"anchor\">\u003Cjats:graphic xmlns:xlink=\"http:\u002F\u002Fwww.w3.org\u002F1999\u002Fxlink\" mimetype=\"image\u002Fgif\" position=\"anchor\" specific-use=\"enlarged-web-image\" xlink:href=\"graphic\u002Fmgra001.gif\">\u003Cjats:alt-text>magnified image\u003C\u002Fjats:alt-text>\u003C\u002Fjats:graphic>\u003C\u002Fjats:boxed-text>\n\u003C\u002Fjats:p>",{"EN":1053},"Ethylene–Propylene–Silsesquioxane Thermoplastic Elastomers",{"VOID":1055},"10.1002\u002Fmacp.200800065",[158],"https:\u002F\u002Fonlinelibrary.wiley.com\u002Fdoi\u002F10.1002\u002Fmacp.200800065",[1059,1080],{"id":1060,"sortIndex":189,"researcher":24,"roles":1061,"affiliations":1062,"properties":1073},"f8842830-a3f6-47de-9621-3c288c5332c8",[],[1063],{"id":1064,"sortIndex":25,"affiliation":1065,"properties":24},"64548830-a628-459f-98cd-9774eb49d6fb",{"id":1066,"createTime":1067,"updateTime":1067,"relativeEntities":1068,"slug":1069,"properties":1070,"entityType":77,"verifyStatus":23,"verifyTime":24,"verifyNote":24,"syncStatus":23,"languages":24,"translateLanguages":24,"viewCount":25},"302d50f4-91c5-436f-97a5-8f917cab46f1","2024-10-13T22:10:43.725+00:00",[],"Department-of-Polymer-Science-and-Engineering-University-of-Massachusetts-Amherst-Amherst-MA-01003-USA",{"title":1071},{"EN":1072},"Department of Polymer Science and Engineering, University of Massachusetts-Amherst, Amherst, MA 01003, USA",{"openalex":1074,"orcid":1076,"title":1078},{"VOID":1075},"A5015628914",{"VOID":1077},"https:\u002F\u002Forcid.org\u002F0000-0001-7065-4366",{"EN":1079},"E. 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IRI, 33, 2",{},{"id":24,"text":1254,"url":24,"identifiers":1255},"Aklonis J., 1983, Introduction to Polymer Viscoelasticity",{},{"id":1257,"createTime":1258,"updateTime":1258,"relativeEntities":1259,"slug":1260,"properties":1261,"entityType":154,"verifyStatus":155,"verifyTime":1258,"verifyNote":156,"syncStatus":23,"languages":1273,"translateLanguages":24,"viewCount":25,"primaryUrl":1274,"fullTextUrl":24,"authors":1275,"publicationType":297,"publisherRelationship":1307,"citationCount":1339,"citationInfo":1340,"publishDate":1342,"publishYear":1147,"citationAnalyzeStatus":23,"lastCitationAnalyze":24,"indexDatabases":24,"openAccess":24,"references":1343,"isForceReanalyzing":505},"afa8bd80-5d61-4c8c-baf9-10627f2103c8","2024-10-13T22:10:39.500+00:00",[],"Fluoroelastomer-Copolymers-Incorporating-Polyhedral-Oligomeric-Silsesquioxane",{"mag":1262,"keywords":1264,"openalex":1265,"abstract":1267,"title":1269,"doi":1271},{"VOID":1263},"2011553498",{},{"VOID":1266},"W2011553498",{"EN":1268},"\u003Cjats:title>Abstract\u003C\u002Fjats:title>\u003Cjats:p>The aggregation of polyhedral oligomeric silsesquioxane (POSS) in copolymers was studied by incorporation of POSS into fluorinated copolymers, namely poly(octafluoropentyl acrylate) elastomers. The aggregation of POSS in copolymers affords unique materials. Studies of these novel polymers show POSS aggregates in these copolymers with both the phenyl and isobutyl peripheries, as the chain‐repulsive fluorinated chains help drive this aggregation. The isooctylPOSS copolymers, however, do not have POSS aggregation. Thermal studies of these copolymers also show an increase in the decomposition temperature by incorporation of POSS, which is directly dependent on the POSS periphery.\u003C\u002Fjats:p>\u003Cjats:p>\u003Cjats:boxed-text content-type=\"graphic\" position=\"anchor\">\u003Cjats:graphic xmlns:xlink=\"http:\u002F\u002Fwww.w3.org\u002F1999\u002Fxlink\" mimetype=\"image\u002Fgif\" position=\"anchor\" specific-use=\"enlarged-web-image\" xlink:href=\"graphic\u002Fmgra001.gif\">\u003Cjats:alt-text>magnified image\u003C\u002Fjats:alt-text>\u003C\u002Fjats:graphic>\u003C\u002Fjats:boxed-text>\n\u003C\u002Fjats:p>",{"EN":1270},"Fluoroelastomer Copolymers Incorporating Polyhedral Oligomeric Silsesquioxane",{"VOID":1272},"10.1002\u002Fmacp.200800220",[158],"https:\u002F\u002Fonlinelibrary.wiley.com\u002Fdoi\u002F10.1002\u002Fmacp.200800220",[1276,1294],{"id":1277,"sortIndex":189,"researcher":24,"roles":1278,"affiliations":1279,"properties":1290},"e9b5abeb-7ad0-4049-97c6-090c21f79f21",[],[1280],{"id":1281,"sortIndex":25,"affiliation":1282,"properties":24},"f4b47fff-1603-4776-af90-0454705dc27d",{"id":1283,"createTime":1284,"updateTime":1284,"relativeEntities":1285,"slug":1286,"properties":1287,"entityType":77,"verifyStatus":23,"verifyTime":24,"verifyNote":24,"syncStatus":23,"languages":24,"translateLanguages":24,"viewCount":25},"ff35028e-78a1-4cb0-ad91-49cc1e2155d7","2024-10-13T22:10:39.524+00:00",[],"Department-of-Polymer-Science-and-Engineering-University-of-Massachusetts-Amherst-Amherst-Massachusetts-01003-USA",{"title":1288},{"EN":1289},"Department of Polymer Science and Engineering, University of Massachusetts Amherst, Amherst, Massachusetts 01003, 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OpePOSS was incorporated into polyurethane to make organic‐inorganic hybrid composites and nano‐composites containing up to 20 wt.‐% POSS were prepared. The formation of the hybrid polyurethane networks is ascribed to two principal cross‐linking reactions: i) the cross‐linking reaction between MOCA and the polyurethane prepolymer and ii) the inter‐component reaction between the PU networks and OpePOSS. The latter was confirmed by model compound reactions. TEM indicates that the POSS was homogeneously dispersed in the polymer matrix at the nanometer scale. DSC showed that the nanocomposites displayed increased glass transition temperatures compared to the control polyurethane. In terms of TGA, the nanocomposites displayed improved thermal stability. Tensile tests indicate that the organic‐inorganic hybrid networks were significantly reinforced with the inclusion of POSS. Contact angle measurements show that the organic‐inorganic nanocomposites displayed a significant enhancement in surface hydrophobicity as well as a reduction in the surface free energy. The improvement in surface properties was ascribed to the presence of the POSS moiety in place of the polar component of polyurethane. XPS shows enrichment with Si‐containing moieties on the surfaces.\u003C\u002Fjats:p>\u003Cjats:p>\u003Cjats:boxed-text content-type=\"graphic\" position=\"anchor\">\u003Cjats:caption>\u003Cjats:p>Organic‐Inorganic Hybrid PU Networks.\u003C\u002Fjats:p>\u003C\u002Fjats:caption>\u003Cjats:graphic xmlns:xlink=\"http:\u002F\u002Fwww.w3.org\u002F1999\u002Fxlink\" mimetype=\"image\u002Fgif\" position=\"anchor\" specific-use=\"enlarged-web-image\" xlink:href=\"graphic\u002Fmgra001.gif\">\u003Cjats:alt-text>magnified image\u003C\u002Fjats:alt-text>\u003Cjats:caption>\u003Cjats:p>Organic‐Inorganic Hybrid PU Networks.\u003C\u002Fjats:p>\u003C\u002Fjats:caption>\u003C\u002Fjats:graphic>\u003C\u002Fjats:boxed-text>\n\u003C\u002Fjats:p>",{"EN":1443},"Polyurethane Networks Modified with Octa(propylglycidyl ether) Polyhedral Oligomeric Silsesquioxane",{"VOID":1445},"10.1002\u002Fmacp.200600241",[158],"https:\u002F\u002Fonlinelibrary.wiley.com\u002Fdoi\u002F10.1002\u002Fmacp.200600241",[1449,1469,1486],{"id":1450,"sortIndex":189,"researcher":24,"roles":1451,"affiliations":1452,"properties":1464},"4d46ce8e-b2a9-4d98-a7bd-339d77cba05c",[],[1453],{"id":1454,"sortIndex":25,"affiliation":1455,"properties":24},"300f3ddc-09a5-4069-a60a-1f525acf605f",{"id":1456,"createTime":1457,"updateTime":1458,"relativeEntities":1459,"slug":1460,"properties":1461,"entityType":77,"verifyStatus":23,"verifyTime":24,"verifyNote":24,"syncStatus":23,"languages":24,"translateLanguages":24,"viewCount":25},"69d8b3dc-5edc-490d-9d97-39936d3fd486","2024-01-07T07:51:47.505+00:00","2024-10-13T22:10:19.795+00:00",[],"Department-of-Polymer-Science-and-Engineering-Shanghai-Jiao-Tong-University-800-Dongchuan-Road-Shanghai-200240-China",{"title":1462},{"VI":1463},"Department of Polymer Science and Engineering, Shanghai Jiao Tong University, 800 Dongchuan Road, Shanghai 200240, China",{"openalex":1465,"title":1467},{"VOID":1466},"A5100945693",{"EN":1468},"Yong Ni",{"id":1470,"sortIndex":25,"researcher":24,"roles":1471,"affiliations":1472,"properties":1479},"7dc789f4-b3ec-47c0-a898-de39c7009425",[],[1473],{"id":1474,"sortIndex":25,"affiliation":1475,"properties":24},"ae6542ea-32e1-4b04-a552-6e241e199d8a",{"id":1456,"createTime":1457,"updateTime":1458,"relativeEntities":1476,"slug":1460,"properties":1477,"entityType":77,"verifyStatus":23,"verifyTime":24,"verifyNote":24,"syncStatus":23,"languages":24,"translateLanguages":24,"viewCount":25},[],{"title":1478},{"VI":1463},{"openalex":1480,"orcid":1482,"title":1484},{"VOID":1481},"A5088756195",{"VOID":1483},"https:\u002F\u002Forcid.org\u002F0000-0003-4496-9270",{"EN":1485},"Yonghong Liu",{"id":1487,"sortIndex":178,"researcher":24,"roles":1488,"affiliations":1489,"properties":1500},"cb3f8dda-e425-45d9-9f6b-bf0d40840c95",[],[1490],{"id":1491,"sortIndex":25,"affiliation":1492,"properties":24},"868a5ce0-8e10-4fff-9902-05df0fcc45f0",{"id":1493,"createTime":1494,"updateTime":1494,"relativeEntities":1495,"slug":1496,"properties":1497,"entityType":77,"verifyStatus":23,"verifyTime":24,"verifyNote":24,"syncStatus":23,"languages":24,"translateLanguages":24,"viewCount":25},"5e553585-c05c-405b-b7c6-dec9a1783a11","2024-10-13T22:10:19.839+00:00",[],"Department-of-Polymer-Science-and-Engineering-Shanghai-Jiao-Tong-University-800-Dongchuan-Road-Shanghai-200240-China-Fax-86-21-5474-1297",{"title":1498},{"EN":1499},"Department of Polymer Science and Engineering, Shanghai Jiao Tong University, 800 Dongchuan Road, Shanghai 200240, China. Fax: +86 21 5474 1297",{"openalex":1501,"orcid":1502,"title":1503},{"VOID":563},{"VOID":565},{"EN":567},{"url":24,"publisher":1505,"properties":1530},{"id":6,"createTime":7,"updateTime":8,"relativeEntities":1506,"slug":10,"properties":1507,"entityType":22,"verifyStatus":23,"verifyTime":24,"verifyNote":24,"syncStatus":23,"languages":24,"translateLanguages":24,"viewCount":25,"subjectFields":1513,"manageAffiliations":1514,"indexDatabases":1515,"url":132,"thumbnailPath":24,"statistic":24,"gsStatistic":24,"type":24,"analyzePriority":24},[],{"country":1508,"issn":1509,"introduce":1510,"eissn":1511,"title":1512},{"VOID":13},{"VOID":15},{"EN":17},{"VOID":19},{"EN":21},[],[],[1516,1523],{"id":110,"indexDatabase":1517,"url":123,"indexYears":124,"academicFieldIds":1522,"indexDatabaseRanking":131},{"id":112,"createTime":113,"updateTime":114,"relativeEntities":1518,"label":1519,"description":1520,"key":120,"publicationTags":1521,"standard":24},[],{"EN":117,"VI":117},{"EN":117,"VI":119},[122],[126,127,128,129,130],{"id":91,"indexDatabase":1524,"url":106,"indexYears":24,"academicFieldIds":1529,"indexDatabaseRanking":24},{"id":93,"createTime":94,"updateTime":95,"relativeEntities":1525,"label":1526,"description":1527,"key":102,"publicationTags":1528,"standard":24},[],{"EN":98,"VI":98},{"VI":100,"EN":101},[104,105],[108],{"volume":1531,"pages":1533,"issue":1535},{"VOID":1532},"207",{"VOID":1534},"1842-1851",{"VOID":1536},"20",82,{"total":1537,"publishYear":24,"statisticByYear":1539},{"2012":163,"2013":1540,"2014":163,"2015":603,"2016":1540,"2017":252,"2018":603,"2019":252,"2020":163,"2021":604,"2022":189,"2023":189,"2024":189},8,"2006-10-24",2006,[1544,1547,1550,1553,1555,1558,1560,1563,1566,1569,1572,1575,1577,1580,1583,1586,1588,1590,1592,1595,1598,1601,1603,1606,1609,1611,1614,1617,1620,1623,1626,1629,1632,1635,1638,1641,1644,1647,1650,1653,1656,1658,1661,1664,1667,1670,1673,1676,1679,1682,1685,1688],{"id":24,"text":1545,"url":24,"identifiers":1546},"10.1126\u002Fscience.1962191",{"doi":1545},{"id":24,"text":1548,"url":24,"identifiers":1549},"10.1016\u002FS0022-328X(96)06821-0",{"doi":1548},{"id":24,"text":1551,"url":24,"identifiers":1552},"10.1021\u002Fcr00037a013",{"doi":1551},{"id":24,"text":884,"url":24,"identifiers":1554},{"doi":884},{"id":24,"text":1556,"url":24,"identifiers":1557},"10.1007\u002F3-540-69711-X_3",{"doi":1556},{"id":24,"text":887,"url":24,"identifiers":1559},{"doi":887},{"id":24,"text":1561,"url":24,"identifiers":1562},"10.1021\u002Fcm00059a023",{"doi":1561},{"id":24,"text":1564,"url":24,"identifiers":1565},"Andrews M. 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Mater. Sci. Eng., 82, 235",{},{"id":24,"text":1668,"url":24,"identifiers":1669},"10.1021\u002Fja010720l",{"doi":1668},{"id":24,"text":1671,"url":24,"identifiers":1672},"10.1021\u002Fma030309d",{"doi":1671},{"id":24,"text":1674,"url":24,"identifiers":1675},"10.1016\u002FS0169-1317(99)00009-5",{"doi":1674},{"id":24,"text":1677,"url":24,"identifiers":1678},"10.1016\u002Fj.progpolymsci.2003.08.002",{"doi":1677},{"id":24,"text":1680,"url":24,"identifiers":1681},"10.1080\u002F0021846708544579",{"doi":1680},{"id":24,"text":1683,"url":24,"identifiers":1684},"Kaelble D. H., 1971, Physical Chemistry of Adhesion",{},{"id":24,"text":1686,"url":24,"identifiers":1687},"10.1021\u002Fma047636l",{"doi":1686},{"id":24,"text":1689,"url":24,"identifiers":1690},"10.1021\u002Fma961442r",{"doi":1689},{"id":1692,"createTime":1693,"updateTime":1693,"relativeEntities":1694,"slug":1695,"properties":1696,"entityType":154,"verifyStatus":155,"verifyTime":1693,"verifyNote":156,"syncStatus":23,"languages":1708,"translateLanguages":24,"viewCount":25,"primaryUrl":1709,"fullTextUrl":24,"authors":1710,"publicationType":297,"publisherRelationship":1742,"citationCount":1773,"citationInfo":1774,"publishDate":1776,"publishYear":335,"citationAnalyzeStatus":23,"lastCitationAnalyze":24,"indexDatabases":24,"openAccess":24,"references":1777,"isForceReanalyzing":505},"b30c7852-3dbf-45aa-aa7b-12508c28b104","2024-10-13T22:10:00.465+00:00",[],"Epoxy-Resin-Containing-Octamaleimidophenyl-Polyhedral-Oligomeric-Silsesquioxane",{"mag":1697,"keywords":1699,"openalex":1700,"abstract":1702,"title":1704,"doi":1706},{"VOID":1698},"2122180817",{},{"VOID":1701},"W2122180817",{"EN":1703},"\u003Cjats:title>Abstract\u003C\u002Fjats:title>\u003Cjats:p>\u003Cjats:bold>Summary:\u003C\u002Fjats:bold> Octamaleimidophenyl polyhedral oligomeric silsesquioxane (OmipPOSS) was synthesized via the imidization reaction between octaaminophenyl polyhedral oligomeric silsesquioxane (OapPOSS) and maleic anhydride, and it was characterized by means of Fourier transform infrared (FTIR) and NMR spectroscopies. OmipPOSS was further employed to prepare epoxy hybrids. The thermosetting hybrids containing OmipPOSS up to 10 wt.‐% were obtained via in situ polymerization of diglycidyl ether of bisphenol A (DGEBA) and 4,4′‐diaminodiphenylmethane (DDM) in the presence of OmipPOSS. High‐resolution transmission electronic microscopy (TEM) indicates that the nanometer‐scaled dispersion of POSS molecules was obtained, suggesting that the nanocomposites were successfully prepared. The results of DSC showed that the glass transition temperatures (\u003Cjats:italic>T\u003C\u002Fjats:italic>\u003Cjats:sub>g\u003C\u002Fjats:sub>'s) of the POSS‐containing nanocomposites are dependent on the content of POSS in the nanocomposites. When the contents of POSS are less than 5 wt.‐%, the nanocomposites displayed the enhanced glass transition temperatures (\u003Cjats:italic>T\u003C\u002Fjats:italic>\u003Cjats:sub>g\u003C\u002Fjats:sub>'s) in comparison with control epoxy. Thermogravimetric analysis (TGA) showed that all the nanocomposites containing POSS displayed improved char yield, suggesting the flame retardance of the materials is improved.\n\u003Cjats:boxed-text content-type=\"graphic\" position=\"anchor\">\u003Cjats:graphic xmlns:xlink=\"http:\u002F\u002Fwww.w3.org\u002F1999\u002Fxlink\" mimetype=\"image\u002Fgif\" position=\"anchor\" specific-use=\"enlarged-web-image\" xlink:href=\"graphic\u002Fmgra001.gif\">\u003Cjats:alt-text>magnified image\u003C\u002Fjats:alt-text>\u003C\u002Fjats:graphic>\u003C\u002Fjats:boxed-text>\n\u003C\u002Fjats:p>",{"EN":1705},"Epoxy Resin Containing Octamaleimidophenyl Polyhedral Oligomeric Silsesquioxane",{"VOID":1707},"10.1002\u002Fmacp.200500267",[158],"https:\u002F\u002Fonlinelibrary.wiley.com\u002Fdoi\u002F10.1002\u002Fmacp.200500267",[1711,1729],{"id":1712,"sortIndex":189,"researcher":24,"roles":1713,"affiliations":1714,"properties":1725},"0e835b59-ff38-42df-8d67-bf6bf76d6e71",[],[1715],{"id":1716,"sortIndex":25,"affiliation":1717,"properties":24},"0c6f37cc-2d82-48ee-bb4f-87b954e2d513",{"id":1718,"createTime":1719,"updateTime":1719,"relativeEntities":1720,"slug":1721,"properties":1722,"entityType":77,"verifyStatus":23,"verifyTime":24,"verifyNote":24,"syncStatus":23,"languages":24,"translateLanguages":24,"viewCount":25},"5c76f7ad-18c6-4c15-b71c-b9377316adf1","2024-10-13T22:10:00.484+00:00",[],"Department-of-Polymer-Science-and-Engineering-Shanghai-Jiao-Tong-University-800-Dongchuan-Road-Shanghai-200240-P-R-China",{"title":1723},{"EN":1724},"Department of Polymer Science and Engineering, Shanghai Jiao Tong University, 800 Dongchuan Road, Shanghai 200240, P. 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The grafting of two hydrophilic vinyl monomers, dimethylaminoethyl acrylate (DMAEA) and dimethylaminoethyl methacrylate (DMAEMA), onto natural rubber latex was carried out by emulsion polymerization using redox initiation. The effects of the redox initiator concentration and type (cumene hydroperoxide\u002Ftetraethylenepentamine, CHP\u002FTEPA; \u003Cjats:italic>tert\u003C\u002Fjats:italic>‐butyl hydroperoxide\u002Ftetraethylenepentamine, \u003Cjats:italic>t\u003C\u002Fjats:italic>‐BHP\u002FTEPA; potassium persulfate\u002Fpotassium metabisulfite, K\u003Cjats:sub>2\u003C\u002Fjats:sub>S\u003Cjats:sub>2\u003C\u002Fjats:sub>O\u003Cjats:sub>8\u003C\u002Fjats:sub>\u002FK\u003Cjats:sub>2\u003C\u002Fjats:sub>S\u003Cjats:sub>2\u003C\u002Fjats:sub>O\u003Cjats:sub>5\u003C\u002Fjats:sub>), the monomer concentration and the reaction temperature on the conversion, the grafting efficiency, the water absorption and the contact angles of the grafted copolymers films, and the colloidal stability of the latexes at low pH, were investigated. Infrared spectroscopic analysis confirmed that DMAEA and DMAEMA were grafted onto the natural rubber particles. The hairy layer structure of NR‐\u003Cjats:italic>g\u003C\u002Fjats:italic>‐poly(DMAEMA) latex particles was investigated by transmission electron microscopy using positive and negative stainings with OsO\u003Cjats:sub>4\u003C\u002Fjats:sub> and phosphotungstic acid, respectively.\u003C\u002Fjats:p>\u003Cjats:p>\u003Cjats:boxed-text content-type=\"graphic\" position=\"anchor\">\u003Cjats:caption>\u003Cjats:p>TEM micrograph of NR‐\u003Cjats:italic>g\u003C\u002Fjats:italic>‐poly(DMAEMA) latex particles stained with 2% OsO\u003Cjats:sub>4\u003C\u002Fjats:sub>.\u003C\u002Fjats:p>\u003C\u002Fjats:caption>\u003Cjats:graphic xmlns:xlink=\"http:\u002F\u002Fwww.w3.org\u002F1999\u002Fxlink\" mimetype=\"image\u002Fjpeg\" position=\"anchor\" specific-use=\"enlarged-web-image\" xlink:href=\"graphic\u002Fmgra001.jpg\">\u003Cjats:alt-text>magnified image\u003C\u002Fjats:alt-text>\u003Cjats:caption>\u003Cjats:p>TEM micrograph of NR‐\u003Cjats:italic>g\u003C\u002Fjats:italic>‐poly(DMAEMA) latex particles stained with 2% OsO\u003Cjats:sub>4\u003C\u002Fjats:sub>.\u003C\u002Fjats:p>\u003C\u002Fjats:caption>\u003C\u002Fjats:graphic>\u003C\u002Fjats:boxed-text>\n\u003C\u002Fjats:p>",{"EN":2240},"Modification of Natural Rubber by Grafting with Hydrophilic Vinyl Monomers",{"VOID":2242},"10.1002\u002Fmacp.200500255",[158],"https:\u002F\u002Fonlinelibrary.wiley.com\u002Fdoi\u002F10.1002\u002Fmacp.200500255",[2246,2267,2289],{"id":2247,"sortIndex":178,"researcher":24,"roles":2248,"affiliations":2249,"properties":2260},"098870d5-c10b-437e-874c-4c12ee5f870e",[],[2250],{"id":2251,"sortIndex":25,"affiliation":2252,"properties":24},"46953b3e-f800-474d-a7f7-b965f4944899",{"id":2253,"createTime":2254,"updateTime":2254,"relativeEntities":2255,"slug":2256,"properties":2257,"entityType":77,"verifyStatus":23,"verifyTime":24,"verifyNote":24,"syncStatus":23,"languages":24,"translateLanguages":24,"viewCount":25},"c3e8c1d3-6271-4a53-90aa-cf1daa69ef64","2024-10-12T21:02:59.494+00:00",[],"Program-of-Petrochemistry-and-Polymer-Science-Faculty-of-Science-Chulalongkorn-University-Phyathai-Road-Bangkok-10330-Thailand",{"title":2258},{"EN":2259},"Program of Petrochemistry and Polymer Science, Faculty of Science, Chulalongkorn University, Phyathai Road, Bangkok 10330, Thailand",{"openalex":2261,"orcid":2263,"title":2265},{"VOID":2262},"A5077448592",{"VOID":2264},"https:\u002F\u002Forcid.org\u002F0000-0002-4471-1037",{"EN":2266},"Suda Kiatkamjornwong",{"id":2268,"sortIndex":189,"researcher":24,"roles":2269,"affiliations":2270,"properties":2282},"b886f35f-b3ac-4267-a654-529816c90983",[],[2271],{"id":2272,"sortIndex":25,"affiliation":2273,"properties":24},"b7f4a22f-56b4-4f2b-a805-af031c14701f",{"id":2274,"createTime":2275,"updateTime":2276,"relativeEntities":2277,"slug":2278,"properties":2279,"entityType":77,"verifyStatus":23,"verifyTime":24,"verifyNote":24,"syncStatus":23,"languages":24,"translateLanguages":24,"viewCount":25},"07220e33-1b38-4546-bee4-c183ef2b71b2","2024-10-12T21:02:59.485+00:00","2025-06-11T20:10:57.519+00:00",[],"Key-Centre-for-Polymer-Colloids-University-of-Sydney-NSW-2006-Australia",{"title":2280},{"EN":2281},"Key Centre for Polymer Colloids, University of Sydney, NSW 2006, Australia",{"openalex":2283,"orcid":2285,"title":2287},{"VOID":2284},"A5008373079",{"VOID":2286},"https:\u002F\u002Forcid.org\u002F0000-0001-6988-114X",{"EN":2288},"Robert G. 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The development of AMFCs and other electrochemical energy systems is currently severely limited by the lack of AEMs with sufficient alkaline stability. Still, significant advances have been made in recent years and one of the most promising approaches to emerge is the design and synthesis of cationic polymers with various side chain arrangements. Especially, synthetic strategies where the cationic ion‐exchange groups are placed on pendant alkyl spacer chains along the backbone seem to significantly improve microphase separation, hydroxide ion conductivity, and alkaline stability in relation to standard AEMs with cations placed in benzylic positions directly on the backbone. 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