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Nhiều nghiên cứu trên người, động vật và \u003Cjats:italic>in vitro\u003C\u002Fjats:italic> đã liên kết catechin trong trà với việc ngăn ngừa một số loại ung thư, giảm nguy cơ béo phì, tiểu đường và bệnh tim mạch, cũng như cải thiện hệ thống miễn dịch. Các catechin trong trà được sử dụng rộng rãi trong nhiều sản phẩm dược phẩm, thực phẩm chức năng và mỹ phẩm để nâng cao tuổi thọ sản phẩm hoặc cải thiện sức khỏe con người. Do đó, nhu cầu về catechin đã tăng lên đáng kể. Catechin đã được chiết xuất và tách riêng từ lá trà bằng nhiều phương pháp qua một số bước khác nhau bao gồm: xử lý lá trà, chiết xuất catechin từ trà vào dung môi, tách isolat catechin khỏi các thành phần khác đã được chiết xuất, và sấy khô các chế phẩm để thu được chiết xuất catechin dưới dạng bột. Bài báo này tóm tắt các đặc điểm vật lý và hóa học của catechin trà và xem xét các bước chiết xuất trong các phương pháp chiết xuất khác nhau, như một cơ sở để cải thiện và phát triển thêm quy trình chiết xuất và tách isolat catechin trà.\u003C\u002Fjats:p>","\u003Cjats:title>Abstract\u003C\u002Fjats:title>\u003Cjats:p>Tea is a major source of catechins, which have become well known for their antioxidant potential. Numerous human, animal, and \u003Cjats:italic>in vitro\u003C\u002Fjats:italic> studies have linked tea catechins with prevention of certain types of cancers, reduction of the risks for obesity, diabetes, and cardiovascular disease, and improvement of the immune system. Tea catechins are widely used in various neutraceuticals, pharmaceuticals, and cosmetics for either enhancing product shelf‐life or for enhancing human health. Thus, the demand for catechins has increased considerably. Catechins have been extracted and isolated from tea leaves by numerous methods through several steps including: treatment of the tea leaves, extraction of catechins from teas into solvents, isolation of catechins from other extracted components, and drying the preparations to obtain catechin extracts in a powder form. 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S., 2008, Food Drying Science and Technology, 1",{},false,{"id":586,"createTime":587,"updateTime":588,"relativeEntities":589,"slug":590,"properties":591,"entityType":120,"verifyStatus":121,"verifyTime":587,"verifyNote":123,"languages":610,"translateLanguages":611,"viewCount":25,"primaryUrl":612,"fullTextUrl":24,"authors":613,"publicationType":215,"publisherRelationship":706,"citationCount":25,"citationInfo":756,"publishDate":759,"publishYear":757,"citationAnalyzeStatus":23,"lastCitationAnalyze":760,"indexDatabases":761,"openAccess":24,"references":762,"isForceReanalyzing":584},"36bf3537-11dd-48e2-adb1-e3fcb671b7f9","2025-01-25T16:23:59.486+00:00","2026-05-14T13:56:59.049+00:00",[],"Optimum-conditions-for-the-water-extraction-of-scp-L-scp-theanine-from-green-tea",{"mag":592,"gsPaper":594,"keywords":596,"openalex":598,"abstract":600,"title":603,"pm":606,"doi":608},{"VOID":593},"2003991782",{"VOID":595},"[\"14523194830547948444\"]",{"VI":597},"",{"VOID":599},"W2003991782",{"EN":601,"VI":602},"\u003Cjats:title>Abstract\u003C\u002Fjats:title>\u003Cjats:p>Theanine is a unique non‐protein amino acid found in tea (\u003Cjats:italic>Camellia sinensis\u003C\u002Fjats:italic>). It contributes to the favourable umami taste of tea and is linked to various beneficial effects in humans. There is an increasing interest in theanine as an important component of tea, as an ingredient for novel functional foods and as a dietary supplement. Therefore, optimal conditions for extracting theanine from tea are required for the accurate quantification of theanine in tea and as an efficient first step for its purification. This study examined the effects of four different extraction conditions on the yield of theanine from green tea using water and applied response surface methodology to further optimise the extraction conditions. The results showed that temperature, extraction time, ratio of water‐to‐tea and tea particle sizes had significant impacts on the extraction yield of theanine. The optimal conditions for extracting theanine from green tea using water were found to be extraction at 80°C for 30 min with a water‐to‐tea ratio of 20:1 mL\u002Fg and a tea particle size of 0.5–1 mm.\u003C\u002Fjats:p>","\u003Cjats:title>Tóm tắt\u003C\u002Fjats:title>\u003Cjats:p>Theanine là một loại axit amin không chứa protein đặc biệt được tìm thấy trong trà (\u003Cjats:italic>Camellia sinensis\u003C\u002Fjats:italic>). Nó góp phần tạo nên vị umami dễ chịu của trà và có liên quan đến nhiều tác dụng có lợi cho con người. Sự quan tâm ngày càng tăng đối với theanine như một thành phần quan trọng của trà, như một nguyên liệu cho thực phẩm chức năng mới và như một chất bổ sung dinh dưỡng. Do đó, cần thiết phải xác định các điều kiện tối ưu cho việc chiết xuất theanine từ trà để có thể định lượng chính xác theanine trong trà và như một bước đầu tiên hiệu quả cho việc tinh chế nó. Nghiên cứu này đã xem xét ảnh hưởng của bốn điều kiện chiết xuất khác nhau lên năng suất của theanine từ trà xanh bằng nước và ứng dụng phương pháp bề mặt phản ứng để tối ưu hóa thêm các điều kiện chiết xuất. Kết quả cho thấy nhiệt độ, thời gian chiết xuất, tỷ lệ nước và trà cũng như kích thước hạt trà có ảnh hưởng đáng kể đến năng suất chiết xuất theanine. Các điều kiện tối ưu cho việc chiết xuất theanine từ trà xanh bằng nước được xác định là chiết xuất ở 80°C trong 30 phút với tỷ lệ nước và trà là 20:1 mL\u002Fg và kích thước hạt trà là 0.5–1 mm.\u003C\u002Fjats:p>",{"EN":604,"VI":605},"Optimum conditions for the water extraction of \u003Cscp>L\u003C\u002Fscp>‐theanine from green tea","Điều kiện tối ưu cho việc chiết xuất \u003Cscp>L\u003C\u002Fscp>‐theanine từ trà xanh bằng nước",{"VOID":607},"21735551",{"VOID":609},"10.1002\u002Fjssc.201100401",[125],[127],"https:\u002F\u002Fanalyticalsciencejournals.onlinelibrary.wiley.com\u002Fdoi\u002F10.1002\u002Fjssc.201100401",[614,629,648,669,691],{"id":615,"sortIndex":25,"researcher":24,"roles":616,"affiliations":617,"properties":624,"displayName":146,"givenName":24,"familyName":24},"f9277d2f-acde-41c9-88c0-d451ce13719c",[],[618],{"id":135,"sortIndex":25,"affiliation":619,"properties":24},{"id":135,"createTime":24,"updateTime":24,"relativeEntities":620,"slug":24,"properties":621,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":623,"statistic":24},[],{"title":622},{"VI":140},[],{"orcid":625,"title":626,"gsAuthor":627,"openalex":628},{"VOID":144},{"EN":146},{"VOID":148},{"VOID":150},{"id":630,"sortIndex":153,"researcher":24,"roles":631,"affiliations":632,"properties":639,"displayName":643,"givenName":24,"familyName":24},"2a22b3a4-21bd-4533-bdee-7a13a9c5964e",[],[633],{"id":135,"sortIndex":25,"affiliation":634,"properties":24},{"id":135,"createTime":24,"updateTime":24,"relativeEntities":635,"slug":24,"properties":636,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":638,"statistic":24},[],{"title":637},{"VI":140},[],{"orcid":640,"title":642,"gsAuthor":644,"openalex":646},{"VOID":641},"https:\u002F\u002Forcid.org\u002F0000-0001-9241-7580",{"EN":643},"Costas E. 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V., 2011, Int. Food Res. J., 18, 329",{},{"id":24,"text":815,"url":24,"identifiers":816},"10.1016\u002Fj.seppur.2007.01.008",{"doi":815},{"id":24,"text":818,"url":24,"identifiers":819},"10.1002\u002Fjssc.200800744",{"doi":818},{"id":24,"text":821,"url":24,"identifiers":822},"Escribano‐Balón M. T., 2003, Methods in Polyphenol Analysis, 1",{},{"id":24,"text":403,"url":24,"identifiers":824},{"doi":403},{"id":24,"text":826,"url":24,"identifiers":827},"10.1016\u002Fj.foodchem.2010.08.071",{"doi":826},{"id":24,"text":457,"url":24,"identifiers":829},{"doi":457},{"id":24,"text":831,"url":24,"identifiers":832},"10.1002\u002Fjsfa.2740370604",{"doi":831},{"id":834,"createTime":835,"updateTime":836,"relativeEntities":837,"slug":838,"properties":839,"entityType":120,"verifyStatus":121,"verifyTime":835,"verifyNote":123,"languages":857,"translateLanguages":858,"viewCount":25,"primaryUrl":859,"fullTextUrl":24,"authors":860,"publicationType":215,"publisherRelationship":948,"citationCount":25,"citationInfo":996,"publishDate":998,"publishYear":757,"citationAnalyzeStatus":23,"lastCitationAnalyze":999,"indexDatabases":1000,"openAccess":24,"references":1001,"isForceReanalyzing":584},"398808eb-3b93-4239-821d-e91eacd63e57","2024-12-25T18:36:14.817+00:00","2026-04-24T07:12:53.962+00:00",[],"Optimizing-conditions-for-the-extraction-of-catechins-from-green-tea-using-hot-water",{"mag":840,"gsPaper":842,"keywords":844,"openalex":845,"abstract":847,"title":850,"pm":853,"doi":855},{"VOID":841},"2072862601",{"VOID":843},"[\"9439170254951307948\"]",{"VI":597},{"VOID":846},"W2072862601",{"VI":848,"EN":849},"\u003Cjats:title>Tóm tắt\u003C\u002Fjats:title>\u003Cjats:p>Sáu yếu tố khác nhau liên quan đến quá trình chiết xuất catechin từ trà xanh bằng nước đã được xem xét để đánh giá tác động của chúng đến sản lượng catechin và hiệu quả sử dụng nước. Tổ hợp nhiệt độ và thời gian tốt nhất cho việc chiết xuất catechin là ở 80°C trong 30 phút. Sản lượng catechin cũng tối ưu với kích thước hạt trà là 1 mm, độ pH của dung dịch pha chế \u003C6 và tỷ lệ trà-so nước là 50:1 (mL\u002Fg). Về hiệu quả sử dụng nước trong một lần chiết xuất, tỷ lệ nước-so trà là 20:1 (mL\u002Fg) cho kết quả tốt nhất; lượng nước sử dụng giảm đi 2,5 lần cho mỗi gram trà xanh. Tại tỷ lệ nước-so trà 20:1 mL\u002Fg, sản lượng catechin cao nhất trên mỗi gram trà xanh đạt được bằng cách chiết xuất cùng một mẫu trà xanh hai lần. Tuy nhiên, để sử dụng nước hiệu quả nhất, phương pháp chiết xuất tốt nhất được tìm thấy là một lần ở tỷ lệ nước-so trà 12:1 (mL\u002Fg) và một lần ở tỷ lệ nước-so trà 8:1 (mL\u002Fg). Do đó, tất cả sáu yếu tố được nghiên cứu đều có tác động đến sản lượng catechin được chiết xuất từ trà xanh bằng nước và hai trong số đó có tác động đến hiệu quả sử dụng nước.\u003C\u002Fjats:p>","\u003Cjats:title>Abstract\u003C\u002Fjats:title>\u003Cjats:p>Six different factors involved in the extraction of catechins from green tea using water were examined for their impact on the yield of catechins and on the efficiency of water use. The best temperature and time combination for catechin extraction was at 80°C for 30 min. The yield of catechins was also optimal with a tea particle size of 1 mm, a brewing solution pH <6 and a tea‐to‐water ratio at 50:1 (mL\u002Fg). In terms of efficient use of water in a single extraction, a water‐to‐tea ratio of 20:1 (mL\u002Fg) gave the best results; 2.5 times less water was used per gram of green tea. At the water‐to‐tea ratio of 20:1 mL\u002Fg, the highest yield of catechins per gram of green tea was achieved by extracting the same sample of green tea twice. However, for the most efficient use of water, the best extraction was found to be once at a water‐to‐tea ratio of 12:1 (mL\u002Fg) and once at a water‐to‐tea ratio of 8:1 (mL\u002Fg). Therefore, all six of the factors investigated had an impact on the yield of catechins extracted from green tea using water and two had an impact on the efficiency of water use.\u003C\u002Fjats:p>",{"EN":851,"VI":852},"Optimizing conditions for the extraction of catechins from green tea using hot water","Tối ưu hóa điều kiện chiết xuất catechin từ trà xanh bằng nước nóng",{"VOID":854},"21905216",{"VOID":856},"10.1002\u002Fjssc.201000863",[125],[127],"https:\u002F\u002Fanalyticalsciencejournals.onlinelibrary.wiley.com\u002Fdoi\u002F10.1002\u002Fjssc.201000863",[861,876,899,914,934],{"id":862,"sortIndex":25,"researcher":24,"roles":863,"affiliations":864,"properties":871,"displayName":146,"givenName":24,"familyName":24},"f64262bc-07d3-4797-b601-d4d3de470969",[],[865],{"id":135,"sortIndex":25,"affiliation":866,"properties":24},{"id":135,"createTime":24,"updateTime":24,"relativeEntities":867,"slug":24,"properties":868,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":870,"statistic":24},[],{"title":869},{"VI":140},[],{"orcid":872,"title":873,"gsAuthor":874,"openalex":875},{"VOID":144},{"EN":146},{"VOID":148},{"VOID":150},{"id":877,"sortIndex":153,"researcher":24,"roles":878,"affiliations":879,"properties":894,"displayName":174,"givenName":24,"familyName":24},"02c878a4-e47e-4978-b603-ac466c7dbb91",[],[880,888],{"id":881,"sortIndex":25,"affiliation":882,"properties":24},"7f5051e6-f46c-4652-bcc0-9453dc21dc0c",{"id":881,"createTime":24,"updateTime":24,"relativeEntities":883,"slug":24,"properties":884,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":887,"statistic":24},[],{"title":885},{"EN":886},"Gosford Primary Industries Institute, NSW Department of Primary Industries, Ourimbah, NSW, Australia",[],{"id":135,"sortIndex":153,"affiliation":889,"properties":24},{"id":135,"createTime":24,"updateTime":24,"relativeEntities":890,"slug":24,"properties":891,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":893,"statistic":24},[],{"title":892},{"VI":140},[],{"orcid":895,"title":896,"gsAuthor":897,"openalex":898},{"VOID":172},{"EN":174},{"VOID":176},{"VOID":178},{"id":900,"sortIndex":181,"researcher":24,"roles":901,"affiliations":902,"properties":909,"displayName":643,"givenName":24,"familyName":24},"41685157-bc6f-493a-935e-6cf308a8c1da",[],[903],{"id":135,"sortIndex":25,"affiliation":904,"properties":24},{"id":135,"createTime":24,"updateTime":24,"relativeEntities":905,"slug":24,"properties":906,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":908,"statistic":24},[],{"title":907},{"VI":140},[],{"orcid":910,"title":911,"gsAuthor":912,"openalex":913},{"VOID":641},{"EN":643},{"VOID":645},{"VOID":647},{"id":915,"sortIndex":199,"researcher":24,"roles":916,"affiliations":917,"properties":930,"displayName":194,"givenName":24,"familyName":24},"e0243993-1679-4eae-a65a-71fb0aa0d35c",[],[918,924],{"id":135,"sortIndex":25,"affiliation":919,"properties":24},{"id":135,"createTime":24,"updateTime":24,"relativeEntities":920,"slug":24,"properties":921,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":923,"statistic":24},[],{"title":922},{"VI":140},[],{"id":680,"sortIndex":153,"affiliation":925,"properties":24},{"id":680,"createTime":24,"updateTime":24,"relativeEntities":926,"slug":24,"properties":927,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":929,"statistic":24},[],{"title":928},{"EN":685},[],{"orcid":931,"title":932,"openalex":933},{"VOID":192},{"EN":194},{"VOID":196},{"id":935,"sortIndex":693,"researcher":24,"roles":936,"affiliations":937,"properties":944,"displayName":212,"givenName":24,"familyName":24},"9fe60200-103a-420e-a0f1-0af48e006eda",[],[938],{"id":135,"sortIndex":25,"affiliation":939,"properties":24},{"id":135,"createTime":24,"updateTime":24,"relativeEntities":940,"slug":24,"properties":941,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":943,"statistic":24},[],{"title":942},{"VI":140},[],{"orcid":945,"title":946,"openalex":947},{"VOID":210},{"EN":212},{"VOID":214},{"url":24,"publisher":949,"properties":991},{"id":6,"createTime":7,"updateTime":8,"relativeEntities":950,"slug":10,"properties":951,"entityType":22,"verifyStatus":23,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":25,"subjectFields":956,"manageAffiliations":965,"indexDatabases":976,"url":90,"thumbnailPath":24,"statistic":24,"gsStatistic":24,"type":24,"analyzePriority":24},[],{"country":952,"eissn":953,"issn":954,"title":955},{"VOID":13},{"VOID":15},{"VOID":17},{"EN":19},[957,961],{"id":28,"createTime":24,"updateTime":24,"relativeEntities":958,"label":959,"description":960,"parentId":24,"standard":24,"scholarHubFieldId":24},[],{"EN":31},{},{"id":34,"createTime":24,"updateTime":24,"relativeEntities":962,"label":963,"description":964,"parentId":24,"standard":24,"scholarHubFieldId":24},[],{"EN":37},{},[966,971],{"id":41,"createTime":24,"updateTime":24,"relativeEntities":967,"slug":24,"properties":968,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":970,"statistic":24},[],{"title":969},{"EN":45},[],{"id":48,"createTime":24,"updateTime":24,"relativeEntities":972,"slug":24,"properties":973,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":975,"statistic":24},[],{"title":974},{"EN":52},[],[977,984],{"id":56,"indexDatabase":978,"url":67,"indexYears":68,"academicFieldIds":983,"indexDatabaseRanking":72},{"id":58,"createTime":24,"updateTime":24,"relativeEntities":979,"label":980,"description":981,"key":64,"publicationTags":982,"standard":24},[],{"EN":61,"VI":61},{"EN":61,"VI":63},[66],[70,71],{"id":74,"indexDatabase":985,"url":87,"indexYears":24,"academicFieldIds":990,"indexDatabaseRanking":24},{"id":76,"createTime":24,"updateTime":24,"relativeEntities":986,"label":987,"description":988,"key":83,"publicationTags":989,"standard":24},[],{"EN":79,"VI":79},{"EN":81,"VI":82},[85,86],[89],{"issue":992,"pages":993,"volume":995},{"VOID":261},{"VOID":994},"3099-3106",{"VOID":755},{"total":25,"publishYear":757,"statisticByYear":997},{},"2011-11-01","2026-04-24T07:12:53.961+00:00",[85,72],[1002,1004,1007,1009,1012,1015,1017,1019,1021,1023,1025,1027,1030,1033,1035,1037,1039,1041,1044,1047,1049,105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S., 1999, Korean J. Food Sci. Technol., 31, 1024",{},{"id":24,"text":421,"url":24,"identifiers":1048},{"doi":421},{"id":24,"text":424,"url":24,"identifiers":1050},{"doi":424},{"id":24,"text":1052,"url":24,"identifiers":1053},"10.1016\u002F0308-8146(87)90083-5",{"doi":1052},{"id":1055,"createTime":1056,"updateTime":1057,"relativeEntities":1058,"slug":1059,"properties":1060,"entityType":120,"verifyStatus":121,"verifyTime":1056,"verifyNote":123,"languages":1076,"translateLanguages":1077,"viewCount":25,"primaryUrl":1078,"fullTextUrl":24,"authors":1079,"publicationType":215,"publisherRelationship":1152,"citationCount":1202,"citationInfo":1203,"publishDate":1211,"publishYear":1204,"citationAnalyzeStatus":23,"lastCitationAnalyze":24,"indexDatabases":1212,"openAccess":24,"references":1213,"isForceReanalyzing":584},"db5540fc-7002-47d1-a324-cfb263646750","2025-01-23T20:34:12.610+00:00","2025-02-17T18:09:18.362+00:00",[],"Simultaneous-determination-of-phenolic-acids-and-flavonoids-in-rice-using-solid-phase-extraction-and-scp-RP-HPLC-scp-with-photodiode-array-detection",{"mag":1061,"keywords":1063,"openalex":1064,"abstract":1066,"title":1069,"pm":1072,"doi":1074},{"VOID":1062},"2121448615",{"VI":597},{"VOID":1065},"W2121448615",{"EN":1067,"VI":1068},"\u003Cjats:p>An analytical method based on an optimized solid‐phase extraction procedure and followed by high‐performance liquid chromatography (\u003Cjats:styled-content style=\"fixed-case\">HPLC\u003C\u002Fjats:styled-content>) separation with diode array detection was developed and validated for the simultaneous determination of phenolic acids (gallic, protocatechuic, 4‐hydroxy‐benzoic, vanillic, caffeic, syringic, \u003Cjats:italic>p\u003C\u002Fjats:italic>‐coumaric, ferulic, sinapic, and cinnamic acids), flavanols (catechin and epicatechin), flavonols (myricetin, quercetin, kaempferol, quercetin‐3‐\u003Cjats:italic>\u003Cjats:styled-content style=\"fixed-case\">O\u003C\u002Fjats:styled-content>\u003C\u002Fjats:italic>‐glucoside, hyperoside, and rutin), flavones (luteolin and apigenin) and flavanones (naringenin and hesperidin) in rice flour (\u003Cjats:italic>\u003Cjats:styled-content style=\"fixed-case\">O\u003C\u002Fjats:styled-content>ryza sativa\u003C\u002Fjats:italic> \u003Cjats:styled-content style=\"fixed-case\">L\u003C\u002Fjats:styled-content>.). Chromatographic separation was carried out on a \u003Cjats:styled-content style=\"fixed-case\">P\u003C\u002Fjats:styled-content>erfect\u003Cjats:styled-content style=\"fixed-case\">S\u003C\u002Fjats:styled-content>il \u003Cjats:styled-content style=\"fixed-case\">T\u003C\u002Fjats:styled-content>arget \u003Cjats:styled-content style=\"fixed-case\">ODS\u003C\u002Fjats:styled-content>‐3 (250 mm × 4.6 mm, 3 μm) column at temperature 25°\u003Cjats:styled-content style=\"fixed-case\">C\u003C\u002Fjats:styled-content> using a mobile phase, consisting of 0.5% (v\u002Fv) acetic acid in water, methanol, and acetonitrile at a flow rate 1 m\u003Cjats:styled-content style=\"fixed-case\">L\u003C\u002Fjats:styled-content> min\u003Cjats:sup>−1\u003C\u002Fjats:sup>, under gradient elution conditions. Application of optimum extraction conditions, elaborated on both \u003Cjats:styled-content style=\"fixed-case\">L\u003C\u002Fjats:styled-content>ichrolut \u003Cjats:styled-content style=\"fixed-case\">C\u003C\u002Fjats:styled-content>\u003Cjats:sub>18\u003C\u002Fjats:sub> and \u003Cjats:styled-content style=\"fixed-case\">O\u003C\u002Fjats:styled-content>asis \u003Cjats:styled-content style=\"fixed-case\">HLB\u003C\u002Fjats:styled-content> cartridges, have led to extraction of phenolic acids and flavonoids from rice flour with mean recoveries 84.3–113.0%. The developed method was validated in terms of linearity, accuracy, precision, stability, and sensitivity. Repeatability (\u003Cjats:italic>n\u003C\u002Fjats:italic> = 5) and inter‐day precision (\u003Cjats:italic>n\u003C\u002Fjats:italic> = 4) revealed relative standard deviation (\u003Cjats:styled-content style=\"fixed-case\">RSD\u003C\u002Fjats:styled-content>) <13%. The optimized method was successfully applied to the analysis of phenolic acids and flavonoids in pigmented (red and black rice) and non‐pigmented rice (brown rice) samples.\u003C\u002Fjats:p>","\u003Cjats:p>Phương pháp phân tích dựa trên quy trình chiết pha rắn tối ưu và tiếp theo là tách bằng sắc ký lỏng hiệu năng cao (\u003Cjats:styled-content style=\"fixed-case\">HPLC\u003C\u002Fjats:styled-content>) với phát hiện bằng dải photodiode đã được phát triển và xác nhận để xác định đồng thời các axit phenolic (acid gallic, acid protocatechuic, acid 4-hydroxy-benzoic, acid vanillic, acid caffeic, acid syringic, acid \u003Cjats:italic>p\u003C\u002Fjats:italic>-coumaric, acid ferulic, acid sinapic, và acid cinnamic), flavanol (catechin và epicatechin), flavonol (myricetin, quercetin, kaempferol, quercetin-3-\u003Cjats:italic>\u003Cjats:styled-content style=\"fixed-case\">O\u003C\u002Fjats:styled-content>\u003C\u002Fjats:italic>-glucoside, hyperoside, và rutin), flavone (luteolin và apigenin) và flavanone (naringenin và hesperidin) trong bột gạo (\u003Cjats:italic>\u003Cjats:styled-content style=\"fixed-case\">O\u003C\u002Fjats:styled-content>ryza sativa\u003C\u002Fjats:italic> \u003Cjats:styled-content style=\"fixed-case\">L\u003C\u002Fjats:styled-content>.). Quá trình tách sắc ký được thực hiện trên cột \u003Cjats:styled-content style=\"fixed-case\">P\u003C\u002Fjats:styled-content>erfect\u003Cjats:styled-content style=\"fixed-case\">S\u003C\u002Fjats:styled-content>il \u003Cjats:styled-content style=\"fixed-case\">T\u003C\u002Fjats:styled-content>arget \u003Cjats:styled-content style=\"fixed-case\">ODS\u003C\u002Fjats:styled-content>‐3 (250 mm × 4.6 mm, 3 μm) ở nhiệt độ 25°\u003Cjats:styled-content style=\"fixed-case\">C\u003C\u002Fjats:styled-content> sử dụng pha động, bao gồm 0.5% (v\u002Fv) acid acetic trong nước, methanol, và acetonitrile với tốc độ dòng chảy 1 m\u003Cjats:styled-content style=\"fixed-case\">L\u003C\u002Fjats:styled-content> min\u003Cjats:sup>−1\u003C\u002Fjats:sup>, dưới điều kiện elution gradient. Việc áp dụng các điều kiện chiết xuất tối ưu, được triển khai trên cả cartridge \u003Cjats:styled-content style=\"fixed-case\">L\u003C\u002Fjats:styled-content>ichrolut \u003Cjats:styled-content style=\"fixed-case\">C\u003C\u002Fjats:styled-content>\u003Cjats:sub>18\u003C\u002Fjats:sub> và \u003Cjats:styled-content style=\"fixed-case\">O\u003C\u002Fjats:styled-content>asis \u003Cjats:styled-content style=\"fixed-case\">HLB\u003C\u002Fjats:styled-content>, đã dẫn đến việc chiết xuất các axit phenolic và flavonoid từ bột gạo với tỷ lệ phục hồi trung bình từ 84.3–113.0%. Phương pháp phát triển đã được xác nhận về mặt tính tuyến tính, độ chính xác, độ chính xác, sự ổn định, và độ nhạy. Độ lặp lại (\u003Cjats:italic>n\u003C\u002Fjats:italic> = 5) và độ chính xác giữa các ngày (\u003Cjats:italic>n\u003C\u002Fjats:italic> = 4) cho thấy độ lệch chuẩn tương đối (\u003Cjats:styled-content style=\"fixed-case\">RSD\u003C\u002Fjats:styled-content>) <13%. Phương pháp tối ưu đã được áp dụng thành công để phân tích các axit phenolic và flavonoid trong mẫu gạo có màu (gạo đỏ và đen) và gạo không có màu (gạo nâu).\u003C\u002Fjats:p>",{"EN":1070,"VI":1071},"Simultaneous determination of phenolic acids and flavonoids in rice using solid‐phase extraction and \u003Cscp>RP‐HPLC\u003C\u002Fscp> with photodiode array detection","Xác định đồng thời các axit phenolic và flavonoid trong gạo bằng cách chiết pha rắn và \u003Cscp>RP‐HPLC\u003C\u002Fscp> với phát hiện bằng dải photodiode",{"VOID":1073},"22761138",{"VOID":1075},"10.1002\u002Fjssc.201200140",[125],[127],"https:\u002F\u002Fanalyticalsciencejournals.onlinelibrary.wiley.com\u002Fdoi\u002F10.1002\u002Fjssc.201200140",[1080,1099,1118,1137],{"id":1081,"sortIndex":25,"researcher":24,"roles":1082,"affiliations":1083,"properties":1092,"displayName":1096,"givenName":24,"familyName":24},"c01f532b-54a2-4e46-9018-6edd93ab588d",[],[1084],{"id":1085,"sortIndex":25,"affiliation":1086,"properties":24},"e9681e6d-9c10-4356-96a5-08a88d03f954",{"id":1085,"createTime":24,"updateTime":24,"relativeEntities":1087,"slug":24,"properties":1088,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":1091,"statistic":24},[],{"title":1089},{"EN":1090},"Cereal Institute, National Agricultural Research Foundation, Thessaloniki, Greece.",[],{"orcid":1093,"title":1095,"openalex":1097},{"VOID":1094},"https:\u002F\u002Forcid.org\u002F0000-0003-2460-9956",{"EN":1096},"Maria Irakli",{"VOID":1098},"A5036954909",{"id":1100,"sortIndex":153,"researcher":24,"roles":1101,"affiliations":1102,"properties":1111,"displayName":1115,"givenName":24,"familyName":24},"93de9421-0800-418d-bc78-da8901846dd2",[],[1103],{"id":1104,"sortIndex":25,"affiliation":1105,"properties":24},"50627f22-afeb-4e45-81bf-6c25700dc985",{"id":1104,"createTime":24,"updateTime":24,"relativeEntities":1106,"slug":24,"properties":1107,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":1110,"statistic":24},[],{"title":1108},{"VI":1109},"Laboratory of Analytical Chemistry, Department of Chemistry, Aristotle University of Thessaloniki, Thessaloniki, Greece",[],{"orcid":1112,"title":1114,"openalex":1116},{"VOID":1113},"https:\u002F\u002Forcid.org\u002F0000-0002-8493-1106",{"EN":1115},"Victoria Samanidou",{"VOID":1117},"A5052164357",{"id":1119,"sortIndex":181,"researcher":24,"roles":1120,"affiliations":1121,"properties":1130,"displayName":1134,"givenName":24,"familyName":24},"5aae754e-a158-4c9a-a714-6b9873715788",[],[1122],{"id":1123,"sortIndex":25,"affiliation":1124,"properties":24},"89e31a44-1e06-42f3-b512-7c31de05bcce",{"id":1123,"createTime":24,"updateTime":24,"relativeEntities":1125,"slug":24,"properties":1126,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":1129,"statistic":24},[],{"title":1127},{"EN":1128},"Laboratory of Food Chemistry and Biochemistry, Department of Food Science and Technology, Aristotle University, School of Agriculture, Thessaloniki, Greece",[],{"orcid":1131,"title":1133,"openalex":1135},{"VOID":1132},"https:\u002F\u002Forcid.org\u002F0000-0001-9641-6278",{"EN":1134},"Costas G. 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Pharmaceutical compounds evaluated were nonsteroidal anti‐inflammatory drugs (acetaminophen, diclofenac, ibuprofen, ketoprofen, naproxen and salicylic acid), antibiotics (sulfamethoxazole and trimethoprim), an anti‐epileptic drug (carbamazepine), a β‐blocker (propranolol), a nervous stimulant (caffeine), estrogens (17α‐ethinylestradiol, 17β‐estradiol, estriol and estrone) and lipid regulators (clofibric acid, metabolite of clofibrate and gemfibrozil). The method is based on the ultrasonic‐assisted extraction, clean‐up by SPE and analytical determination by HPLC with diode array and fluorescence detectors. The best extraction recoveries were achieved in a three‐step extraction procedure with methanol and acetone as extraction solvents. Extraction recoveries of several pharmaceutical compounds as caffeine were highly dependent on the type of sample evaluated. The applicability of the method was tested by analyzing primary, secondary and anaerobically digested dehydrated sludge, compost and sediment samples from Seville (Southern Spain). Ten of the sixteen pharmaceutical compounds were detected in sludge samples and five in compost and sediment samples. The highest concentration levels were recorded for ibuprofen in sewage samples, whereas salicylic acid and 17α‐ethinylestradiol were detected in all of the samples analyzed.\u003C\u002Fjats:p>",{"EN":1325},"Multi‐residue method for the analysis of pharmaceutical compounds in sewage sludge, compost and sediments by sonication‐assisted extraction and LC 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European Union Brussels Belgium.",{},{"id":24,"text":1463,"url":24,"identifiers":1464},"10.1016\u002Fj.wasman.2008.01.009",{"doi":1463},{"id":24,"text":1466,"url":24,"identifiers":1467},"10.1016\u002Fj.chemosphere.2005.03.018",{"doi":1466},{"id":24,"text":1469,"url":24,"identifiers":1470},"10.1007\u002Fs00216-009-2604-4",{"doi":1469},{"id":24,"text":1472,"url":24,"identifiers":1473},"10.1016\u002Fj.chroma.2005.05.051",{"doi":1472},{"id":24,"text":1475,"url":24,"identifiers":1476},"10.1039\u002Fb717453e",{"doi":1475},{"id":24,"text":1478,"url":24,"identifiers":1479},"10.1002\u002Fjssc.200600360",{"doi":1478},{"id":24,"text":1481,"url":24,"identifiers":1482},"10.1016\u002Fj.envint.2009.01.006",{"doi":1481},{"id":24,"text":1484,"url":24,"identifiers":1485},"10.1016\u002Fj.chroma.2004.10.096",{"doi":1484},{"id":24,"text":1487,"url":24,"identifiers":1488},"10.1021\u002Fes048143z",{"doi":1487},{"id":24,"text":1490,"url":24,"identifiers":1491},"10.1016\u002Fj.chroma.2003.08.089",{"doi":1490},{"id":24,"text":1493,"url":24,"identifiers":1494},"10.1007\u002Fs00216-006-0947-7",{"doi":1493},{"id":24,"text":1496,"url":24,"identifiers":1497},"10.1021\u002Fac015717z",{"doi":1496},{"id":24,"text":1499,"url":24,"identifiers":1500},"10.1002\u002Fjssc.200900128",{"doi":1499},{"id":1502,"createTime":1503,"updateTime":1503,"relativeEntities":1504,"slug":1505,"properties":1506,"entityType":120,"verifyStatus":121,"verifyTime":1503,"verifyNote":123,"languages":1519,"translateLanguages":24,"viewCount":25,"primaryUrl":1520,"fullTextUrl":24,"authors":1521,"publicationType":215,"publisherRelationship":1571,"citationCount":1621,"citationInfo":1622,"publishDate":1625,"publishYear":1623,"citationAnalyzeStatus":23,"lastCitationAnalyze":24,"indexDatabases":1626,"openAccess":24,"references":1627,"isForceReanalyzing":584},"117051db-fd36-44be-8b90-c4568cfc55fa","2025-02-07T23:42:44.333+00:00",[],"Synthesis-and-application-of-novel-phenylboronate-affinity-materials-based-on-organic-polymer-particles-for-selective-trapping-of-glycoproteins",{"openalex":1507,"mag":1509,"abstract":1511,"title":1513,"pm":1515,"doi":1517},{"VOID":1508},"W2137450982",{"VOID":1510},"2137450982",{"EN":1512},"\u003Cjats:title>Abstract\u003C\u002Fjats:title>\u003Cjats:p>We report on synthesis concepts for the fabrication of various novel phenylboronate affinity materials based on polymethacrylate epoxy beads (Fractogel® EMD Epoxy (M) 40–90 μm) and the testing of these functionalized polymer particles for selective trapping of a glycoprotein from a standard mixture containing a glycosylated and a nonglycosylated protein. Two inherently different approaches for the functionalization of the bare beads with boronate groups have been elucidated. In the first, the epoxy residues of the polymer particles were converted into reactive thiol groups which were subsequently used as anchor moieties for the immobilization of 4‐vinylphenylboronic acid by radical addition or radical polymerization reaction. Three different ways for the generation of sulfhydryl groups have been examined leading to materials with distinct linker chemistries. In the second and more straightforward approach, the epoxy groups were reacted with 4‐mercaptophenylboronic acid. The novel materials were thoroughly characterized by (i) quantitation of the sulfur content by elemental analysis, (ii) reactive sulfhydryls were determined in a photospectrometric assay, (iii) boron content was measured by inductively coupled plasma‐atomic emission spectrometry, and (iv) the amount of reactive boronate groups was evaluated in a fast binding assay employing adenosine as test compound. A maximum concentration of 1.2 mmol boronate groups \u003Cjats:italic>per \u003C\u002Fjats:italic>gram dry beads could be achieved by the presented synthesis routes. Employing the novel phenylboronate affinity materials in capture and release experiments in the batch mode, a standard glycoprotein,\u003Cjats:italic> viz\u003C\u002Fjats:italic>. transferrin (Tf) from human serum was separated from a nonglycosylated protein, BSA. A commercial boronate affinity material based on 3‐aminophenylboronic acid modified agarose gel was employed as reference material and was found to perform significantly worse compared to the herein presented novel polymethacrylate particles.\u003C\u002Fjats:p>",{"EN":1514},"Synthesis and application of novel phenylboronate affinity materials based on organic polymer particles for selective trapping of glycoproteins",{"VOID":1516},"19472289",{"VOID":1518},"10.1002\u002Fjssc.200800679",[125],"https:\u002F\u002Fanalyticalsciencejournals.onlinelibrary.wiley.com\u002Fdoi\u002F10.1002\u002Fjssc.200800679",[1522,1539,1554],{"id":1523,"sortIndex":25,"researcher":24,"roles":1524,"affiliations":1525,"properties":1534,"displayName":1536,"givenName":24,"familyName":24},"bae68f3f-a7b7-4e92-a916-af975167b7a2",[],[1526],{"id":1527,"sortIndex":25,"affiliation":1528,"properties":24},"da2836d8-c637-45c5-adaf-5961fc5904f7",{"id":1527,"createTime":24,"updateTime":24,"relativeEntities":1529,"slug":24,"properties":1530,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":1533,"statistic":24},[],{"title":1531},{"EN":1532},"Christian Doppler Laboratory for Molecular Recognition Materials, Department of Analytical Chemistry and Food Chemistry, University of Vienna, Vienna, Austria. Fax: 43‐1‐4277‐9523",[],{"title":1535,"openalex":1537},{"EN":1536},"Beatrix Preinerstorfer",{"VOID":1538},"A5054990053",{"id":1540,"sortIndex":153,"researcher":24,"roles":1541,"affiliations":1542,"properties":1549,"displayName":1551,"givenName":24,"familyName":24},"930f7043-eab6-478c-9933-1188f1c316f4",[],[1543],{"id":1527,"sortIndex":25,"affiliation":1544,"properties":24},{"id":1527,"createTime":24,"updateTime":24,"relativeEntities":1545,"slug":24,"properties":1546,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":1548,"statistic":24},[],{"title":1547},{"EN":1532},[],{"title":1550,"openalex":1552},{"EN":1551},"Michael 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Các CSP được chọn, phụ thuộc vào cấu trúc của các hợp chất được phân tách, có thể dựa trên các tác nhân chiral β‐cyclodextrin - β‐cyclodextrin không thay thế và β‐cyclodextrin ether hydroxypropyl, hoặc dựa trên kháng sinh đại phân tử - vancomycin, teicoplanin, aglycone teicoplanin và ristocetin A. Các phép đo được thực hiện trong chế độ phân tách pha đảo. Ảnh hưởng của thành phần pha di động lên khả năng giữ lại và phân tách enantiomer đã được nghiên cứu. Benzodiazepine có thể được phân tách enantiomer gần như với tất cả các pha tĩnh chiral được sử dụng, ngoại trừ CSP liên kết với vancomycin. Sự kết hợp đỉnh của oxazepam và lorazepam đã được quan sát nếu sự phân tách được thực hiện ở nhiệt độ phòng thí nghiệm. Nhiệt độ giảm cần thiết trong một số trường hợp để tránh sự racemization trên cột. Hệ thống phân tách gồm CSP liên kết với teicoplanin và các pha di động đệm-metanol hoặc metanol tinh khiết đã được chứng minh là phù hợp ngay cả cho các mục đích chuẩn bị do giá trị độ phân giải cao của các enantiomer. Sự phân tách enantiomer của các dẫn xuất phenothiazine khó đạt được hơn nhưng vẫn thành công, ít nhất một phần, với cả hai loại CSP được sử dụng (trừ levomepromazine).\u003C\u002Fjats:p>","\u003Cjats:title>Abstract\u003C\u002Fjats:title>\u003Cjats:p>Enantioselective separation of some phenothiazine and benzodiazepine derivatives was studied on six different chiral stationary phases (CSPs) in HPLC. Selected CSPs, with respect to the structure of the separated compounds, were either based on β‐cyclodextrin chiral selectors – underivatized β‐cyclodextrin and hydroxypropyl ether β‐cyclodextrin, or on macrocyclic antibiotics – vancomycin, teicoplanin, teicoplanin aglycone, and ristocetin A. Measurements were carried out in a reversed‐phase separation mode. The influence of mobile phase composition on retention and enantioseparation was studied. Benzodiazepines could be enantioresolved with almost all the chiral stationary phases used, except for the vancomycin‐bonded CSP. Peak coalescence of oxazepam and lorazepam was observed if separation was carried out at laboratory temperature. Reduced temperature was required in some instances in order to avoid the on‐column racemization. Separation systems composed of teicoplanin‐bonded CSP and buffer‐methanolic or pure methanolic mobile phases were shown to be suitable even for preparative purposes due to high resolution values of the enantiomers. Enantioseparation of phenothiazine derivatives was more difficult to achieve but it was successful, at least partly, also with both types of the CSPs used (except for levomepromazine).\u003C\u002Fjats:p>",{"EN":1788,"VI":1789},"Comparison of enantioseparation of selected benzodiazepine and phenothiazine derivatives on chiral stationary phases based on β‐cyclodextrin and macrocyclic antibiotics","So sánh sự phân tách enantiomer của một số dẫn xuất benzodiazepine và phenothiazine trên các pha tĩnh chiral dựa trên β‐cyclodextrin và kháng sinh đại phân tử",{"VI":597},{"VOID":1792},"10.1002\u002Fjssc.200301373","Author affiliation is blank",[125],[127],"https:\u002F\u002Fanalyticalsciencejournals.onlinelibrary.wiley.com\u002Fdoi\u002F10.1002\u002Fjssc.200301373",[1798,1809],{"id":1799,"sortIndex":25,"researcher":24,"roles":1800,"affiliations":1801,"properties":1802,"displayName":1806,"givenName":24,"familyName":24},"1a9660ac-48ba-436f-b260-618d384d1bc0",[],[],{"orcid":1803,"title":1805,"openalex":1807},{"VOID":1804},"https:\u002F\u002Forcid.org\u002F0000-0002-4372-8494",{"EN":1806},"Eva Tesařová",{"VOID":1808},"A5056898153",{"id":1810,"sortIndex":153,"researcher":24,"roles":1811,"affiliations":1812,"properties":1821,"displayName":1825,"givenName":24,"familyName":24},"82b19b4a-1487-44a6-a5b4-23592b4436c2",[],[1813],{"id":1814,"sortIndex":25,"affiliation":1815,"properties":24},"29aa1d5e-2474-40d3-9376-ba11f9ef6a5c",{"id":1814,"createTime":24,"updateTime":24,"relativeEntities":1816,"slug":24,"properties":1817,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":1820,"statistic":24},[],{"title":1818},{"VI":1819},"Department of Analytical Chemistry, Faculty of Science, Charles University, Albertov 2030, 12840 Prague 2, Czech Republic",[],{"orcid":1822,"title":1824,"openalex":1826},{"VOID":1823},"https:\u002F\u002Forcid.org\u002F0000-0002-8483-5739",{"EN":1825},"Zuzana Bosáková",{"VOID":1827},"A5034776627",{"url":24,"publisher":1829,"properties":1871},{"id":6,"createTime":7,"updateTime":8,"relativeEntities":1830,"slug":10,"properties":1831,"entityType":22,"verifyStatus":23,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":25,"subjectFields":1836,"manageAffiliations":1845,"indexDatabases":1856,"url":90,"thumbnailPath":24,"statistic":24,"gsStatistic":24,"type":24,"analyzePriority":24},[],{"country":1832,"eissn":1833,"issn":1834,"title":1835},{"VOID":13},{"VOID":15},{"VOID":17},{"EN":19},[1837,1841],{"id":28,"createTime":24,"updateTime":24,"relativeEntities":1838,"label":1839,"description":1840,"parentId":24,"standard":24,"scholarHubFieldId":24},[],{"EN":31},{},{"id":34,"createTime":24,"updateTime":24,"relativeEntities":1842,"label":1843,"description":1844,"parentId":24,"standard":24,"scholarHubFieldId":24},[],{"EN":37},{},[1846,1851],{"id":41,"createTime":24,"updateTime":24,"relativeEntities":1847,"slug":24,"properties":1848,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":1850,"statistic":24},[],{"title":1849},{"EN":45},[],{"id":48,"createTime":24,"updateTime":24,"relativeEntities":1852,"slug":24,"properties":1853,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":1855,"statistic":24},[],{"title":1854},{"EN":52},[],[1857,1864],{"id":56,"indexDatabase":1858,"url":67,"indexYears":68,"academicFieldIds":1863,"indexDatabaseRanking":72},{"id":58,"createTime":24,"updateTime":24,"relativeEntities":1859,"label":1860,"description":1861,"key":64,"publicationTags":1862,"standard":24},[],{"EN":61,"VI":61},{"EN":61,"VI":63},[66],[70,71],{"id":74,"indexDatabase":1865,"url":87,"indexYears":24,"academicFieldIds":1870,"indexDatabaseRanking":24},{"id":76,"createTime":24,"updateTime":24,"relativeEntities":1866,"label":1867,"description":1868,"key":83,"publicationTags":1869,"standard":24},[],{"EN":79,"VI":79},{"EN":81,"VI":82},[85,86],[89],{"issue":1872,"pages":1874,"volume":1876},{"VOID":1873},"8",{"VOID":1875},"661-668",{"VOID":1877},"26",9,{"total":1878,"publishYear":1880,"statisticByYear":1881},2003,{"2014":153,"2018":153},"2003-06-01",[85,72],[1885,1888,1891,1894,1897,1900,1903,1906,1909,1912,1915,1918,1921,1924,1927,1930,1933,1936,1939,1942,1945,1948,1951,1954,1957,1960,1963,1966,1969,1972,1975,1978],{"id":24,"text":1886,"url":24,"identifiers":1887},"10.1021\u002Fac00279a055",{"doi":1886},{"id":24,"text":1889,"url":24,"identifiers":1890},"10.1016\u002F0021-9673(92)85192-V",{"doi":1889},{"id":24,"text":1892,"url":24,"identifiers":1893},"10.1016\u002FS0021-9673(01)89435-8",{"doi":1892},{"id":24,"text":1895,"url":24,"identifiers":1896},"Beesley T. E., 1998, Chiral Chromatography",{},{"id":24,"text":1898,"url":24,"identifiers":1899},"10.1021\u002Fac00081a019",{"doi":1898},{"id":24,"text":1901,"url":24,"identifiers":1902},"10.1002\u002Fchir.530070614",{"doi":1901},{"id":24,"text":1904,"url":24,"identifiers":1905},"10.1002\u002F(SICI)1520-636X(1998)10:5\u003C434::AID-CHIR10>3.0.CO;2-0",{"doi":1904},{"id":24,"text":1907,"url":24,"identifiers":1908},"10.1080\u002F10826079808003415",{"doi":1907},{"id":24,"text":1910,"url":24,"identifiers":1911},"10.1080\u002F10826079308020940",{"doi":1910},{"id":24,"text":1913,"url":24,"identifiers":1914},"10.1016\u002FS0021-9673(97)00025-3",{"doi":1913},{"id":24,"text":1916,"url":24,"identifiers":1917},"10.1002\u002Fchir.530050206",{"doi":1916},{"id":24,"text":1919,"url":24,"identifiers":1920},"10.1016\u002F0021-9673(95)01123-4",{"doi":1919},{"id":24,"text":1922,"url":24,"identifiers":1923},"10.1080\u002F00032719708001675",{"doi":1922},{"id":24,"text":1925,"url":24,"identifiers":1926},"10.1016\u002FS0021-9673(97)00836-4",{"doi":1925},{"id":24,"text":1928,"url":24,"identifiers":1929},"10.1016\u002FS0021-9673(97)00928-X",{"doi":1928},{"id":24,"text":1931,"url":24,"identifiers":1932},"10.1016\u002FS0021-9673(99)01244-3",{"doi":1931},{"id":24,"text":1934,"url":24,"identifiers":1935},"10.1016\u002F0021-9673(94)80402-8",{"doi":1934},{"id":24,"text":1937,"url":24,"identifiers":1938},"10.1016\u002FS0021-9673(96)01097-7",{"doi":1937},{"id":24,"text":1940,"url":24,"identifiers":1941},"10.1002\u002Fchir.530040708",{"doi":1940},{"id":24,"text":1943,"url":24,"identifiers":1944},"10.1016\u002F0731-7085(91)80100-N",{"doi":1943},{"id":24,"text":1946,"url":24,"identifiers":1947},"10.1002\u002F1097-0231(20000715)14:13\u003C1128::AID-RCM1>3.0.CO;2-5",{"doi":1946},{"id":24,"text":1949,"url":24,"identifiers":1950},"Ameyibor E., 1997, J. High Resol. Chromatogr., 20, 855",{},{"id":24,"text":1952,"url":24,"identifiers":1953},"10.1007\u002FBF02276243",{"doi":1952},{"id":24,"text":1955,"url":24,"identifiers":1956},"Jira T., 1993, Pharmazie, 48, 196",{},{"id":24,"text":1958,"url":24,"identifiers":1959},"10.1016\u002FS0021-9673(01)88506-X",{"doi":1958},{"id":24,"text":1961,"url":24,"identifiers":1962},"10.1002\u002Fjhrc.1240201214",{"doi":1961},{"id":24,"text":1964,"url":24,"identifiers":1965},"10.1016\u002F0021-9673(94)00997-N",{"doi":1964},{"id":24,"text":1967,"url":24,"identifiers":1968},"10.1016\u002F0021-9673(95)01329-6",{"doi":1967},{"id":24,"text":1970,"url":24,"identifiers":1971},"10.1016\u002FS0378-4347(01)00559-X",{"doi":1970},{"id":24,"text":1973,"url":24,"identifiers":1974},"10.1016\u002F0731-7085(93)80207-H",{"doi":1973},{"id":24,"text":1976,"url":24,"identifiers":1977},"10.1021\u002Fac991004t",{"doi":1976},{"id":24,"text":1979,"url":24,"identifiers":1980},"10.1021\u002Fac960154q",{"doi":1979},{"id":1982,"createTime":1983,"updateTime":1984,"relativeEntities":1985,"slug":1986,"properties":1987,"entityType":120,"verifyStatus":121,"verifyTime":1983,"verifyNote":123,"languages":2003,"translateLanguages":2004,"viewCount":25,"primaryUrl":2005,"fullTextUrl":24,"authors":2006,"publicationType":215,"publisherRelationship":2079,"citationCount":2129,"citationInfo":2130,"publishDate":2133,"publishYear":2131,"citationAnalyzeStatus":23,"lastCitationAnalyze":24,"indexDatabases":2134,"openAccess":24,"references":2135,"isForceReanalyzing":584},"7ff4dff7-ea1c-448c-bc94-4c8e62c5b19d","2024-12-06T07:34:43.427+00:00","2025-01-08T18:24:14.254+00:00",[],"Preparative-isolation-and-purification-of-three-flavonoid-glycosides-from-i-Taraxacum-mongolicum-i-by-high-speed-counter-current-chromatography",{"mag":1988,"keywords":1990,"openalex":1991,"abstract":1993,"title":1996,"pm":1999,"doi":2001},{"VOID":1989},"1965126777",{"VI":597},{"VOID":1992},"W1965126777",{"VI":1994,"EN":1995},"\u003Cjats:title>Tóm tắt\u003C\u002Fjats:title>\u003Cjats:p>Phương pháp sắc ký đảo ngược tốc độ cao (HSCCC) đã được áp dụng để tinh chế ba glycosid flavonoid từ phần trên mặt đất của \u003Cjats:italic>Taraxacum mongolicum\u003C\u002Fjats:italic>, một loại thuốc truyền thống của Trung Quốc. Các phân tích tiếp theo bằng UV, MS và NMR đã dẫn đến việc xác định ba glycosid flavonoid bao gồm hai hợp chất mới là isoetin‐7‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐β‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐glucopyranosyl‐2′‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐α‐\u003Cjats:sc>L\u003C\u002Fjats:sc>‐arabinopyranoside và isoetin‐7‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐β‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐glucopyranosyl‐2′‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐α‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐glucopyranoside, cùng với một hợp chất đã biết, isoetin‐7‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐β‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐glucopyranosyl‐2′‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐α‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐xyloypyranoside, lần đầu tiên được tách chiết từ \u003Cjats:italic>T. mongolicum\u003C\u002Fjats:italic>. Hệ thống dung môi hai pha bao gồm ethyl acetate\u002F\u003Cjats:italic>n\u003C\u002Fjats:italic>‐butanol\u002Fnước (2:1:3, v\u002Fv\u002Fv) đã được thực hiện trong HSCCC. Kết quả, tổng cộng có 25,7 mg isoetin‐7‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐β‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐glucopyranosyl‐2′‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐α‐\u003Cjats:sc>L\u003C\u002Fjats:sc>‐arabinopyranoside, 19,1 mg isoetin‐7‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐β‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐glucopyranosyl‐2′‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐α‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐glucopyranoside, và 10,6 mg isoetin‐7‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐β‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐glucopyranosyl‐2′‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐α‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐xyloypyranoside đã được thu được với độ tinh khiết lần lượt là 98,7%, 98,3% và 99,1%, theo phương pháp HPLC từ 500 mg chiết xuất giàu sau khi làm sạch bằng nhựa polyamide.\u003C\u002Fjats:p>","\u003Cjats:title>Abstract\u003C\u002Fjats:title>\u003Cjats:p>A preparative high‐speed counter‐current chromatography (HSCCC) was successively applied to purify three flavonoid glycosides from the aerial part of\u003Cjats:italic> Taraxacum mongolicum\u003C\u002Fjats:italic>, a traditional Chinese medicine. Subsequent UV, MS, and NMR analyses have led to the characterization of three flavonoid glycosides including two new compounds isoetin‐7‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐β‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐glucopyranosyl‐2′‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐α‐\u003Cjats:sc>L\u003C\u002Fjats:sc>‐arabinopyranoside and isoetin‐7‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐β‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐glucopyranosyl‐2′‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐α‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐glucopyranoside, and a known compound, isoetin‐7‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐β‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐glucopyranosyl‐2′‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐α‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐xyloypyranoside, which were first isolated from\u003Cjats:italic> T. mongolicum\u003C\u002Fjats:italic>. The two‐phase solvent system composed of ethyl acetate\u002F\u003Cjats:italic>n\u003C\u002Fjats:italic>‐butanol\u002Fwater (2:1:3, v\u002Fv\u002Fv) was performed in HSCCC. Consequently, a total of 25.7 mg isoetin‐7‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐β‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐glucopyranosyl‐2′‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐α‐\u003Cjats:sc>L\u003C\u002Fjats:sc>‐arabinopyranoside, 19.1 mg isoetin‐7‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐β‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐glucopyranosyl‐2′‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐α‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐glucopyranoside, and 10.6 mg isoetin‐7‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐β‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐glucopyranosyl‐2′‐\u003Cjats:italic>O\u003C\u002Fjats:italic>‐α‐\u003Cjats:sc>D\u003C\u002Fjats:sc>‐xyloypyranoside were obtained with purity of 98.7, 98.3, and 99.1%, respectively, as determined by HPLC from 500 mg enriched extract after cleaning‐up by polyamide resin.\u003C\u002Fjats:p>",{"EN":1997,"VI":1998},"Preparative isolation and purification of three flavonoid glycosides from \u003Ci>Taraxacum mongolicum\u003C\u002Fi> by high‐speed counter‐current chromatography","Cách ly và tinh chế ba glycosid flavonoid từ \u003Ci>Taraxacum mongolicum\u003C\u002Fi> bằng sắc ký đảo ngược tốc độ cao",{"VOID":2000},"18240133",{"VOID":2002},"10.1002\u002Fjssc.200700409",[125],[127],"https:\u002F\u002Fanalyticalsciencejournals.onlinelibrary.wiley.com\u002Fdoi\u002F10.1002\u002Fjssc.200700409",[2007,2026,2045,2064],{"id":2008,"sortIndex":25,"researcher":24,"roles":2009,"affiliations":2010,"properties":2019,"displayName":2023,"givenName":24,"familyName":24},"b937f821-962e-4ebc-b03b-545ea3a5d152",[],[2011],{"id":2012,"sortIndex":25,"affiliation":2013,"properties":24},"47d49b6b-2471-44ca-8805-7b8eafdcfa60",{"id":2012,"createTime":24,"updateTime":24,"relativeEntities":2014,"slug":24,"properties":2015,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":2018,"statistic":24},[],{"title":2016},{"VI":2017},"School of Chemistry and Chemical Engineering, Central South University, Changsha, China",[],{"orcid":2020,"title":2022,"openalex":2024},{"VOID":2021},"https:\u002F\u002Forcid.org\u002F0000-0002-2873-9478",{"EN":2023},"Shuyun Shi",{"VOID":2025},"A5028093999",{"id":2027,"sortIndex":153,"researcher":24,"roles":2028,"affiliations":2029,"properties":2038,"displayName":2042,"givenName":24,"familyName":24},"6b78d1a8-9730-4693-8b33-aa096330ee9e",[],[2030],{"id":2031,"sortIndex":25,"affiliation":2032,"properties":24},"1b610d3d-1d26-4d0b-92f9-f2cf4810d5b3",{"id":2031,"createTime":24,"updateTime":24,"relativeEntities":2033,"slug":24,"properties":2034,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":2037,"statistic":24},[],{"title":2035},{"EN":2036},"School of Chemistry and Chemical Engineering, Central South University, Changsha, China. Fax: +86-731-8879850",[],{"orcid":2039,"title":2041,"openalex":2043},{"VOID":2040},"https:\u002F\u002Forcid.org\u002F0000-0002-3062-9382",{"EN":2042},"Yuping Zhang",{"VOID":2044},"A5100458685",{"id":2046,"sortIndex":181,"researcher":24,"roles":2047,"affiliations":2048,"properties":2057,"displayName":2061,"givenName":24,"familyName":24},"0afb69f9-d55c-47e0-a894-e45676b9f51a",[],[2049],{"id":2050,"sortIndex":25,"affiliation":2051,"properties":24},"c729f463-16ea-4028-8677-e64f88085f66",{"id":2050,"createTime":24,"updateTime":24,"relativeEntities":2052,"slug":24,"properties":2053,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":2056,"statistic":24},[],{"title":2054},{"VI":2055},"College of Pharmaceutical Sciences, Zhejiang University, Hangzhou, China",[],{"orcid":2058,"title":2060,"openalex":2062},{"VOID":2059},"https:\u002F\u002Forcid.org\u002F0000-0003-3100-893X",{"EN":2061},"Yu Zhao",{"VOID":2063},"A5101693162",{"id":2065,"sortIndex":199,"researcher":24,"roles":2066,"affiliations":2067,"properties":2074,"displayName":2076,"givenName":24,"familyName":24},"18b934b6-b2df-41ba-b04f-5ab08f84d872",[],[2068],{"id":2031,"sortIndex":25,"affiliation":2069,"properties":24},{"id":2031,"createTime":24,"updateTime":24,"relativeEntities":2070,"slug":24,"properties":2071,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":2073,"statistic":24},[],{"title":2072},{"EN":2036},[],{"title":2075,"openalex":2077},{"EN":2076},"Huang Ke-long",{"VOID":2078},"A5110367426",{"url":24,"publisher":2080,"properties":2122},{"id":6,"createTime":7,"updateTime":8,"relativeEntities":2081,"slug":10,"properties":2082,"entityType":22,"verifyStatus":23,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":25,"subjectFields":2087,"manageAffiliations":2096,"indexDatabases":2107,"url":90,"thumbnailPath":24,"statistic":24,"gsStatistic":24,"type":24,"analyzePriority":24},[],{"country":2083,"eissn":2084,"issn":2085,"title":2086},{"VOID":13},{"VOID":15},{"VOID":17},{"EN":19},[2088,2092],{"id":28,"createTime":24,"updateTime":24,"relativeEntities":2089,"label":2090,"description":2091,"parentId":24,"standard":24,"scholarHubFieldId":24},[],{"EN":31},{},{"id":34,"createTime":24,"updateTime":24,"relativeEntities":2093,"label":2094,"description":2095,"parentId":24,"standard":24,"scholarHubFieldId":24},[],{"EN":37},{},[2097,2102],{"id":41,"createTime":24,"updateTime":24,"relativeEntities":2098,"slug":24,"properties":2099,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":2101,"statistic":24},[],{"title":2100},{"EN":45},[],{"id":48,"createTime":24,"updateTime":24,"relativeEntities":2103,"slug":24,"properties":2104,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":2106,"statistic":24},[],{"title":2105},{"EN":52},[],[2108,2115],{"id":56,"indexDatabase":2109,"url":67,"indexYears":68,"academicFieldIds":2114,"indexDatabaseRanking":72},{"id":58,"createTime":24,"updateTime":24,"relativeEntities":2110,"label":2111,"description":2112,"key":64,"publicationTags":2113,"standard":24},[],{"EN":61,"VI":61},{"EN":61,"VI":63},[66],[70,71],{"id":74,"indexDatabase":2116,"url":87,"indexYears":24,"academicFieldIds":2121,"indexDatabaseRanking":24},{"id":76,"createTime":24,"updateTime":24,"relativeEntities":2117,"label":2118,"description":2119,"key":83,"publicationTags":2120,"standard":24},[],{"EN":79,"VI":79},{"EN":81,"VI":82},[85,86],[89],{"issue":2123,"pages":2125,"volume":2127},{"VOID":2124},"4",{"VOID":2126},"683-688",{"VOID":2128},"31",38,{"total":2129,"publishYear":2131,"statisticByYear":2132},2008,{"2012":153,"2013":199,"2014":199,"2015":181,"2016":199,"2017":153,"2019":153,"2020":181,"2021":693,"2022":153,"2023":153,"2024":181},"2008-03-01",[85,72],[2136,2139,2142,2145,2148,2151,2154,2157,2160,2163,2166,2169,2172,2175,2178,2181,2184,2187,2190,2193,2196,2199,2202,2205,2208,2211,2214],{"id":24,"text":2137,"url":24,"identifiers":2138},"Chinese National Pharmacopoeia Committee Pharmacopoeia Chinensis (Zhong Hua Ren Min Gong He Guo Yao Dian) Chemistry Engineering Publishers Beijing 2000 p. 289.",{},{"id":24,"text":2140,"url":24,"identifiers":2141},"Song L. Hong X. Ding X. Dictionary of Modern Chinese Medicine People's Health Publishers Beijing 2001 p. 2241.",{},{"id":24,"text":2143,"url":24,"identifiers":2144},"Ling Y., 1999, Zhongguo Zhongyao Zazhi, 24, 225",{},{"id":24,"text":2146,"url":24,"identifiers":2147},"Ling Y., 1997, Zhongguo Yaoxue Zazhi, 32, 584",{},{"id":24,"text":2149,"url":24,"identifiers":2150},"Yao W., 2007, Zhongguo Zhongyao Zazhi, 32, 926",{},{"id":24,"text":2152,"url":24,"identifiers":2153},"10.1016\u002Fj.fitote.2005.04.016",{"doi":2152},{"id":24,"text":2155,"url":24,"identifiers":2156},"10.1248\u002Fcpb.53.853",{"doi":2155},{"id":24,"text":2158,"url":24,"identifiers":2159},"Michalska K., 2005, Polym. J. Chem., 79, 1547",{},{"id":24,"text":2161,"url":24,"identifiers":2162},"10.1016\u002FS0367-326X(99)00158-6",{"doi":2161},{"id":24,"text":2164,"url":24,"identifiers":2165},"10.1021\u002Fjs980367q",{"doi":2164},{"id":24,"text":2167,"url":24,"identifiers":2168},"10.1016\u002Fj.jep.2006.07.021",{"doi":2167},{"id":24,"text":2170,"url":24,"identifiers":2171},"10.5012\u002Fbkcs.2007.28.8.1261",{"doi":2170},{"id":24,"text":2173,"url":24,"identifiers":2174},"10.1016\u002Fj.jchromb.2007.02.056",{"doi":2173},{"id":24,"text":2176,"url":24,"identifiers":2177},"10.1002\u002Fjssc.200500464",{"doi":2176},{"id":24,"text":2179,"url":24,"identifiers":2180},"10.1002\u002Fjssc.200600440",{"doi":2179},{"id":24,"text":2182,"url":24,"identifiers":2183},"10.1016\u002Fj.chroma.2007.04.027",{"doi":2182},{"id":24,"text":2185,"url":24,"identifiers":2186},"10.1016\u002Fj.seppur.2006.10.022",{"doi":2185},{"id":24,"text":2188,"url":24,"identifiers":2189},"10.1080\u002F10826070601093846",{"doi":2188},{"id":24,"text":2191,"url":24,"identifiers":2192},"10.1016\u002Fj.jchromb.2006.04.030",{"doi":2191},{"id":24,"text":2194,"url":24,"identifiers":2195},"10.1016\u002Fj.chroma.2004.12.026",{"doi":2194},{"id":24,"text":2197,"url":24,"identifiers":2198},"10.1016\u002Fj.chroma.2005.04.072",{"doi":2197},{"id":24,"text":2200,"url":24,"identifiers":2201},"10.1002\u002F1439-2054(20010301)286:3\u003C161::AID-MAME161>3.0.CO;2-Z",{"doi":2200},{"id":24,"text":2203,"url":24,"identifiers":2204},"Wu L. J. Natural Medicine Chemistry People's Health Publishers Beijing 2003 p. 183.",{},{"id":24,"text":2206,"url":24,"identifiers":2207},"10.1021\u002Fnp50052a014",{"doi":2206},{"id":24,"text":2209,"url":24,"identifiers":2210},"10.1016\u002F0031-9422(75)85050-3",{"doi":2209},{"id":24,"text":2212,"url":24,"identifiers":2213},"10.1016\u002Fj.enzmictec.2006.08.019",{"doi":2212},{"id":24,"text":2215,"url":24,"identifiers":2216},"10.1016\u002F0031-9422(91)84231-G",{"doi":2215},{"id":2218,"createTime":2219,"updateTime":2220,"relativeEntities":2221,"slug":2222,"properties":2223,"entityType":120,"verifyStatus":121,"verifyTime":2239,"verifyNote":123,"languages":2240,"translateLanguages":2241,"viewCount":25,"primaryUrl":2242,"fullTextUrl":24,"authors":2243,"publicationType":215,"publisherRelationship":2312,"citationCount":2361,"citationInfo":2362,"publishDate":2364,"publishYear":757,"citationAnalyzeStatus":23,"lastCitationAnalyze":24,"indexDatabases":2365,"openAccess":24,"references":2366,"isForceReanalyzing":584},"7c688368-4f4f-4929-9e4f-a901695ff242","2024-12-13T01:20:58.416+00:00","2025-01-08T18:23:14.608+00:00",[],"Simultaneous-separation-and-identification-of-limonoids-from-citrus-using-liquid-chromatography-collision-induced-dissociation-mass-spectra",{"mag":2224,"keywords":2226,"openalex":2227,"abstract":2229,"title":2232,"pm":2235,"doi":2237},{"VOID":2225},"1985072511",{"VI":597},{"VOID":2228},"W1985072511",{"VI":2230,"EN":2231},"\u003Cjats:title>Tóm tắt\u003C\u002Fjats:title>\u003Cjats:p>Các limonoid được coi là những tác nhân tiềm năng trong việc phòng ngừa ung thư và được phân bố rộng rãi trong chi \u003Cjats:italic>Citrus\u003C\u002Fjats:italic> dưới dạng aglycone và glucoside. Trong nghiên cứu hiện tại, phương pháp HPLC đảo ngược kết hợp với phổ khối lượng CID đã được phát triển để phân tách và xác định đồng thời các aglycone và glucoside từ limonoid có trong trái cây họ cam quýt. Năm aglycone như limonin, deacetyl nomilin, ichangin, axit isolimonoic và nomilin đã được xác định qua phổ khối lượng ion dương CID MS\u002FMS, trong khi năm glucoside, bao gồm: limonin glucoside, isoobacunoic acid glucoside, obacunone glucoside, deacetyl nomilinic acid glucoside và nomilinic acid glucoside được phân tích qua phổ khối lượng ion âm CID. Phương pháp đã phát triển được áp dụng thành công cho các mẫu trái cây họ cam quýt phức tạp để phân tách và xác định các aglycone và glucoside. Hạt cam quýt được chiết xuất bằng methanol và được tinh chế một phần, sau đó phân tích bằng phổ khối lượng LC-CID. Việc phân tách được thực hiện bằng cột C-18; tám loại limonoid đã được xác định bằng cách so sánh thời gian lưu và sự phân mảnh phổ khối lượng. Theo như chúng tôi biết, đây là báo cáo đầu tiên về việc xác định các limonoid trong trái cây họ cam quýt bằng kỹ thuật CID.\u003C\u002Fjats:p>","\u003Cjats:title>Abstract\u003C\u002Fjats:title>\u003Cjats:p>Limonoids are considered as potential cancer chemopreventive agents and are widely distributed in the \u003Cjats:italic>Citrus\u003C\u002Fjats:italic> genus as aglycones and glucosides. In the present study, reversed‐phase HPLC coupled with CID mass spectra was developed for the simultaneous separation and identification of aglycones and glucosides of limonoids from citrus. Five aglycones such as limonin, deacetyl nomilin, ichangin, isolimonoic acid and nomilin were identified by positive ion CID MS\u002FMS, whereas five glucosides, \u003Cjats:italic>viz.\u003C\u002Fjats:italic> limonin glucoside, isoobacunoic acid glucoside, obacunone glucoside, deacetyl nomilinic acid glucoside and nomilinic acid glucoside were analyzed by negative ion CID mass spectra. The developed method was successfully applied to complex citrus samples for the separation and identification of aglycones and glucosides. Citrus seeds were extracted with methanol and partially purified and analyzed by LC‐CID mass spectra. The separation was achieved by C‐18 column; eight limonoids were identified by comparing the retention times and mass spectral fragmentation. To the best of our knowledge, this is the first report on the identification of citrus limonoids using CID technique.\u003C\u002Fjats:p>",{"EN":2233,"VI":2234},"Simultaneous separation and identification of limonoids from citrus using liquid chromatography‐collision‐induced dissociation mass spectra","Phân tách và xác định đồng thời các limonoid từ trái cây họ cam quýt bằng phổ khối lượng gây ra bởi va chạm-điện tích",{"VOID":2236},"21171170",{"VOID":2238},"10.1002\u002Fjssc.201000644","2024-12-13T01:20:58.415+00:00",[125],[127],"https:\u002F\u002Fanalyticalsciencejournals.onlinelibrary.wiley.com\u002Fdoi\u002F10.1002\u002Fjssc.201000644",[2244,2263,2278,2295],{"id":2245,"sortIndex":25,"researcher":24,"roles":2246,"affiliations":2247,"properties":2256,"displayName":2260,"givenName":24,"familyName":24},"1f1c0ff0-1241-4a48-a4f6-0fb721c529a2",[],[2248],{"id":2249,"sortIndex":25,"affiliation":2250,"properties":24},"9d356a12-3495-4f72-9ba1-b89c8b71b68e",{"id":2249,"createTime":24,"updateTime":24,"relativeEntities":2251,"slug":24,"properties":2252,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":2255,"statistic":24},[],{"title":2253},{"VI":2254},"Vegetable and Fruit Improvement Center, Department of Horticultural Sciences, Texas A&M University, College Station, TX, USA",[],{"orcid":2257,"title":2259,"openalex":2261},{"VOID":2258},"https:\u002F\u002Forcid.org\u002F0000-0003-1749-9699",{"EN":2260},"G.K. Jayaprakasha",{"VOID":2262},"A5005034471",{"id":2264,"sortIndex":153,"researcher":24,"roles":2265,"affiliations":2266,"properties":2273,"displayName":2275,"givenName":24,"familyName":24},"be04d981-ab5e-4cea-8f4e-d9f4a3e27fc6",[],[2267],{"id":2249,"sortIndex":25,"affiliation":2268,"properties":24},{"id":2249,"createTime":24,"updateTime":24,"relativeEntities":2269,"slug":24,"properties":2270,"entityType":24,"verifyStatus":24,"verifyTime":24,"verifyNote":24,"languages":24,"translateLanguages":24,"viewCount":24,"url":24,"parentIds":2272,"statistic":24},[],{"title":2271},{"VI":2254},[],{"title":2274,"openalex":2276},{"EN":2275},"Deepak V. 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Các yếu tố ảnh hưởng đến hiệu suất làm giàu như thể tích mẫu, số lượng ống nanotube carbon đa thành và thể tích dung dịch eluent đã được nghiên cứu. Phương pháp tối ưu đã được xác minh dựa trên việc hiệu chuẩn tương thích ma trận, độ thu hồi, độ chính xác và độ tin cậy cho ba mẫu phân tích. Trong trường hợp cuối cùng, bài kiểm tra Student’s \u003Cjats:italic>t\u003C\u002Fjats:italic> phát triển đã chứng minh rằng không có sự khác biệt đáng kể giữa nồng độ thực tế và nồng độ được bổ sung. Điều kiện chiết tách pha rắn phân tán tối ưu (chiết 200 mL nước, pH 6.0, với 130 mg ống nanotube carbon đa thành, eluent bằng 25 mL dichloromethane cho nước chảy và nước máy và 30 mL cho nước khoáng) cho phép chiết xuất định lượng các chất phân tích ở mức thấp hơn giới hạn tối đa dư lượng được quy định bởi Liên minh Châu Âu, với LOD giao động từ 1.16 đến 93.6 ng\u002FL. Giá trị thu hồi tuyệt đối đạt được nằm trong khoảng 67–107% (giá trị RSD <10.1%).\u003C\u002Fjats:p>","\u003Cjats:p>In this manuscript, a dispersive SPE method based on the use of multiwalled carbon nanotubes has been developed for the determination of 15 organophosphorus pesticides residues including some of their metabolites (disulfoton sulfoxide, ethoprophos, cadusafos, dimethoate, terbufos, disulfoton, chlorpyrifos‐methyl, malaoxon, fenitrothion, pirimiphos‐methyl, malathion, chlorpyrifos, terbufos sulfone, disulfoton sulfone, and fensulfothion) from real environmental waters (run‐off, mineral and tap water) by GC with nitrogen phosphorus detection. Factors that affect the enrichment efficiency such as sample volume, multiwalled carbon nanotubes amount, and volume of eluent were studied. The optimized method was validated in terms of matrix‐matched calibration, recovery, precision, and accuracy for the three analyzed samples. In this last case, the developed Student´s \u003Cjats:italic>t\u003C\u002Fjats:italic> test demonstrated that there were no significant differences between real and spiked concentrations. Optimum dispersive SPE conditions (extraction of 200 mL of water, pH 6.0, with 130 mg of multiwalled carbon nanotubes, elution with 25 mL of dichloromethane for run‐off and tap water and 30 mL for mineral water) allowed the quantitative extraction of analytes at levels lower than the maximum residues limits legislated by the European Union, with LODs between 1.16 and 93.6 ng\u002FL. 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