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Hot‐pressing and pressureless sintering techniques were employed and the effects of heating rate, firing atmosphere, and composition were used to characterize the sintering behavior. Pressureless sintering at temperatures up to 2300°C produces only limited densification. Microstructural coarsening is responsible for this since it leads to conditions where densification is slow. Hot‐pressing and carbon additions suppressed coarsening and permitted densification to >95% of theoretical density.\u003C\u002Fjats:p>",{"EN":1475},"Microstructural Coarsening During Sintering of Boron Carbide",{"VOID":1441},"2024-09-17T23:51:04.626+00:00",[131],"https:\u002F\u002Fceramics.onlinelibrary.wiley.com\u002Fdoi\u002F10.1111\u002Fj.1151-2916.1989.tb06252.x",[1481,1501,1516],{"id":1482,"sortIndex":221,"researcher":24,"roles":1483,"affiliations":1484,"properties":1496},"eb8a9848-dfd9-4e2b-8c4f-2b8cf2a650f5",[],[1485],{"id":1486,"sortIndex":25,"affiliation":1487,"properties":24},"db7f7d50-f341-422e-a3d7-a72d23b0c9b1",{"id":1488,"createTime":1489,"updateTime":1490,"relativeEntities":1491,"slug":1492,"properties":1493,"entityType":52,"verifyStatus":23,"verifyTime":24,"verifyNote":24,"syncStatus":23,"languages":24,"translateLanguages":24,"viewCount":25},"030ce3e7-7818-43bc-8183-e25e8070e76d","2024-09-17T23:51:04.655+00:00","2025-06-11T16:25:03.888+00:00",[],"Research-and-Development-Center-General-Electric-Company-Schenectady-New-York-12301",{"title":1494},{"EN":1495},"Research and Development Center, General Electric Company Schenectady, New York 12301",{"openalex":1497,"title":1499},{"VOID":1498},"A5083440455",{"EN":1500},"Robert H. 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M., 1975, Sintering Behavior of Boron, Am. Ceram. Soc. Bull., 54, 178",{},{"id":24,"text":1592,"url":24,"identifiers":1593},"10.1007\u002F978-1-4613-2761-5_9",{"doi":1592},{"id":24,"text":1595,"url":24,"identifiers":1596},"10.1111\u002Fj.1151-2916.1986.tb04797.x",{"doi":1595},{"id":24,"text":1598,"url":24,"identifiers":1599},"10.1007\u002F978-1-4684-7706-1_17",{"doi":1598},{"id":24,"text":1601,"url":24,"identifiers":1602},"10.1179\u002Fpom.1972.15.30.006",{"doi":1601},{"id":24,"text":1604,"url":24,"identifiers":1605},"Prochazka S., 1987, Ceramic Powder Science, 311",{},{"id":24,"text":1607,"url":24,"identifiers":1608},"S. L.Dole “Sintering of Boron Carbide;”Ph.D. Thesis.Rensselaer Polytechnic Institute Troy NY 1985.",{},{"id":24,"text":1610,"url":24,"identifiers":1611},"Hillebrand W. F., 1953, Applied Inorganic Analysis",{},{"id":24,"text":1613,"url":24,"identifiers":1614},"Rhines F. N., 1984, Sintering and Heterogeneous Catalysis, 49",{},{"id":24,"text":1616,"url":24,"identifiers":1617},"10.1007\u002F978-1-4615-8999-0_9",{"doi":1616},{"id":24,"text":1619,"url":24,"identifiers":1620},"10.1063\u002F1.1695991",{"doi":1619},{"id":24,"text":1622,"url":24,"identifiers":1623},"Cahn J. W., 1966, A Model for Connectivity in Multiphase Structures, Acta Metall., 14, 447",{},{"id":24,"text":1625,"url":24,"identifiers":1626},"Underwood E. E., 1972, The mathematical Foundations of Quantitative Stereology, ASTM Spec. Tech. Publ., 504, 3",{},{"id":24,"text":1628,"url":24,"identifiers":1629},"1970, JANAF Thermochemical Tables",{},{"id":24,"text":1631,"url":24,"identifiers":1632},"Harmer M., 1979, Rapid Sintering of Pure and Doped α‐Al2O3, Trans. J. Br. Ceram. Soc., 78, 22",{},{"id":24,"text":1634,"url":24,"identifiers":1635},"Kingery W. D., 1967, Sintering and Related Phenomena, 471",{},{"id":24,"text":1637,"url":24,"identifiers":1638},"10.1111\u002Fj.1151-2916.1984.tb09620.x",{"doi":1637},{"id":1640,"createTime":1641,"updateTime":1641,"relativeEntities":1642,"slug":1643,"properties":1644,"entityType":127,"verifyStatus":128,"verifyTime":1641,"verifyNote":129,"syncStatus":23,"languages":1656,"translateLanguages":24,"viewCount":25,"primaryUrl":1657,"fullTextUrl":24,"authors":1658,"publicationType":302,"publisherRelationship":1703,"citationCount":1736,"citationInfo":1737,"publishDate":1739,"publishYear":1740,"citationAnalyzeStatus":23,"lastCitationAnalyze":24,"indexDatabases":24,"openAccess":24,"references":1741,"isForceReanalyzing":485},"77203142-e223-4598-a771-0a987e1b5e86","2025-01-31T23:48:21.697+00:00",[],"Equilibrium-Cation-Distribution-in-NiAl-sub-2-sub-O-sub-4-sub-CuAl-sub-2-sub-O-sub-4-sub-and-ZnAl-sub-2-sub-O-sub-4-sub-Spinels",{"mag":1645,"keywords":1647,"openalex":1648,"abstract":1650,"title":1652,"doi":1654},{"VOID":1646},"2116362045",{},{"VOID":1649},"W2116362045",{"EN":1651},"\u003Cjats:p>Stoichiometric NiAl\u003Cjats:sub>2\u003C\u002Fjats:sub>O\u003Cjats:sub>4\u003C\u002Fjats:sub>, CuAl\u003Cjats:sub>2\u003C\u002Fjats:sub>O\u003Cjats:sub>4\u003C\u002Fjats:sub>, and ZnAl\u003Cjats:sub>2\u003C\u002Fjats:sub>O\u003Cjats:sub>4\u003C\u002Fjats:sub> spinels were prepared and equilibrated at temperatures from 600° to 1400°C. The parameters \u003Cjats:italic>u\u003C\u002Fjats:italic> and \u003Cjats:italic>x\u003C\u002Fjats:italic>, denoting the oxygen position and fraction of divalent cations on tetrahedral sites, respectively, were determined from a detailed X‐ray diffraction analysis. In NiAl\u003Cjats:sub>2\u003C\u002Fjats:sub>O\u003Cjats:sub>4\u003C\u002Fjats:sub>, \u003Cjats:italic>x\u003C\u002Fjats:italic> increased from 0.07 at 595° to 0.26 at 1391°C; in CuAl\u003Cjats:sub>2\u003C\u002Fjats:sub>O\u003Cjats:sub>4\u003C\u002Fjats:sub>, \u003Cjats:italic>x\u003C\u002Fjats:italic> decreased from 0.68 at 613° to 0.64 at 1195°C; and in ZnAl\u003Cjats:sub>2\u003C\u002Fjats:sub>O\u003Cjats:sub>4\u003C\u002Fjats:sub>, \u003Cjats:italic>x\u003C\u002Fjats:italic> decreased from 0.96 at 905° to 0.94 at 1197°C. The form of the temperature dependence of \u003Cjats:italic>x\u003C\u002Fjats:italic> could not be described using theoretically based equations advanced in the literature. A more general equation which allows for a non‐distributional contribution to the configurational entropy was derived and observed to properly describe the temperature dependence; the results indicate that short‐range order is of definite significance in these intermediate aluminate spinels.\u003C\u002Fjats:p>",{"EN":1653},"Equilibrium Cation Distribution in NiAl\u003Csub>2\u003C\u002Fsub>O\u003Csub>4\u003C\u002Fsub>, CuAl\u003Csub>2\u003C\u002Fsub>O\u003Csub>4\u003C\u002Fsub>, and ZnAl\u003Csub>2\u003C\u002Fsub>O\u003Csub>4\u003C\u002Fsub> Spinels",{"VOID":1655},"10.1111\u002Fj.1151-2916.1972.tb11320.x",[131],"https:\u002F\u002Fceramics.onlinelibrary.wiley.com\u002Fdoi\u002F10.1111\u002Fj.1151-2916.1972.tb11320.x",[1659,1688],{"id":1660,"sortIndex":25,"researcher":24,"roles":1661,"affiliations":1662,"properties":1683},"e5acaee2-3cfc-4ba2-b1be-46a48b75f2a1",[],[1663,1673],{"id":1664,"sortIndex":136,"affiliation":1665,"properties":24},"218421ec-31d1-48b0-9b74-5e0658fd5b08",{"id":1666,"createTime":1667,"updateTime":1667,"relativeEntities":1668,"slug":1669,"properties":1670,"entityType":52,"verifyStatus":23,"verifyTime":24,"verifyNote":24,"syncStatus":23,"languages":24,"translateLanguages":24,"viewCount":25},"b2096b9a-81f3-45bb-b225-4cfffabecc39","2025-01-31T23:48:21.738+00:00",[],"State-University-of-New-York-College-of-Ceramics-at-Alfred-University-Alfred-New-York-14802",{"title":1671},{"EN":1672},"State University of New York College of Ceramics at Alfred University, Alfred, New York 14802",{"id":1674,"sortIndex":25,"affiliation":1675,"properties":24},"26dab3e2-c7b1-4c49-b404-864d20e9327f",{"id":1676,"createTime":1677,"updateTime":1677,"relativeEntities":1678,"slug":1679,"properties":1680,"entityType":52,"verifyStatus":23,"verifyTime":24,"verifyNote":24,"syncStatus":23,"languages":24,"translateLanguages":24,"viewCount":25},"95d71000-26ad-4308-8e56-c28b8729793e","2025-01-31T23:48:21.733+00:00",[],"Now-with-Materials-Studies-Section-Owens-Illinois-Technical-Center-Owens-Illinois-Inc-Toledo-Ohio-43604-",{"title":1681},{"EN":1682},"Now with Materials Studies Section, Owens-Illinois Technical Center, Owens-Illinois, Inc., Toledo, Ohio 43604.",{"openalex":1684,"title":1686},{"VOID":1685},"A5051196750",{"EN":1687},"RICHARD F. 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H.vanSanten andE. J. W.Verwey “Electrostatic Contribution to the Lattice Energy of Some Ordered Spinels ”ibid. 18[8]1032–34(1950).",{},{"id":24,"text":1755,"url":24,"identifiers":1756},"10.1051\u002Fjphysrad:01951001203024900",{"doi":1755},{"id":24,"text":1758,"url":24,"identifiers":1759},"10.1103\u002FPhysRev.94.847",{"doi":1758},{"id":24,"text":1761,"url":24,"identifiers":1762},"10.1063\u002F1.1740465",{"doi":1761},{"id":24,"text":1764,"url":24,"identifiers":1765},"10.1103\u002FPhysRev.103.857",{"doi":1764},{"id":24,"text":1767,"url":24,"identifiers":1768},"10.1063\u002F1.1723141",{"doi":1767},{"id":24,"text":1770,"url":24,"identifiers":1771},"10.1524\u002Fzpch.1961.28.3_4.203",{"doi":1770},{"id":24,"text":1773,"url":24,"identifiers":1774},"10.1051\u002Fjphys:01964002505044700",{"doi":1773},{"id":24,"text":1776,"url":24,"identifiers":1777},"Chapple F. H., 1964, Optical Properties of Cupric Ion in Oxide Crystal Fields of Differing Symmetries, Proc. Brit. Ceram. Soc., 1, 45",{},{"id":24,"text":1779,"url":24,"identifiers":1780},"Stone F. S., 1959, Fifth International Symposium on the Reactivity of Solids, 583",{},{"id":24,"text":1782,"url":24,"identifiers":1783},"10.1111\u002Fj.1151-2916.1967.tb15002.x",{"doi":1782},{"id":24,"text":1785,"url":24,"identifiers":1786},"Azaroff L. V., 1968, Elements of X‐Ray Crystallography",{},{"id":24,"text":1788,"url":24,"identifiers":1789},"Klug H. P., 1954, Alexander, X‐Ray Diffraction Procedures",{},{"id":24,"text":1791,"url":24,"identifiers":1792},"10.1111\u002Fj.1151-2916.1971.tb12265.x",{"doi":1791},{"id":24,"text":1794,"url":24,"identifiers":1795},"Colin Francois, 1966, Chemical Properties of Mixed Oxides Based on Alumina: Reduction of the Spinels MgAl2O4 and ZnAl2O4, Rev. Chim. Miner., 3, 121",{},{"id":24,"text":1797,"url":24,"identifiers":1798},"Romeijn F. C., 1953, Physical and Crystallographical Properties of Some Spinels: I and II, Philips Res. 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Physical properties of the prepared films such as film strength, thermal conductivity, and dielectrics were determined. The BN films vacuum‐pyrolyzed at 900°C showed residual N–H bonds with a 0.75 N\u002FB ratio, interdiffusion phenomena, and preferred orientation at the interfacial zone. Hardness and the elastic modulus of the film increased to 1.6 GPa and 50 GPa by nanoindentation loading. It had a thermal conductivity of 134 W\u002F(m·K) at 296.5 K, and a dielectric constant in the range of 5–7, with tan ∂ between 0.01 and 0.47, depending on the film thickness.\u003C\u002Fjats:p>",{"EN":1841},"Properties of Boron Nitride (B\u003Csub>\u003Ci>x\u003C\u002Fi>\u003C\u002Fsub>N\u003Csub>\u003Ci>y\u003C\u002Fi>\u003C\u002Fsub>) Films Produced by the Spin‐Coating Process of 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The influence of the preparation conditions on the PTCR properties is experimentally tested. The PTCR effect in metallic‐conducting BaPb\u003Cjats:sub>1+y\u003C\u002Fjats:sub>O\u003Cjats:sub>3\u003C\u002Fjats:sub> is confirmed around 700°C. The temperature where the PTCR effect starts can be shifted to a higher temperature range by substituting strontium for the A‐site barium. By the enhancement of the sintering, the magnitude of the PTCR effect was increased and the resisitivity was reduced. 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This approach may replace the more costly and dangerous operation of supercritical drying. The tetraethoxysilane (TEOS)‐derived wet gel was made hydrophobic with multiple treatments of trimethylchlorosilane and dried under ambient pressure. The multiple treatments were found to be necessary to achieve sufficient modification of the wet gel for reduction in drying‐induced surface tension force to maintain product integrity and high porosity. Comparisons in nuclear magnetic resonance spectroscopy and Fourier transform infrared spectroscopy for surface bonding and contact angle measurement for hydrophobicity between the no, single, and multiple surface modification (MSM) samples were conducted to reveal the difference in the extent of the resulting surface modification. 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