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Journal of Medicine and Pharmacy","Tạp chí Y Dược học Cần Thơ",{"EN":487,"VI":488},"\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">04\u002F10\u002F2015 Ministry of Information and Communications allowed Can Tho journal of medicine and pharmacy to operate (102 \u002FGP-BTTTT)\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">07\u002F16\u002F2015 Can Tho journal of medicine and pharmacy is internationally recognized: ISSN 2354-1210\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">In 2016, The journal has been included in the list of medical science journals by The State Council for professorship which is awarded a work score of 0-0.5 points for a published article.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Can Tho Journal of Medicine and Pharmacy welcome original works that haven’t been submitted or published in other medical journals. Posts must contain content related to one of the journal’s categories.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">The content published\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">The journal is divided into 3 categories:\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">- Scientific research article: are valuable scientific works, which have been researched and accepted.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">- Overview of medicine, biology and pharmacy: serving the objective of continuing training in the fields of medicine, biology and pharmacy; to systematize classical and modern knowledge.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">- Update information on new knowledge about medicine, biology, pharmacy in the country and in the world.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Scope\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">- Publication and introduction of scientific research in the fields:\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">+ Medicine (internal medicine, surgery, pediatrics, obstetrics and gynecology, odonto-stomatology, laboratory, oncology, traditional medicine, nursing).\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">+ Biology (genetics, biotechnology).\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">+ Pharmacology (pharmaceutics, drug quality analysis-control, synthetic pharmaceutical chemistry, biochemistry, pharmacognosy, botany, clinical pharmacy).\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">- To enhance the quality of undergraduate, postgraduate education, scientifically researching and meet the necessary treatment in hospital.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">- Introducing the updated domestic and oversea information about science technology to promote scientific research and exchanging technology in local, other universities.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">- Exchanging pharmaceutical and medical information for social health developing in the Mekong Delta and Vietnam.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">The object\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Postgraduate students, student of Can Tho University of Medicine and Pharmacy, scientists from schools, research institutes, hospitals, health centers, pharmaceutical companies of the Mekong Delta; other provinces and regions in Vietnam and other country.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Address\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Headquarters of Can Tho Journal of Medicine and Pharmacy, located Scientific Research and International Cooperation Office: 179 Nguyen Van Cu Street, An Khanh Ward, Ninh Kieu District, Can Tho City, Vietnam.\u003C\u002Fspan>\u003C\u002Fp>","\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Ngày 16\u002F7\u002F2015, Tạp chí Y Dược học Cần Thơ được cấp chỉ số quốc tế: ISSN 2354-1210.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Từ tháng 4\u002F2016, Tạp chí đã được Hội đồng Giáo sư ngành Y đưa vào danh sách các tạp chí khoa học Y học được tính điểm công trình 0-0,5 điểm cho một bài báo đăng.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Năm 2020 Tạp chí Y Dược học Cần Thơ đã được phê duyệt vào danh mục của các Hội đồng Giáo sư ngành Dược học được tính điểm công trình 0-0,5 điểm cho một bài báo đăng.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Tạp chí Y Dược học Cần Thơ ra 12 số\u002Fnăm, 180-200 trang\u002Fsố.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Từ tháng 12\u002F2022 Tạp chí Y Dược học Cần Thơ là thành viên của hệ thống Crossref và từ tháng 01\u002F2023 tạp chí thực hiện bình duyệt online kín 2 chiều nhằm tăng tính minh bạch, tin cậy của các công trình nghiên cứu khoa học và đảm bảo tốt nhất chất lượng khoa học của bài viết.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Tôn chỉ, mục đích và phạm vi của tạp chí\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Tôn chỉ và mục đích hoạt động của tạp chí: xuất bản nhằm mục đích phổ biến kết quả từ các đề tài nghiên cứu khoa học; giao lưu trao đổi khoa học, chia sẻ kinh nghiệm, học tập, đồng thời cập nhật thông tin khoa học mới trong các lĩnh vực y, sinh, dược học trong và ngoài nước.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Phạm vi của tạp chí: Tạp chí xuất bản được chia thành 3 chuyên mục: (i) Bài báo nghiên cứu khoa học là kết quả công trình nghiên cứu khoa học có giá trị đã được triển khai nghiên cứu, (ii) Bài tổng quan y, sinh, dược học: phục vụ mục tiêu đào tạo liên tục trong lĩnh vực y, sinh, dược học; nhằm hệ thống hóa những kiến thức kinh điển và hiện đại; (iii) Thông tin cập nhật kiến thức mới về y, sinh, dược học trong nước và trên thế giới.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Chính sách truy cập mở\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Tạp chí Y Dược học Cần Thơ áp dụng chính sách truy cập mở đối với các bài báo đã xuất bản đến với độc giả, nhằm mở rộng cơ hội tiếp cận các kết quả nghiên cứu chất lượng cao và tăng cường trao đổi kiến thức. Tạp chí đăng tải trực tuyến (miễn phí) toàn văn các bài báo được công bố trên website của Tạp chí (https:\u002F\u002Ftapchi.ctump.edu.vn).\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Đạo đức xuất bản\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Tạp chí Y Dược học Cần Thơ cam kết tuân thủ đạo đức xuất bản phù hợp với các hướng dẫn và tiêu chuẩn của the Committee on Publication Ethics (COPE), tuân thủ các nguyên tắc của COPE’s Core Practices, Best Practices Guidelines for Journal Editors và Guidelines on Good Publication Practices.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Bản thảo bài báo chỉ được chấp nhận khi được tác giả chịu trách nhiệm chính cam kết các nội dung sau: Các nội dung của bản thảo chưa được đăng tải toàn bộ hoặc một phần ở các tạp chí khác; Tất cả các tác giả đều có đóng góp một cách đáng kể vào quá trình nghiên cứu hoặc chuẩn bị bản thảo và cùng chịu trách nhiệm về các nội dung của bản thảo; Tuân thủ các biện pháp đảm bảo đạo đức nghiên cứu (ví dụ thỏa thuận đồng ý tham gia nghiên cứu).\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Cam kết bảo mật\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Tạp chí cam kết thực hiện và tuân thủ các quy định của luật và các văn bản hướng dẫn liên quan đến bảo mật thông tin cá nhân trên không gian mạng. Các thông tin mà người dùng (tác giả, độc giả, biên tập viên, người phản biện) nhập vào các biểu mẫu trên Hệ thống Quản lý xuất bản trực tuyến của tạp chí chỉ được sử dụng vào các mục đích đã được tuyên bố rõ ràng và sẽ không được cung cấp cho bất kỳ bên thứ ba nào khác, hay dùng vào bất kỳ mục đích nào khác.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Phí gửi bài\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Lệ phí gửi đăng bài: 1.000.000đ\u002Fbài báo\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Lệ phí gửi đăng nhanh: 1.500.000đ\u002Fbài báo\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Đối với tác giả là cán bộ viên chức thuộc Trường Đại học Y Dược Cần Thơ thì được hỗ trợ 50% lệ phí gửi đăng bài.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Đối với sinh viên thực hiện đề tài nghiên cứu khoa học cấp trường được hỗ trợ 100% lệ phí đăng bài ( Tác giả gửi đính kèm “ Quyết định về việc giao tổ chức thực hiện đề tài nghiên cứu khoa học cấp Trường của sinh viên”).\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Hình thức nộp lệ phí:\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">1. Tiền mặt:\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Nộp trực tiếp tại Phòng Tài chính - Kế toán, Trường Đại học Y Dược Cần Thơ, số 179 Nguyễn Văn Cừ, P. An Khánh, Q. Ninh Kiều, thành phố Cần Thơ.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">2. Chuyển khoản:\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Tên Tài khoản: Trường ĐHYD Cần Thơ, Số TK: 0111000115668, tại ngân hàng Vietcombank chi nhánh Cần Thơ.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Thời gian: Áp dụng từ ngày 01\u002F02\u002F2023.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">* Phí gửi bài không được hoàn trả khi bài viết bị từ chối hoặc tác giả xin rút bài viết.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Quy trình phản biện bài báo\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Tạp chí Y Dược học Cần Thơ thực hiện quy trình phản biện kín hai chiều nghiêm ngặt. Danh tính của những người phản biện không được tiết lộ cho các tác giả và ngược lại. Quy trình thẩm định bài báo đăng gồm các bước sau:\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Tiếp nhận bản thảo\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Tác giả liên hệ gửi bản thảo đến Tạp chí qua hệ thống trực tuyến tại website: https:\u002F\u002Ftapchi.ctump.edu.vn. Hướng dẫn về cách đăng ký, gửi bài và chuẩn bị bản thảo được cung cấp trên website của Tạp chí.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Sàng lọc sơ bộ\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Sau khi Tòa soạn nhận được bài báo của tác giả, Ban Thư ký sẽ tiến hành kiểm tra sơ bộ bài báo (các yêu cầu về nội dung và hình thức). Những bài báo không đúng quy cách hoặc có nội dung không phù hợp hoặc vi phạm bản quyền sẽ bị từ chối (Ban Thư ký thông báo phản hồi đến tác giả trong vòng 1 tuần). Những bài báo đủ điều kiện, được Ban Thư ký tòa soạn chuyển đến Ban Biên tập có cùng chuyên môn với nội dung bài báo để đề xuất người phản biện. Thời gian kể từ khi Ban Biên tập nhận bài báo đến khi đề xuất người phản biện bài báo chậm nhất là 5 ngày.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Vòng phản biện\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">1. Ban Thư ký gửi bài và yêu cầu phản biện đến 02 phản biện độc lập.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">2. Các phản biện gởi nhận xét cho Ban Thư ký. Thời gian từ khi gửi bài cho phản biện đến khi nhận ý kiến của phản biện tối đa là 20 ngày.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Xử ký kết quả phản biện\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">1. Nếu ý kiến đồng ý cho đăng và không cần chỉnh sửa, Ban Thư ký tiếp tục đăng bài theo qui trình.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">2. Nếu ý kiến đồng ý đăng và cần chỉnh sửa, Ban Thư ký sẽ thông tin đến tác giả chỉnh sửa theo yêu cầu của người phản biện. Thời gian chỉnh sửa và gửi lại kéo dài không quá 2 tuần, từ khi tác giả bài báo nhận được thông tin (Quá trình này có thể lặp lại tối đa 2 lần\u002F1 bài báo). Khi có sự thống nhất, đồng ý của người phản biện; bài báo được tiếp tục đăng theo qui trình.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">3. Những bài báo có chất lượng không đạt yêu cầu, cả 2 phản biện không đồng ý cho đăng sẽ bị Tòa soạn từ chối đăng.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">Xuất bản\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">1. Ban Thư ký tổng hợp các bản thảo đã được tác giả hoàn thiện sau thẩm định trình Ban Biên tập xem xét, Tổng Biên tập phê duyệt, quyết định bài đăng theo các tiêu chí: sự phù hợp nội dung với tôn chỉ và mục đích, thể loại bài viết (ưu tiên các bài có bài có nghiên cứu chuyên sâu, hàm lượng khoa học cao), đóng góp mới bài báo, bài báo được ưu tiên đăng trong số gần nhất của Tạp chí theo thứ tự: tính thời sự, chất lượng bài báo và thời gian gửi bài.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">2. Ban Biên tập và Ban Thư ký biên tập bản thảo, chế bản, đọc rà soát lỗi. Thời gian hoàn thành từ 10-15 ngày.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">3. Ban Thư ký có trách nhiệm thông báo cho tác giả bài báo (bằng e-mail) về tình hình phê duyệt bài báo, thời gian, số kỳ, tập xuất bản bài báo theo qui định.\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>\u003Cp>\u003Cspan style=\"color: rgb(0, 0, 0);\">4. Danh sách bài báo theo số Tạp chí được in ấn và phát hành trong năm định kỳ được công bố chính thức trên website: https:\u002F\u002Ftapchi.ctump.edu.vn\u003C\u002Fspan>\u003C\u002Fp>\u003Cp>\u003Cbr>\u003C\u002Fp>",{"VOID":490},"wcQ1uqwAAAAJ","2023-05-30T08:17:21.868+00:00",[],[494],{"id":495,"createTime":28,"updateTime":28,"relativeEntities":496,"slug":28,"properties":497,"entityType":28,"verifyStatus":28,"verifyTime":28,"verifyNote":28,"languages":28,"translateLanguages":28,"viewCount":28,"url":507,"parentIds":508,"statistic":28},"6413896b-eca9-442b-a73f-182a58a0ce40",[],{"title":498,"address":501,"country":504,"abbreviation":505},{"EN":499,"VI":500},"Can Tho University of Medicine and Pharmacy","Trường Đại học Y Dược Cần Thơ",{"EN":502,"VI":503},"No 179, Nguyen Van Cu street, An Khanh ward, Ninh Kieu district, Can Tho city, Vietnam","Số 179, đường Nguyễn Văn Cừ, phường An Khánh, quận Ninh Kiều, thành phố Cần Thơ, Việt Nam",{"VOID":15},{"VOID":506},"ctump","http:\u002F\u002Fwww.ctump.edu.vn\u002F",[],[],"https:\u002F\u002Ftapchi.ctump.edu.vn\u002Findex.php\u002Fctump",{"impactFactor":32,"impactFactorByYear":512,"i10Index":32,"i10IndexLast5Year":32,"totalPublication":514,"totalPublicationByYear":515,"totalCitation":520,"totalCitationByYear":521,"totalCitationPerPublication":108,"totalCitationPerPublicationByYear":523,"hindexLast5Year":45,"hindex":45},{"2022":513,"2023":111,"2024":106},0.01,1556,{"2020":47,"2021":516,"2022":517,"2023":518,"2024":519,"2025":122},57,306,801,358,161,{"2021":146,"2022":280,"2023":522},99,{"2021":524,"2022":318,"2023":104},0.23,{"impactFactor":28,"impactFactorByYear":28,"i10Index":123,"i10IndexLast5Year":123,"totalPublication":526,"totalPublicationByYear":527,"totalCitation":526,"totalCitationByYear":528,"totalCitationPerPublication":40,"totalCitationPerPublicationByYear":531,"hindexLast5Year":49,"hindex":49},476,{"0":205,"2019":123,"2021":139,"2022":459,"2023":451,"2024":357,"2025":49,"2026":48},{"2021":42,"2022":123,"2023":161,"2024":529,"2025":360,"2026":530},136,83,{"2021":105,"2022":513,"2023":532,"2024":127,"2025":533,"2026":534},0.62,25.43,13.83,{"id":536,"createTime":537,"updateTime":382,"relativeEntities":538,"slug":539,"properties":540,"entityType":25,"verifyStatus":26,"verifyTime":28,"verifyNote":28,"languages":552,"translateLanguages":28,"viewCount":133,"subjectFields":553,"manageAffiliations":554,"indexDatabases":555,"url":556,"thumbnailPath":557,"statistic":558,"gsStatistic":594,"type":55,"analyzePriority":28},"6984a56a-db70-403b-9cc4-4013e1ceaffa","2023-05-09T06:47:40.346+00:00",[],"T%E1%BA%A1p%20ch%C3%AD%20Nghi%C3%AAn%20c%E1%BB%A9u%20n%C6%B0%E1%BB%9Bc%20ngo%C3%A0i",{"country":541,"issn":542,"title":544,"introduce":547,"gsId":550},{"VOID":15},{"VOID":543},"25252445",{"EN":545,"VI":546},"VNU Journal of Foreign Studies","Tạp chí Nghiên cứu nước ngoài",{"EN":548,"VI":549},"{\"ops\":[{\"insert\":\"\\n\\nThe \\n\"},{\"attributes\":{\"italic\":true},\"insert\":\"VNU Journal of Science\"},{\"insert\":\"\\n was established in 1985 for the publication of national and international research papers in all fields of natural sciences and technology, social sciences and humanities. 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H., 1957, Vapor Phase Chromatography",{},{"id":28,"text":1106,"url":28,"identifiers":1107},"Unter Kolonnenvolumen W soll das korrigierte Kolonnenvolumen W = W′–WIverstanden werden wobei W′ das Volumen der leeren Kolonne und WIdas durch den inaktiven Träger besetzte Volumen bedeuten. Siehe A.J. P.Martin&R. L. M.Synge2). Die Volumenanteile m und s werden auf W bezogen so dass m + s = 1.",{},{"id":28,"text":1109,"url":28,"identifiers":1110},"James D. H., J. chem. Soc., 1953, 1600",{},{"id":28,"text":1112,"url":28,"identifiers":1113},"James A. T., 1952, Anal. Chemistry, 77, 1915",{},{"id":28,"text":1115,"url":28,"identifiers":1116},"10.1042\u002Fbj0520242",{"doi":1115},{"id":28,"text":1118,"url":28,"identifiers":1119},"Cvetanovic R. J., 1957, Vapor Phase Chromatography",{},{"id":28,"text":1121,"url":28,"identifiers":1122},"10.1021\u002Fac50161a024",{"doi":1121},{"id":28,"text":1124,"url":28,"identifiers":1125},"10.1021\u002Fac60123a001",{"doi":1124},{"id":28,"text":1127,"url":28,"identifiers":1128},"Über die Art der verwendeten Standardverbindungen siehe4).",{},{"id":28,"text":1130,"url":28,"identifiers":1131},"Dadurch werden die n‐Paraffine gerader C‐Anzahl zur Standardreihe gewählt. Die physikalischen Eigenschaften der n‐Paraffine zeigen in Funktion der C‐Anzahl eine Oscillation zwischen n‐Paraffinen gerader und solchen ungerader C‐Anzahl. In der Reihe der n‐Paraffine mit gerader bzw. ungerader C‐Anzahl zeigt sich eine regelmässige Veränderung derselben Eigenschaften.",{},{"id":28,"text":1133,"url":28,"identifiers":1134},"Dieses Beispiel zeigt eine der Methoden zur Ermittlung des Retentionsindex. Standardverbindungen und die zu charakterisierende Substanz müssen nicht im selben Versuch jedoch bei der gleichen Temperatur und am selben Tag chromatographiert werden.",{},{"id":28,"text":1136,"url":28,"identifiers":1137},"Für eine nähere Beschreibung der stationären Phase siehe Abschnitt 1.",{},{"id":28,"text":1139,"url":28,"identifiers":1140},"Betr. die Ausgleichsrechnung siehe Anhang 33\u002F3.",{},{"id":28,"text":1142,"url":28,"identifiers":1143},"Zu dieser graphischen Darstellung wurden um einer grösseren Übersicht willen auch Daten herangezogen die in dieser Arbeit noch nicht tabelliert sind.",{},{"id":28,"text":1145,"url":28,"identifiers":1146},"Es scheint dass die hier abgeleiteten Beziehungen (8) und (9) für andere apolare stationäre Phasen ihre Gültigkeit beibehalten. Die Retentionsindices I78A die auf Grund der experimentellen Daten der Arbeit vonD. H.Desty&B. H. F.Whyman9) errechnet wurden (Apolare Kolonne: Hexatriacontan) stimmen mit unseren Resultaten befrie‐digend überein.",{},{"id":28,"text":1148,"url":28,"identifiers":1149},"Konstanz der Verdampfungsentropie bei der Siedetemperatur.",{},{"id":28,"text":1151,"url":28,"identifiers":1152},"Die Zahl und auch weitgehend die räumliche Anordnung der Elektronen in gleichlangen Abschnitten der Polyäthylenglykol‐Kette oder der n‐Paraffin‐Kette sind identisch.",{},{"id":28,"text":1154,"url":28,"identifiers":1155},"Weiterhin Komplexbildung wie davon z. B. an stationären Phasen mit Silbernitrat‐Zusatz (Komplexbildungzwischen Ag⊕und Doppelbindung) Gebrauch gemacht wird.",{},{"id":28,"text":1157,"url":28,"identifiers":1158},"F.Eisenlohr Spektrochemie organischer Verbindungen Enke Stuttgart1912.",{},{"id":28,"text":1160,"url":28,"identifiers":1161},"Ingold C. K., 1953, Structure and Mechanism in Organic Chemistry",{},{"id":28,"text":1163,"url":28,"identifiers":1164},"In dieser Diskussion wurde angenommen dass die polare stationäre Phase nur Äther‐Gruppen enthält. Die Äthylenglykol‐Kette ist aber nur einseitig veräthert so dass eine OH‐Gruppe frei bleibt. Wegen der niedrigen Konzentration wird die Wirkung dieser Gruppierung in den meisten Fällen vernachlässigbar sein jedoch könnte die mit dieser Gruppierung gebildete Wasserstoffbrücke im Falle der Aldehyde auch eine zusätzliche Retention bewirken.",{},{"id":28,"text":1166,"url":28,"identifiers":1167},"Der Autor dankt HerrnDr.T.Gäumannfür die kritische Auswahl der Dipolmomente. Die Dipolmomente der Halogenide wurden in der Gas‐Phase bestimmt die der Alkohole Aldehyde und Ketone wurden in Benzol gemessen.",{},{"id":28,"text":1169,"url":28,"identifiers":1170},"Keulemans A. I. M., 1957, Gas Chromatography",{},{"id":28,"text":1172,"url":28,"identifiers":1173},"Natl. Bureau of Standards Selected Valuès of Properties of Hydrocarbons API Res. Proj. 44.",{},{"id":28,"text":1175,"url":28,"identifiers":1176},"Dieser Korrekturfaktor fDist verschieden wenn sich der Strömungsmesser am Kolonnenanfang (fD= 3\u002F2 (p3–p) (p3–1)) oder am Ende der Kolonne (fD= 3\u002F2 (p2–1)\u002F(p3–1)) befindet.",{},{"id":28,"text":1178,"url":28,"identifiers":1179},"Wenn man die thermische Ausdehnung der Kolonnenfüllung und der Kolonne ausser Betracht lässt.",{},{"id":28,"text":1181,"url":28,"identifiers":1182},"E.Graf Dissertation ETH Zürich1955; «Scotch‐light»‐Kugeln: Minnesota Mining Corp. Mesh‐Fraktion 50–100.",{},{"id":28,"text":1184,"url":28,"identifiers":1185},"Als Manometerflüssigkeit diente Tetraäthylenglykol‐di‐n‐butyläther.",{},{"id":28,"text":1187,"url":28,"identifiers":1188},"Vgl.A. T.James&A. J. P.Martin1).",{},false,{"id":1191,"createTime":1192,"updateTime":1193,"relativeEntities":1194,"slug":1195,"properties":1196,"entityType":996,"verifyStatus":26,"verifyTime":1192,"verifyNote":997,"languages":1210,"translateLanguages":1211,"viewCount":32,"primaryUrl":1212,"fullTextUrl":28,"authors":1213,"publicationType":1019,"publisherRelationship":1231,"citationCount":1297,"citationInfo":1298,"publishDate":1301,"publishYear":1299,"citationAnalyzeStatus":884,"lastCitationAnalyze":28,"indexDatabases":1302,"openAccess":28,"references":1303,"isForceReanalyzing":1189},"9c296f80-7ccf-4e55-8544-7d8538c9a977","2024-09-20T06:14:58.905+00:00","2025-02-25T01:49:48.552+00:00",[],"Protonenresonanzspektrosopie-und-Steroidstruktur-II-Die-Lage-der-C-18-und-C-19-Methylsignale-in-Abh%C3%A4ngigkeit-von-den-Substituenten-am-Steroidger%C3%BCst",{"openalex":1197,"mag":1199,"abstract":1201,"title":1204,"keywords":1207,"doi":1208},{"VOID":1198},"W1967602172",{"VOID":1200},"1967602172",{"EN":1202,"VI":1203},"\u003Cjats:title>Abstract\u003C\u002Fjats:title>\u003Cjats:p>The proton NMR spectra of 265 steroids of known structure have been recorded for 0,1M solutions in deuterochloroform and the positions of the signals of the 18‐and 19‐hydrogen atoms have been measured. The additional chemical shifts due to various substituents at many different positions of the steroid skeleton are compiled in a table. With its help most chemical shifts of the 18‐ and 19‐hydrogen atoms of these and unknown steroids may be computed with an accuracy of ± 0,015 ppm. An example show how to calculate the chemical shifts. The physical basis of teh influences due to substituents and double bond, as well as the reasons for the generally small deviations from the calculated chemical shifts, are reviewed and illustrated. The additional chemical shifts due to identical funcitonal groups in equivalent positions, \u003Cjats:italic>i. e.\u003C\u002Fjats:italic> in approximately the same steric relation to one of the tertiary methyl groups, are collected in a table. Possible reason for teh variation of these additional chemical shifts within sets of identical functional functional groups in equivalent positions are discussed. The table furnishes interesting insights into the conformation of certain steroids and shows the average values and deviations one has to reckon with if the chemical shifts on methyl groups in non‐steroidal compounds due to functional groups in corresponding positions to those in steroids are to be computed.\u003C\u002Fjats:p>","\u003Cjats:title>Tóm tắt\u003C\u002Fjats:title>\u003Cjats:p>Quang phổ NMR proton của 265 steroid có cấu trúc đã biết được ghi lại cho dung dịch 0,1M trong deuterochloroform và vị trí của các tín hiệu của nguyên tử hydro 18 và 19 được đo. Các chuyển dịch hóa học bổ sung do các substituent khác nhau ở nhiều vị trí khác nhau của khung steroid đã được tổng hợp trong một bảng. Với sự trợ giúp của nó, hầu hết các chuyển dịch hóa học của các nguyên tử hydro 18 và 19 của những steroid này và các steroid chưa biết có thể được tính toán với độ chính xác ± 0,015 ppm. Một ví dụ cho thấy cách tính toán các chuyển dịch hóa học. Cơ sở vật lý của những ảnh hưởng do các substituent và liên kết đôi, cũng như lý do cho những sai lệch nhỏ nói chung so với các chuyển dịch hóa học đã tính toán, được xem xét và minh họa. Các chuyển dịch hóa học bổ sung do các nhóm chức tương tự ở các vị trí tương đương, \u003Cjats:italic>tức là\u003C\u002Fjats:italic> ở mối quan hệ không gian tương tự với một trong các nhóm methyl bậc ba, được thu thập trong một bảng. Các lý do có thể cho sự biến thiên của các chuyển dịch hóa học bổ sung này trong các tập hợp các nhóm chức tương tự ở các vị trí tương đương được thảo luận. Bảng cung cấp những hiểu biết thú vị về hình dạng của một số steroid và cho thấy các giá trị trung bình và sai lệch mà người ta phải tính đến nếu các chuyển dịch hóa học trên các nhóm methyl trong các hợp chất không giống steroid do các nhóm chức ở các vị trí tương ứng với những trong steroid được tính toán.\u003C\u002Fjats:p>",{"EN":1205,"VI":1206},"Protonenresonanzspektrosopie und Steroidstruktur. II. Die Lage der C‐18‐ und C‐19‐Methylsignale in Abhängigkeit von den Substituenten am Steroidgerüst","Quang phổ NMR proton và cấu trúc steroid. II. Vị trí của tín hiệu C‐18 và C‐19 methyl phụ thuộc vào các substituent trên khung steroid",{"VI":993},{"VOID":1209},"10.1002\u002Fhlca.19630460625",[31],[30],"https:\u002F\u002Fonlinelibrary.wiley.com\u002Fdoi\u002F10.1002\u002Fhlca.19630460625",[1214],{"id":1215,"sortIndex":32,"researcher":28,"roles":1216,"affiliations":1217,"properties":1226,"displayName":1228,"givenName":28,"familyName":28},"a91e9844-6d07-4b03-b9e1-bb8f2b5dd304",[],[1218],{"id":1219,"sortIndex":32,"affiliation":1220,"properties":28},"e897f169-1821-4433-acf5-677ec2dfcceb",{"id":1219,"createTime":28,"updateTime":28,"relativeEntities":1221,"slug":28,"properties":1222,"entityType":28,"verifyStatus":28,"verifyTime":28,"verifyNote":28,"languages":28,"translateLanguages":28,"viewCount":28,"url":28,"parentIds":1225,"statistic":28},[],{"title":1223},{"EN":1224},"CIBA AKTIENGESELLSCHAFT, Basel Physikalisches Laboratorium",[],{"title":1227,"openalex":1229},{"EN":1228},"R. F. Zürcher",{"VOID":1230},"A5089747581",{"url":28,"publisher":1232,"properties":1290},{"id":868,"createTime":869,"updateTime":870,"relativeEntities":1233,"slug":872,"properties":1234,"entityType":25,"verifyStatus":884,"verifyTime":28,"verifyNote":28,"languages":28,"translateLanguages":28,"viewCount":32,"subjectFields":1239,"manageAffiliations":1264,"indexDatabases":1275,"url":970,"thumbnailPath":28,"statistic":28,"gsStatistic":28,"type":28,"analyzePriority":28},[],{"country":1235,"eissn":1236,"issn":1237,"title":1238},{"VOID":875},{"VOID":877},{"VOID":879},{"EN":881},[1240,1244,1248,1252,1256,1260],{"id":887,"createTime":28,"updateTime":28,"relativeEntities":1241,"label":1242,"description":1243,"parentId":28,"standard":28,"scholarHubFieldId":28},[],{"EN":890},{},{"id":911,"createTime":28,"updateTime":28,"relativeEntities":1245,"label":1246,"description":1247,"parentId":28,"standard":28,"scholarHubFieldId":28},[],{"EN":914},{},{"id":893,"createTime":28,"updateTime":28,"relativeEntities":1249,"label":1250,"description":1251,"parentId":28,"standard":28,"scholarHubFieldId":28},[],{"EN":896},{},{"id":899,"createTime":28,"updateTime":28,"relativeEntities":1253,"label":1254,"description":1255,"parentId":28,"standard":28,"scholarHubFieldId":28},[],{"EN":902},{},{"id":905,"createTime":28,"updateTime":28,"relativeEntities":1257,"label":1258,"description":1259,"parentId":28,"standard":28,"scholarHubFieldId":28},[],{"EN":908},{},{"id":917,"createTime":28,"updateTime":28,"relativeEntities":1261,"label":1262,"description":1263,"parentId":28,"standard":28,"scholarHubFieldId":28},[],{"EN":920},{},[1265,1270],{"id":924,"createTime":28,"updateTime":28,"relativeEntities":1266,"slug":28,"properties":1267,"entityType":28,"verifyStatus":28,"verifyTime":28,"verifyNote":28,"languages":28,"translateLanguages":28,"viewCount":28,"url":28,"parentIds":1269,"statistic":28},[],{"title":1268},{"EN":928},[],{"id":931,"createTime":28,"updateTime":28,"relativeEntities":1271,"slug":28,"properties":1272,"entityType":28,"verifyStatus":28,"verifyTime":28,"verifyNote":28,"languages":28,"translateLanguages":28,"viewCount":28,"url":28,"parentIds":1274,"statistic":28},[],{"title":1273},{"EN":935},[],[1276,1283],{"id":939,"indexDatabase":1277,"url":945,"indexYears":946,"academicFieldIds":1282,"indexDatabaseRanking":954},{"id":775,"createTime":28,"updateTime":28,"relativeEntities":1278,"label":1279,"description":1280,"key":781,"publicationTags":1281,"standard":28},[],{"EN":778,"VI":778},{"EN":778,"VI":780},[783],[948,949,950,951,952,953],{"id":956,"indexDatabase":1284,"url":968,"indexYears":28,"academicFieldIds":1289,"indexDatabaseRanking":28},{"id":958,"createTime":28,"updateTime":28,"relativeEntities":1285,"label":1286,"description":1287,"key":965,"publicationTags":1288,"standard":28},[],{"EN":961,"VI":961},{"EN":963,"VI":964},[967,813],[816],{"issue":1291,"pages":1293,"volume":1295},{"VOID":1292},"6",{"VOID":1294},"2054-2088",{"VOID":1296},"46",500,{"total":1297,"publishYear":1299,"statisticByYear":1300},1963,{"2012":40,"2013":40,"2016":123},"1963-01-01",[954,967],[1304,1307,1310,1313,1316,1319,1322,1325,1328,1331,1334,1337,1340,1343,1346,1349,1352,1355,1358,1361,1364,1367,1370,1373,1376,1379,1382,1385,1388,1391,1394,1397,1400,1403,1406,1409,1412,1415,1418,1421,1424,1427,1430,1433,1436,1439,1442,1445,1448,1451],{"id":28,"text":1305,"url":28,"identifiers":1306},"10.1002\u002Fhlca.19610440525",{"doi":1305},{"id":28,"text":1308,"url":28,"identifiers":1309},"δ: chemische Verschiebung in ppm auf internes Tetramethylsilan (δ = 0) bezogen.",{},{"id":28,"text":1311,"url":28,"identifiers":1312},"10.1021\u002Fja01552a031",{"doi":1311},{"id":28,"text":1314,"url":28,"identifiers":1315},"10.1063\u002F1.1743676",{"doi":1314},{"id":28,"text":1317,"url":28,"identifiers":1318},"10.1098\u002Frspa.1957.0060",{"doi":1317},{"id":28,"text":1320,"url":28,"identifiers":1321},"Leichtverständliche Darstellung beiL. M.Jackman Applications of Nuclear Magnetic Resonance Spectroscopy in Organic Chemistry London1959 p.112ff.",{},{"id":28,"text":1323,"url":28,"identifiers":1324},"10.1139\u002Fv60-040",{"doi":1323},{"id":28,"text":1326,"url":28,"identifiers":1327},"In der demnächst erscheinenden Arbeit (III) vonR. F.Zürcher K.Heusler&J.Kalvodaüber die chemischen Verschiebungen der tertiären Methylgruppen bei Steroiden mit inneren Äthern und Lactonen wurde diese Arbeitsmethode ausgiebig angewendet.",{},{"id":28,"text":1329,"url":28,"identifiers":1330},"10.1063\u002F1.1733020",{"doi":1329},{"id":28,"text":1332,"url":28,"identifiers":1333},"10.1002\u002Fhlca.19610440632",{"doi":1332},{"id":28,"text":1335,"url":28,"identifiers":1336},"10.1063\u002F1.1732974",{"doi":1335},{"id":28,"text":1338,"url":28,"identifiers":1339},"10.1063\u002F1.1732975",{"doi":1338},{"id":28,"text":1341,"url":28,"identifiers":1342},"10.1039\u002Fdf9623400007",{"doi":1341},{"id":28,"text":1344,"url":28,"identifiers":1345},"Alle Angaben in Hz beziehen sich auf eine Resonanzfrequenz von 60 MHz.",{},{"id":28,"text":1347,"url":28,"identifiers":1348},"10.1021\u002Fja01489a059",{"doi":1347},{"id":28,"text":1350,"url":28,"identifiers":1351},"10.1021\u002Fj150567a041",{"doi":1350},{"id":28,"text":1353,"url":28,"identifiers":1354},"G. V. D.Tiers Proton Nuclear Shielding Values private Mitteilung.",{},{"id":28,"text":1356,"url":28,"identifiers":1357},"HerrProf.Ch.Tamm(Universitä Basel) hat uns diese Verbindungen freundlicherweise zur Verfügung gestelt.",{},{"id":28,"text":1359,"url":28,"identifiers":1360},"Eir danken HerrnDr.A.Fürst( F. Hoffmann‐La Roche) für die Überlassung dieser Verbindung.",{},{"id":28,"text":1362,"url":28,"identifiers":1363},"Wir sind HerrnProf.C. W.Shoppee(University of Sydney) fü die Überlassung dieser Substanzen zu Dank verpflichtet.",{},{"id":28,"text":1365,"url":28,"identifiers":1366},"Wir Danken HerrnDr.H. B.Mac Phillamy(CIBA Summit) bestens fü diese beiden Substanzen.",{},{"id":28,"text":1368,"url":28,"identifiers":1369},"Diese Verbindung verdanken wir HerrnDr.A.Von Wartburg(Sandoz).",{},{"id":28,"text":1371,"url":28,"identifiers":1372},"Diese Werte wurden nach Abschluss dieser Arbeit anhand von Steroiden berechnet die nicht in den Tabellen 1 und 2 aufgeführt sind.",{},{"id":28,"text":1374,"url":28,"identifiers":1375},"Jacquesy J.‐C., Bull. Soc. chim. France, 1961, 2444",{},{"id":28,"text":1377,"url":28,"identifiers":1378},"10.1021\u002Fja00875a048",{"doi":1377},{"id":28,"text":1380,"url":28,"identifiers":1381},"10.1248\u002Fcpb.10.338",{"doi":1380},{"id":28,"text":1383,"url":28,"identifiers":1384},"10.1021\u002Fja01518a047",{"doi":1383},{"id":28,"text":1386,"url":28,"identifiers":1387},"Diese Beiträge wurden nur anhandeinerVerbindung berechnet. Sie stimmen aber mit den in23) angegebenen Werten überein.",{},{"id":28,"text":1389,"url":28,"identifiers":1390},"Tori & Kondo28) berechnen auf Grund der Spektren von 3 20‐Dioxo‐17α‐hydroxy‐21‐acetoxy‐Δ4‐pregnen und 3 17‐Dioxo‐Δ4‐androsten den Beitrag einer 8β‐Hydroxygruppe zur chemischen Verschiebung der 18‐Wasserstoffatome auf 15 5 Hz (0 26 ppm). Unser Wert für diesen Beitrag fällt vielleicht etwas zu medrig aus infolge Wasserstoffbrückenbildung mit der 14β‐Hydroxygruppe (Steroide Nr. 233 und 234).",{},{"id":28,"text":1392,"url":28,"identifiers":1393},"10.1002\u002Fhlca.19630460139",{"doi":1392},{"id":28,"text":1395,"url":28,"identifiers":1396},"Tori K., 1963, Tetrahedron Letters, 10, 645",{},{"id":28,"text":1398,"url":28,"identifiers":1399},"Cox J. S. G., J. chem. Soc., 1960, 5118",{},{"id":28,"text":1401,"url":28,"identifiers":1402},"R. F.Zürcher wird veröffentlicht.",{},{"id":28,"text":1404,"url":28,"identifiers":1405},"30a Anmerkung bei der Korrektur: Der berechnete Beitrag der 11‐Ketogruppe zur chemischen Verschiebung der 19‐Wasserstoffatome stimmt dann mit dem experimentell bestimmten Wert überein wenn angenommen wird dass die Wasserstoffatome der tertiären Methylgruppen praktisch auf Lücke (staggered) stehen.",{},{"id":28,"text":1407,"url":28,"identifiers":1408},"Manhas M. S., Tetrahedron Letters, 1963, 1161",{},{"id":28,"text":1410,"url":28,"identifiers":1411},"10.1063\u002F1.1742249",{"doi":1410},{"id":28,"text":1413,"url":28,"identifiers":1414},"10.1139\u002Fv57-156",{"doi":1413},{"id":28,"text":1416,"url":28,"identifiers":1417},"Jacquesy Lehn & Levisalles21) finden für den Beitrag einer 5α‐Hydroxygruppe 10 0 Hz (19‐H). Dieser Wert ist im Vergleich zu den Beiträgen von 1α‐ und 12α‐Hydroxylen merkwürdig gross.",{},{"id":28,"text":1419,"url":28,"identifiers":1420},"Tori & Kondo28) berechnen eine zusätzliche chemische Verschiebung von 10 5 Hz (19‐H) verursacht durch eine 2β‐Hydroxygruppe jedoch in einem 3‐Oxo‐Δ4‐Steroid.",{},{"id":28,"text":1422,"url":28,"identifiers":1423},"Dieser Wert gilt für 5α‐Konfiguration. Bei 6β‐Hydroxy‐5α‐ oder 6β‐Hydroxy‐Δ4‐Steroiden beträgt die zusätzliche chemische Verschiebung 11 5 Hz (19‐H).",{},{"id":28,"text":1425,"url":28,"identifiers":1426},"Okamoto Tsuda und Mitarbeiter23) finden für die 7α‐Acetoxygruppe im 3 20‐Dioxo‐7α‐acetoxy‐pregnan Beiträge von 2 0 Hz (19‐H) und 1 5 Hz (18‐H).",{},{"id":28,"text":1428,"url":28,"identifiers":1429},"Dieser Wert stimmt bei 5α‐Konfiguration. Bei 5β‐ oder Δ4‐Steroiden ist der Beitrag einer 6β‐Acetoxygruppe 5 5 Hz (19‐H).",{},{"id":28,"text":1431,"url":28,"identifiers":1432},"Cox Bishop & Richards29) schätzen den Beitrag eines 9α‐Bromatoms auf 12 0 Hz (19‐H).",{},{"id":28,"text":1434,"url":28,"identifiers":1435},"10.1021\u002Fja01480a015",{"doi":1434},{"id":28,"text":1437,"url":28,"identifiers":1438},"Trenner N. R., Proc. chem. Soc. (London), 1961, 214",{},{"id":28,"text":1440,"url":28,"identifiers":1441},"E. L.Eliel Stereochemistry of Carbon Compounds New York1962 Tabelle 8–7 p.237.",{},{"id":28,"text":1443,"url":28,"identifiers":1444},"10.1021\u002Fja01483a028",{"doi":1443},{"id":28,"text":1446,"url":28,"identifiers":1447},"10.1063\u002F1.1729860",{"doi":1446},{"id":28,"text":1449,"url":28,"identifiers":1450},"Abraham R. J., J. chem. Soc., 1963, 806",{},{"id":28,"text":1452,"url":28,"identifiers":1453},"10.1016\u002F0040-4020(58)88024-2",{"doi":1452},{"id":1455,"createTime":1456,"updateTime":1457,"relativeEntities":1458,"slug":1459,"properties":1460,"entityType":996,"verifyStatus":26,"verifyTime":1456,"verifyNote":997,"languages":1474,"translateLanguages":1475,"viewCount":32,"primaryUrl":1476,"fullTextUrl":28,"authors":1477,"publicationType":1019,"publisherRelationship":1495,"citationCount":1561,"citationInfo":1562,"publishDate":1565,"publishYear":1563,"citationAnalyzeStatus":884,"lastCitationAnalyze":28,"indexDatabases":1566,"openAccess":28,"references":1567,"isForceReanalyzing":1189},"000a3320-bac1-4c33-94d6-847c67c8536f","2024-10-09T22:13:38.953+00:00","2025-02-25T01:50:46.259+00:00",[],"Chiral-and-Achiral-Crystal-Structures",{"openalex":1461,"mag":1463,"abstract":1465,"title":1468,"keywords":1471,"doi":1472},{"VOID":1462},"W2166602283",{"VOID":1464},"2166602283",{"EN":1466,"VI":1467},"\u003Cjats:title>Abstract\u003C\u002Fjats:title>\u003Cjats:p>An extensive study and analysis of the concepts, classification, presentation, and nomenclature of chirality and lack of chirality in crystal structures and their constituents is presented. Oriented crystal structures are classified. The chirality rules for existence of molecular crystal structures are examined and the relation to segmentation and latent symmetry highlighted. The nomenclature of chirality and related terms, and the relationship of chirality to optical activity is covered. The uses and limitations of the Euclidean normalizer are treated. An improved glossary of terms is included.\u003C\u002Fjats:p>","\u003Cjats:title>Tóm tắt\u003C\u002Fjats:title>\u003Cjats:p>Đã trình bày một nghiên cứu và phân tích sâu rộng về các khái niệm, phân loại, cách trình bày và cách đặt tên của tính xoay chiral và sự thiếu hụt tính xoay chiral trong các cấu trúc kết tinh và các thành phần của chúng. Các cấu trúc kết tinh có định hướng được phân loại. Các quy tắc chiral cho sự tồn tại của các cấu trúc kết tinh phân tử được xem xét và mối quan hệ với sự phân đoạn và đối xứng tiềm ẩn được làm nổi bật. Cách đặt tên cho chiral và các thuật ngữ liên quan, cũng như mối quan hệ giữa chiral và hoạt động quang được đề cập. Các ứng dụng và giới hạn của bộ chuẩn Euclid cũng được đề cập. Một từ điển thuật ngữ cải tiến được bao gồm.\u003C\u002Fjats:p>",{"EN":1469,"VI":1470},"Chiral and Achiral Crystal Structures","Cấu Trúc Kết Tinh Chiral và Achiral",{"VI":993},{"VOID":1473},"10.1002\u002Fhlca.200390109",[31],[30],"https:\u002F\u002Fonlinelibrary.wiley.com\u002Fdoi\u002F10.1002\u002Fhlca.200390109",[1478],{"id":1479,"sortIndex":32,"researcher":28,"roles":1480,"affiliations":1481,"properties":1490,"displayName":1492,"givenName":28,"familyName":28},"e153fced-b8fb-4856-8192-ceb5c528eef8",[],[1482],{"id":1483,"sortIndex":32,"affiliation":1484,"properties":28},"89a9d1bd-2266-421e-9aff-a2ea03a20893",{"id":1483,"createTime":28,"updateTime":28,"relativeEntities":1485,"slug":28,"properties":1486,"entityType":28,"verifyStatus":28,"verifyTime":28,"verifyNote":28,"languages":28,"translateLanguages":28,"viewCount":28,"url":28,"parentIds":1489,"statistic":28},[],{"title":1487},{"EN":1488},"Laboratoire de Cristallographie, University of Geneva, 24 quai Ernest-Ansermet, CH1211 Geneva 4 (phone: + 41 22 702 62 49, fax: + 41 22 702 61 08)",[],{"title":1491,"openalex":1493},{"EN":1492},"H. D. 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Bertaut",{},{"id":28,"text":1755,"url":28,"identifiers":1756},"10.1021\u002Fcm00044a010",{"doi":1755},{"id":1758,"createTime":1759,"updateTime":1760,"relativeEntities":1761,"slug":1762,"properties":1763,"entityType":996,"verifyStatus":26,"verifyTime":1759,"verifyNote":997,"languages":1777,"translateLanguages":1778,"viewCount":32,"primaryUrl":1779,"fullTextUrl":28,"authors":1780,"publicationType":1019,"publisherRelationship":1839,"citationCount":1905,"citationInfo":1906,"publishDate":1909,"publishYear":1907,"citationAnalyzeStatus":884,"lastCitationAnalyze":28,"indexDatabases":1910,"openAccess":28,"references":1911,"isForceReanalyzing":1189},"3038f3c5-ab1c-4483-bcee-b4614b524cfa","2024-11-25T19:22:21.451+00:00","2025-02-25T01:51:43.474+00:00",[],"Synthesis-of-Open-Chain-2-3-Disubstituted-4-nitroketones-by-Diastereoselective-i-Michael-i-addition-of-i-E-i-Enamines-to-i-E-i-Nitroolefins-A-topological-rule-for-C-C-bond-forming-processes-between-prochiral-centres-Preliminary-communication",{"openalex":1764,"mag":1766,"abstract":1768,"title":1771,"keywords":1774,"doi":1775},{"VOID":1765},"W2063316574",{"VOID":1767},"2063316574",{"EN":1769,"VI":1770},"\u003Cjats:title>Abstract\u003C\u002Fjats:title>\u003Cjats:p>The \u003Cjats:italic>Michael\u003C\u002Fjats:italic>‐additions of aliphatic, alicyclic, and arylsubstituted nitroolefins and enamines lead to γ‐nitroketones \u003Cjats:bold>3\u003C\u002Fjats:bold> in good chemical and excellent (> 90%) diastereomeric yields (see \u003Cjats:italic>Table 1\u003C\u002Fjats:italic>).\u003C\u002Fjats:p>\u003Cjats:p>The known \u003Cjats:italic>threo\u003C\u002Fjats:italic>‐configuration of one type of adducts \u003Cjats:bold>3\u003C\u002Fjats:bold> (entries 8, 10, and 11 of \u003Cjats:italic>Table 1\u003C\u002Fjats:italic>) can be arrived at by assuming the approach \u003Cjats:bold>8\u003C\u002Fjats:bold> of the \u003Cjats:italic>Michael\u003C\u002Fjats:italic>‐acceptor and ‐donor; the reaction follows a \u003Cjats:italic>topological rule\u003C\u002Fjats:italic>, which is formulated and which is applicable to such diverse reactions as the diene synthesis, cyclopropanations, carbonyl olefinations and methylenations, aldol‐ and nitroaldol‐type additions, as well as additions of lithium, boron, and chromium derivatives to aldehydes (see \u003Cjats:bold>9\u003C\u002Fjats:bold>, \u003Cjats:bold>10\u003C\u002Fjats:bold>, \u003Cjats:bold>11\u003C\u002Fjats:bold>, and \u003Cjats:italic>Table 2\u003C\u002Fjats:italic>).\u003C\u002Fjats:p>","\u003Cjats:title>Tóm tắt\u003C\u002Fjats:title>\u003Cjats:p>Phản ứng \u003Cjats:italic>Michael\u003C\u002Fjats:italic> của các nitroolefins và enamines không phân nhánh, vòng và aryl dẫn đến các γ‐nitroketones \u003Cjats:bold>3\u003C\u002Fjats:bold> với hiệu suất hóa học tốt và độ chọn lọc diastereomer trên 90% (xem \u003Cjats:italic>Bảng 1\u003C\u002Fjats:italic>).\u003C\u002Fjats:p>\u003Cjats:p>Cấu hình \u003Cjats:italic>threo\u003C\u002Fjats:italic> đã biết của một loại sản phẩm \u003Cjats:bold>3\u003C\u002Fjats:bold> (các mục 8, 10 và 11 của \u003Cjats:italic>Bảng 1\u003C\u002Fjats:italic>) có thể đạt được bằng cách giả định cách tiếp cận \u003Cjats:bold>8\u003C\u002Fjats:bold> của chất nhận và chất cho \u003Cjats:italic>Michael\u003C\u002Fjats:italic>; phản ứng tuân theo một \u003Cjats:italic>quy tắc hình học\u003C\u002Fjats:italic> được xây dựng và có thể áp dụng cho những phản ứng đa dạng như tổng hợp diene, cyclopropanations, carbonyl olefinations và methylenations, cũng như các phản ứng aldol và nitroaldol, cũng như sự bổ sung của các dẫn xuất lithium, boron và chromium vào aldehyde (xem \u003Cjats:bold>9\u003C\u002Fjats:bold>, \u003Cjats:bold>10\u003C\u002Fjats:bold>, \u003Cjats:bold>11\u003C\u002Fjats:bold> và \u003Cjats:italic>Bảng 2\u003C\u002Fjats:italic>).\u003C\u002Fjats:p>",{"EN":1772,"VI":1773},"Synthesis of Open‐Chain 2,3‐Disubstituted 4‐nitroketones by Diastereoselective \u003Ci>Michael\u003C\u002Fi>‐addition of (\u003Ci>E\u003C\u002Fi>)‐Enamines to (\u003Ci>E\u003C\u002Fi>)‐Nitroolefins. A topological rule for C, C‐bond forming processes between prochiral centres. Preliminary communication","Tổng hợp 4‐nitroketones 2,3‐Disubstituted chuỗi mở bằng phản ứng \u003Ci>Michael\u003C\u002Fi> chọn lọc diastereomer giữa (\u003Ci>E\u003C\u002Fi>)-Enamines và (\u003Ci>E\u003C\u002Fi>)-Nitroolefins. 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I bezeichnet; siehe auchWo.Ostwald",{},{"id":28,"text":2489,"url":28,"identifiers":2490},"1927, Koll. Z., 53, 190",{},{"id":28,"text":2492,"url":28,"identifiers":2493},"10.1007\u002FBF01428306",{"doi":2492},{"id":28,"text":2495,"url":28,"identifiers":2496},"10.1007\u002FBF01422711",{"doi":2495},{"id":28,"text":2498,"url":28,"identifiers":2499},"10.1007\u002FBF01425465",{"doi":2498},{"id":28,"text":2501,"url":28,"identifiers":2502},"Kuhn W., 1932, Z. physikal. Ch. [A], 161, 427",{},{"id":28,"text":2504,"url":28,"identifiers":2505},"10.1002\u002Fhlca.19430260111",{"doi":2504},{"id":28,"text":2507,"url":28,"identifiers":2508},"Über eine genauere theoretische Begründung dieser empirischen Formel soll später berichtet werden.",{},{"id":28,"text":2510,"url":28,"identifiers":2511},"Polson A., 1938, Koll. Z., 83, 173",{},{"id":28,"text":2513,"url":28,"identifiers":2514},"10.1002\u002Fhlca.19380210176",{"doi":2513},{"id":28,"text":2474,"url":28,"identifiers":2516},{"doi":2474},{"id":28,"text":2474,"url":28,"identifiers":2518},{"doi":2474},{"id":28,"text":2520,"url":28,"identifiers":2521},"10.1007\u002FBF01793684",{"doi":2520},{"id":28,"text":2523,"url":28,"identifiers":2524},"10.1007\u002FBF01451143",{"doi":2523},{"id":28,"text":2526,"url":28,"identifiers":2527},"l. c. IV.",{},{"id":28,"text":2529,"url":28,"identifiers":2530},"10.1007\u002FBF01510431",{"doi":2529},{"id":28,"text":2532,"url":28,"identifiers":2533},"l. c. I.",{},{"id":28,"text":2535,"url":28,"identifiers":2536},"10.1007\u002FBF01341776",{"doi":2535},{"id":28,"text":2538,"url":28,"identifiers":2539},"A.Wissler Diss. Bern1941.",{},{"id":28,"text":2541,"url":28,"identifiers":2542},"Die Gestzmässigkeit ist umso mehr hervorzuheben als sie den Autoren der Messungen selbst entgangen ist.",{},{"id":28,"text":2544,"url":28,"identifiers":2545},"Signer R., 1933, Z. physikal. Ch. [A], 165, 161, 10.1515\u002Fzpch-1933-16517",{"doi":2546},"10.1515\u002Fzpch-1933-16517",{"id":28,"text":2548,"url":28,"identifiers":2549},"10.1002\u002Fhlca.19340170112",{"doi":2548},{"id":28,"text":2551,"url":28,"identifiers":2552},"Tatsächlich werden wir unten (Abschnitt 10a) sehen dass die (negative) Eigendoppelbrechung des Polystyrols gerade im Lösungsmittel Cyclohexanon weitgehend durch die (stets positive) Stäbchendoppelbrechung kompensiert wird. Wir haben daher für α1–α2einen zu hohen Wert eingesetzt. Dieser Fehler hob sich weg indem auch der Raumerfüllungseffekt welcher sich auf den Winkel β auswirken würde nicht berücksichtigt wurde.",{},{"id":28,"text":2554,"url":28,"identifiers":2555},"10.1007\u002FBF01512208",{"doi":2554},{"id":28,"text":2557,"url":28,"identifiers":2558},"1933, Koll. 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Auf Grund der dort angegebenen Zahlenwerte würde λ = 6 3 erhalten; der von uns geschätzte Wert 3 π\u002F2 = 4 7 ist hiervon nur wenig verschieden so dass der Wert λ = 3 π\u002F2 als durchaus gute Näherung vorläufig weiter benützt werden soll.",{},{"id":28,"text":2589,"url":28,"identifiers":2590},"Staudinger, 1935, B., 68, 2320",{},{"id":28,"text":2592,"url":28,"identifiers":2593},"10.1002\u002Fhlca.193601901176",{"doi":2592},{"id":28,"text":2595,"url":28,"identifiers":2596},"Die angeführten Km‐Werte wurden aus Philippoff viskostät der Kolloide Dresden und Leipzig1942 S.364",{},{"id":28,"text":2598,"url":28,"identifiers":2599},"und ausHouwink Chemie und Technologie der Kunststoffe Leipzig1939 S.64entanommen.",{},{"id":28,"text":2601,"url":28,"identifiers":2602},"1936, G., 66, 491",{},{"id":28,"text":2580,"url":28,"identifiers":2604},{},{"id":28,"text":2606,"url":28,"identifiers":2607},"SignerundGross l. c.",{},{"id":28,"text":2609,"url":28,"identifiers":2610},"Bei Nitrocellulosen sind die angegebenen ηsp\u002Fc Werte aus Messungen von Fivian Diss. Bern 1939 an den gleichen Produkten im Lösungsmittel Butylacetat auf das für die Strömungsdoppelbrechungsversuche als Lösungsmittel verwendete Cyclohexanon umgerechnet.",{},{"id":28,"text":2612,"url":28,"identifiers":2613},"A.Wissler l. c.",{},{"id":28,"text":2615,"url":28,"identifiers":2616},"Es muss allerdings gesagt werden dass bei den von Signer und Gross untersuchten Nitrocellulosen der Quotient ν·c\u002Fηspmit steigendem Molekulargewicht beträchtlich zunimmt während er bei den an der gleichen Stoffart von Wissler gemachten Untersuchungen konstant bleibt; die Abweichung beruht möglicherweise darauf dass die Signer'schen Produkte nicht genügend monodispers waren.",{},{"id":28,"text":2618,"url":28,"identifiers":2619},"Signer, 1930, Z. physikal. Ch. [A], 150, 257, 10.1515\u002Fzpch-1930-15023",{"doi":2620},"10.1515\u002Fzpch-1930-15023",{"id":28,"text":2612,"url":28,"identifiers":2622},{},{"id":28,"text":2624,"url":28,"identifiers":2625},"R.SignerundP.v. Tavel l. c.",{},{"id":28,"text":2627,"url":28,"identifiers":2628},"Wir können diese Tatsache beispielsweise dazu verwenden um aus den strömungsoptischen Messungen vonA.Wissleran thymonucleinsaurem Natrium das ungefähre Molekulargewicht dieser Substanz zu ermitteln. Wissler (l.c.) stellte an einer wässerigen Lösung von Natriumthymonucleinat der er zur Aufhebung des elektroviskosen Effekts 1% Natriumchlorid beigefügt hatte eine Viskositätsazhl (ηsp\u002FP) = 5 7 und eine Orientierungsazhl (ω\u002Fη0q) = 0 041 fest.",{},{"id":28,"text":2630,"url":28,"identifiers":2631},"Nun ist das thymonucleinasure Natrium eine hochpolymere Kettenmolekel über deren Gestalt (Stäbchen durchspülte Knäuel) wir von vornherein nichts aussagen können. Wir werden daher versuchsweise das Molekulargewicht aus (55b) oder (56b) berechnen. Durch Einstezen der Wissler′schen Messresultate in (55b) erhalten wir ein Molekulargewicht M = 1 7 × 106liegen dürfte. Dieser Wert steht mit demjenigen den man auf Grund verschiedener Beobachtungen an Thymonucleinsäure schätzt (etwa 106) in guter Übereinstimmung",{},{"id":28,"text":2633,"url":28,"identifiers":2634},"10.1007\u002FBF01475301",{"doi":2633},{"id":28,"text":2636,"url":28,"identifiers":2637},"Auf Grund eines weiter unten (im Anschluss an Gl. (63)) mitgeteilten Kriteriums lässt sich zeigen dans Natriumthymonucleinat nicht aus starren eine Valenzkette bildenden Stäben mit monomolekularer Querabmessung bestehen kann (für die Länge des monomeren Restes würde sich ein unmöglicher Wert nämlich b = 1 8 × 10−9cm ergeben während man unter der gemachten Annahme 6 × 10−8cm erwartet). Dagegen lässt sich aus denWissler′schen Angaben nicht entscheiden ob man es mit undurchspülten Knäueln oder mit kurzen relativ dicken Krystallistäben zu tun hat. Die Auswertung der Annahme dass bespülte Knäel vorliegen führt zu einem an sich möglichen Wert für die Parameter b Amusw. jedoch mit deutlichen Anzeichen defür dass undurschspülte Knäuel oder sogar eine Art länglicher Krystallite (= in sich stark assoziierte längliche undurchspülte Knäel) vorliegen.",{},{"id":2639,"createTime":2640,"updateTime":2641,"relativeEntities":2642,"slug":2643,"properties":2644,"entityType":996,"verifyStatus":26,"verifyTime":2640,"verifyNote":997,"languages":2658,"translateLanguages":2659,"viewCount":32,"primaryUrl":2660,"fullTextUrl":28,"authors":2661,"publicationType":1019,"publisherRelationship":2693,"citationCount":2758,"citationInfo":2759,"publishDate":2762,"publishYear":2760,"citationAnalyzeStatus":884,"lastCitationAnalyze":28,"indexDatabases":2763,"openAccess":28,"references":2764,"isForceReanalyzing":1189},"1adaac34-1afe-4582-bb02-9db501c076e3","2024-09-12T01:58:25.495+00:00","2025-02-25T01:53:34.059+00:00",[],"Substitution-of-HMPT-by-the-cyclic-urea-DMPU-as-a-cosolvent-for-highly-reactive-nucleophiles-and-bases",{"openalex":2645,"mag":2647,"abstract":2649,"title":2652,"keywords":2655,"doi":2656},{"VOID":2646},"W2070419964",{"VOID":2648},"2070419964",{"EN":2650,"VI":2651},"\u003Cjats:title>Abstract\u003C\u002Fjats:title>\u003Cjats:p>The cyclic urea DMPU (N, N′‐dimethyl‐N, N′‐propylene urea = 1,3‐dimethyl‐2‐oxo‐hexahydropyrimidine) is shown to exhibit the same effects HMPT in oxirane‐opening with Li‐acetylide, in a Wittig olefination, in the double deprotonation of nitroalkane, in the Michael addition of Li‐dithiane to cyclohexenone, and in selective generations of certain enolates (\u003Cjats:italic>Schemes 1–7\u003C\u002Fjats:italic>) DMPU might therefore be as safe substitute of the carcinogenic HMPT as a cosolvent with unique properties in diverse type of reaction.\u003C\u002Fjats:p>","\u003Cjats:title>Tóm tắt\u003C\u002Fjats:title>\u003Cjats:p>Urea vòng DMPU (N, N′‐dimethyl‐N, N′‐propylene urea = 1,3‐dimethyl‐2‐oxo‐hexahydropyrimidine) được chứng minh có tác dụng tương tự như HMPT trong việc mở oxirane với Li-acetylide, trong phản ứng olefination Wittig, trong việc khử proton kép của nitroalkane, trong sự bổ sung Michael của Li-dithiane vào cyclohexenone, và trong việc tạo ra có chọn lọc một số enolate (\u003Cjats:italic>Schemes 1–7\u003C\u002Fjats:italic>). Do đó, DMPU có thể là một chất thay thế an toàn cho HMPT có khả năng gây ung thư, như một dung môi đồng với các đặc tính độc đáo trong nhiều loại phản ứng.\u003C\u002Fjats:p>",{"EN":2653,"VI":2654},"Substitution of HMPT by the cyclic urea DMPU as a cosolvent for highly reactive nucleophiles and bases","Thay thế HMPT bằng urea vòng DMPU làm dung môi cho các nucleophiles và bazơ cực kỳ hoạt động",{"VI":993},{"VOID":2657},"10.1002\u002Fhlca.19820650141",[31],[30],"https:\u002F\u002Fonlinelibrary.wiley.com\u002Fdoi\u002F10.1002\u002Fhlca.19820650141",[2662,2679],{"id":2663,"sortIndex":32,"researcher":28,"roles":2664,"affiliations":2665,"properties":2674,"displayName":2676,"givenName":28,"familyName":28},"7d24ff9a-dc3f-4954-bd30-1d016f7b4803",[],[2666],{"id":2667,"sortIndex":32,"affiliation":2668,"properties":28},"79d9d704-c951-424d-b84d-9fcaac7e38f9",{"id":2667,"createTime":28,"updateTime":28,"relativeEntities":2669,"slug":28,"properties":2670,"entityType":28,"verifyStatus":28,"verifyTime":28,"verifyNote":28,"languages":28,"translateLanguages":28,"viewCount":28,"url":28,"parentIds":2673,"statistic":28},[],{"title":2671},{"EN":2672},"Laboratorium für Organishe Chemie der Eidgenössischen Technischen Hochschule, Eth‐Zentrum, Universitätstrasse 16, CH‐8092 Zürich",[],{"title":2675,"openalex":2677},{"EN":2676},"T. Mukhopadhyay",{"VOID":2678},"A5043602397",{"id":2680,"sortIndex":40,"researcher":28,"roles":2681,"affiliations":2682,"properties":2689,"displayName":1797,"givenName":28,"familyName":28},"9d324e03-67b9-4fe9-ba3f-9bec13db6694",[],[2683],{"id":2667,"sortIndex":32,"affiliation":2684,"properties":28},{"id":2667,"createTime":28,"updateTime":28,"relativeEntities":2685,"slug":28,"properties":2686,"entityType":28,"verifyStatus":28,"verifyTime":28,"verifyNote":28,"languages":28,"translateLanguages":28,"viewCount":28,"url":28,"parentIds":2688,"statistic":28},[],{"title":2687},{"EN":2672},[],{"orcid":2690,"title":2691,"openalex":2692},{"VOID":1795},{"EN":1797},{"VOID":1799},{"url":28,"publisher":2694,"properties":2752},{"id":868,"createTime":869,"updateTime":870,"relativeEntities":2695,"slug":872,"properties":2696,"entityType":25,"verifyStatus":884,"verifyTime":28,"verifyNote":28,"languages":28,"translateLanguages":28,"viewCount":32,"subjectFields":2701,"manageAffiliations":2726,"indexDatabases":2737,"url":970,"thumbnailPath":28,"statistic":28,"gsStatistic":28,"type":28,"analyzePriority":28},[],{"country":2697,"eissn":2698,"issn":2699,"title":2700},{"VOID":875},{"VOID":877},{"VOID":879},{"EN":881},[2702,2706,2710,2714,2718,2722],{"id":887,"createTime":28,"updateTime":28,"relativeEntities":2703,"label":2704,"description":2705,"parentId":28,"standard":28,"scholarHubFieldId":28},[],{"EN":890},{},{"id":911,"createTime":28,"updateTime":28,"relativeEntities":2707,"label":2708,"description":2709,"parentId":28,"standard":28,"scholarHubFieldId":28},[],{"EN":914},{},{"id":893,"createTime":28,"updateTime":28,"relativeEntities":2711,"label":2712,"description":2713,"parentId":28,"standard":28,"scholarHubFieldId":28},[],{"EN":896},{},{"id":899,"createTime":28,"updateTime":28,"relativeEntities":2715,"label":2716,"description":2717,"parentId":28,"standard":28,"scholarHubFieldId":28},[],{"EN":902},{},{"id":905,"createTime":28,"updateTime":28,"relativeEntities":2719,"label":2720,"description":2721,"parentId":28,"standard":28,"scholarHubFieldId":28},[],{"EN":908},{},{"id":917,"createTime":28,"updateTime":28,"relativeEntities":2723,"label":2724,"description":2725,"parentId":28,"standard":28,"scholarHubFieldId":28},[],{"EN":920},{},[2727,2732],{"id":924,"createTime":28,"updateTime":28,"relativeEntities":2728,"slug":28,"properties":2729,"entityType":28,"verifyStatus":28,"verifyTime":28,"verifyNote":28,"languages":28,"translateLanguages":28,"viewCount":28,"url":28,"parentIds":2731,"statistic":28},[],{"title":2730},{"EN":928},[],{"id":931,"createTime":28,"updateTime":28,"relativeEntities":2733,"slug":28,"properties":2734,"entityType":28,"verifyStatus":28,"verifyTime":28,"verifyNote":28,"languages":28,"translateLanguages":28,"viewCount":28,"url":28,"parentIds":2736,"statistic":28},[],{"title":2735},{"EN":935},[],[2738,2745],{"id":939,"indexDatabase":2739,"url":945,"indexYears":946,"academicFieldIds":2744,"indexDatabaseRanking":954},{"id":775,"createTime":28,"updateTime":28,"relativeEntities":2740,"label":2741,"description":2742,"key":781,"publicationTags":2743,"standard":28},[],{"EN":778,"VI":778},{"EN":778,"VI":780},[783],[948,949,950,951,952,953],{"id":956,"indexDatabase":2746,"url":968,"indexYears":28,"academicFieldIds":2751,"indexDatabaseRanking":28},{"id":958,"createTime":28,"updateTime":28,"relativeEntities":2747,"label":2748,"description":2749,"key":965,"publicationTags":2750,"standard":28},[],{"EN":961,"VI":961},{"EN":963,"VI":964},[967,813],[816],{"issue":2753,"pages":2754,"volume":2756},{"VOID":2324},{"VOID":2755},"385-391",{"VOID":2757},"65",309,{"total":2758,"publishYear":2760,"statisticByYear":2761},1982,{"2012":205,"2013":48,"2014":46,"2015":48,"2016":45,"2017":46,"2018":145,"2019":46,"2020":42,"2021":49,"2022":46,"2023":123,"2024":49},"1982-02-03",[954,967],[2765,2768,2771,2774,2777,2780,2783,2786,2789,2792,2795,2798,2801,2804,2807,2810,2813,2816,2819,2822,2825,2828,2831,2834,2837,2840,2843,2846,2849,2852,2855,2858,2861,2864,2867,2870,2873],{"id":28,"text":2766,"url":28,"identifiers":2767},"Normant H., Bull. Soc. Chim. Fr., 1968, 791",{},{"id":28,"text":2769,"url":28,"identifiers":2770},"Fieser M., Reagents for Organic Synthesis, 1",{},{"id":28,"text":2772,"url":28,"identifiers":2773},"Fieser M., 1980, Reagents for Organic Synthesis, 8",{},{"id":28,"text":2775,"url":28,"identifiers":2776},"Fieser M., 1981, Reagents for Organic Synthesis, 9",{},{"id":28,"text":2778,"url":28,"identifiers":2779},"10.1021\u002Fja00509a015",{"doi":2778},{"id":28,"text":2781,"url":28,"identifiers":2782},"Schmutz J. F., Chem. Eng. News 16th Jan., 1978, 39",{},{"id":28,"text":2784,"url":28,"identifiers":2785},"Spencer H., Chem. Ind., 1979, 728",{},{"id":28,"text":2787,"url":28,"identifiers":2788},"10.1002\u002Fange.19630752204",{"doi":2787},{"id":28,"text":2790,"url":28,"identifiers":2791},"10.1002\u002Fanie.196402601",{"doi":2790},{"id":28,"text":2793,"url":28,"identifiers":2794},"10.1002\u002Fange.19790910707",{"doi":2793},{"id":28,"text":2796,"url":28,"identifiers":2797},"10.1002\u002Fanie.197905031",{"doi":2796},{"id":28,"text":2799,"url":28,"identifiers":2800},"10.1021\u002Fjo00326a054",{"doi":2799},{"id":28,"text":2802,"url":28,"identifiers":2803},"10.1080\u002F00304948009355419",{"doi":2802},{"id":28,"text":2805,"url":28,"identifiers":2806},"10.1021\u002Fjm00308a005",{"doi":2805},{"id":28,"text":2808,"url":28,"identifiers":2809},"10.1021\u002Fja01465a025",{"doi":2808},{"id":28,"text":2811,"url":28,"identifiers":2812},"10.1016\u002FS0022-328X(00)85692-2",{"doi":2811},{"id":28,"text":2814,"url":28,"identifiers":2815},"10.1016\u002FS0022-328X(00)87266-6",{"doi":2814},{"id":28,"text":2817,"url":28,"identifiers":2818},"Shaw J. E., Tetrahedron Lett., 1973, 689",{},{"id":28,"text":2820,"url":28,"identifiers":2821},"10.1021\u002Fjo00927a048",{"doi":2820},{"id":28,"text":2823,"url":28,"identifiers":2824},"10.1055\u002Fs-1976-24054",{"doi":2823},{"id":28,"text":2826,"url":28,"identifiers":2827},"10.1080\u002F00304947409355119",{"doi":2826},{"id":28,"text":2829,"url":28,"identifiers":2830},"10.1080\u002F00304947809354996",{"doi":2829},{"id":28,"text":2832,"url":28,"identifiers":2833},"Magnusson G., Tetrahedron Lett., 1977, 2713",{},{"id":28,"text":2835,"url":28,"identifiers":2836},"10.1002\u002Fange.19790910404",{"doi":2835},{"id":28,"text":2838,"url":28,"identifiers":2839},"10.1002\u002Fanie.197902393",{"doi":2838},{"id":28,"text":2841,"url":28,"identifiers":2842},"10.1002\u002Fhlca.19790620722",{"doi":2841},{"id":28,"text":2844,"url":28,"identifiers":2845},"Brown C. A., J. Chem. Soc., Chem. Commun., 1979, 100",{},{"id":28,"text":2847,"url":28,"identifiers":2848},"10.1021\u002Fja00426a033",{"doi":2847},{"id":28,"text":2850,"url":28,"identifiers":2851},"10.1021\u002Fja00531a052",{"doi":2850},{"id":28,"text":2853,"url":28,"identifiers":2854},"10.1002\u002Fange.19810931239",{"doi":2853},{"id":28,"text":2856,"url":28,"identifiers":2857},"10.1002\u002Fanie.198110301",{"doi":2856},{"id":28,"text":2859,"url":28,"identifiers":2860},"R.Naef ETH Zürich1980.",{},{"id":28,"text":2862,"url":28,"identifiers":2863},"D.Seebach R.Henning&T.Mukhopadhyay Chem. Ber. in press",{},{"id":28,"text":2865,"url":28,"identifiers":2866},"10.1002\u002Fcber.19660990417",{"doi":2865},{"id":28,"text":2868,"url":28,"identifiers":2869},"10.1021\u002Fjo00890a018",{"doi":2868},{"id":28,"text":2871,"url":28,"identifiers":2872},"10.1021\u002Fjo01269a123",{"doi":2871},{"id":28,"text":2874,"url":28,"identifiers":2875},"10.1002\u002Fhlca.19770600202",{"doi":2874},{"id":2877,"createTime":2878,"updateTime":2879,"relativeEntities":2880,"slug":2881,"properties":2882,"entityType":996,"verifyStatus":26,"verifyTime":2878,"verifyNote":997,"languages":2896,"translateLanguages":2897,"viewCount":32,"primaryUrl":2898,"fullTextUrl":28,"authors":2899,"publicationType":1019,"publisherRelationship":2951,"citationCount":3017,"citationInfo":3018,"publishDate":3021,"publishYear":3019,"citationAnalyzeStatus":884,"lastCitationAnalyze":28,"indexDatabases":3022,"openAccess":28,"references":3023,"isForceReanalyzing":1189},"23a07b56-8a37-42b7-bc76-c805f291c0cc","2024-09-01T03:44:35.057+00:00","2025-02-25T01:54:33.300+00:00",[],"Improved-Purification-of-C-sub-60-sub-and-Formation-of-%CF%83-and-%CF%80-Homoaromatic-methano-bridged-fullerenes-by-reaction-with-alkyl-diazoacetates",{"openalex":2883,"mag":2885,"abstract":2887,"title":2890,"keywords":2893,"doi":2894},{"VOID":2884},"W2126265750",{"VOID":2886},"2126265750",{"EN":2888,"VI":2889},"\u003Cjats:title>Abstract\u003C\u002Fjats:title>\u003Cjats:p>A rapid and inexpensive method for the large‐scale purification of C\u003Cjats:sub>60\u003C\u002Fjats:sub> is the simple filtration of the toluenesoluble extract of commercial fullerene soot through a short plug of charcoal\u002Fsilica gel with toluene as the eluent. Reactions of C\u003Cjats:sub>60\u003C\u002Fjats:sub> with ethyl and \u003Cjats:italic>tert\u003C\u002Fjats:italic>‐butyl diazoacetates in refluxing toluene lead to the formation of the (alkoxycarbonyl)methylene‐bridged isomers \u003Cjats:bold>1a\u003C\u002Fjats:bold>–\u003Cjats:bold>3a\u003C\u002Fjats:bold> and \u003Cjats:bold>1b\u003C\u002Fjats:bold>–\u003Cjats:bold>3b\u003C\u002Fjats:bold>, respectively, which can be equilibrated, upon further heating, into the single compounds \u003Cjats:bold>1a\u003C\u002Fjats:bold> and \u003Cjats:bold>1b\u003C\u002Fjats:bold>, respectively. Isomers \u003Cjats:bold>1a\u003C\u002Fjats:bold>\u002F\u003Cjats:bold>b\u003C\u002Fjats:bold> possess the methano bridge at the 6–6 ring junction, whereas structures \u003Cjats:bold>2a\u003C\u002Fjats:bold>\u002F\u003Cjats:bold>b\u003C\u002Fjats:bold> and \u003Cjats:bold>3a\u003C\u002Fjats:bold>\u002F\u003Cjats:bold>b\u003C\u002Fjats:bold> are bridged at the 6–5 junction. A dramatic influence of local and π‐ring current anisotropic effects of the fullerene sphere on the NMR chemical shifts of the methine protons in the bridge is observed: the chemical shifts of the protons located over a pentagon ring in \u003Cjats:bold>2a\u003C\u002Fjats:bold>\u002F\u003Cjats:bold>b\u003C\u002Fjats:bold> and over a hexagon ring in \u003Cjats:bold>3a\u003C\u002Fjats:bold>\u002F\u003Cjats:bold>b\u003C\u002Fjats:bold> differ by Δδ = 3.47 and 3.45 ppm, respectively. The analysis of the \u003Cjats:sup>13\u003C\u002Fjats:sup>C‐NMR chemical shifts of the bridgehead C‐atoms and the \u003Cjats:sup>1\u003C\u002Fjats:sup>\u003Cjats:italic>J\u003C\u002Fjats:italic>(C,H) coupling constants for the methano‐bridge atoms reveals conclusively that the 6‐5‐ring‐bridged structures \u003Cjats:bold>2a\u003C\u002Fjats:bold>\u002F\u003Cjats:bold>2b\u003C\u002Fjats:bold> and \u003Cjats:bold>3a\u003C\u002Fjats:bold>\u002F\u003Cjats:bold>3b\u003C\u002Fjats:bold> are π‐homoaromatic (‘open’ transannular bond) and the 6‐6‐ring‐bridged structures \u003Cjats:bold>1a\u003C\u002Fjats:bold>\u002F\u003Cjats:bold>b\u003C\u002Fjats:bold> are π‐homoaromatic (‘closed’ transannular bond). The electronic absorption spectra show that π‐homoconjugation in \u003Cjats:bold>2a\u003C\u002Fjats:bold>\u002F\u003Cjats:bold>b\u003C\u002Fjats:bold> and \u003Cjats:bold>3a\u003C\u002Fjats:bold>\u002F\u003Cjats:bold>b\u003C\u002Fjats:bold> represents a much smaller electronic perturbation of the original C\u003Cjats:sub>60\u003C\u002Fjats:sub> chromophore than σ‐homoconjugation in \u003Cjats:bold>1a\u003C\u002Fjats:bold>\u002F\u003Cjats:bold>b\u003C\u002Fjats:bold>. The results of this study demonstrate an impressive linkage between the chemistry of methano‐bridged annulenes and methano‐bridged fullerenes.\u003C\u002Fjats:p>","Một phương pháp nhanh chóng và chi phí thấp để tinh chế quy mô lớn C\u003Csub>60\u003C\u002Fsub> là lọc đơn giản chiết xuất hòa tan trong toluene của bồ hóng fullerene thương mại qua một cục than\u002Fsilica gel ngắn với toluene là dung môi rửa. Các phản ứng của C\u003Csub>60\u003C\u002Fsub> với ethyl và \u003Ci>tert\u003C\u002Fi>-butyl diazoacetates trong toluene được đun sôi dẫn đến việc hình thành các đồng phân (alkoxycarbonyl)methylene-bridged \u003Cb>1a\u003C\u002Fb>–\u003Cb>3a\u003C\u002Fb> và \u003Cb>1b\u003C\u002Fb>–\u003Cb>3b\u003C\u002Fb>, tương ứng, có thể cân bằng, khi tiếp tục gia nhiệt, thành các hợp chất đơn lẻ \u003Cb>1a\u003C\u002Fb> và \u003Cb>1b\u003C\u002Fb>, tương ứng. Các đồng phân \u003Cb>1a\u003C\u002Fb>\u002F\u003Cb>b\u003C\u002Fb> có cầu methano tại điểm nối vòng 6–6, trong khi các cấu trúc \u003Cb>2a\u003C\u002Fb>\u002F\u003Cb>b\u003C\u002Fb> và \u003Cb>3a\u003C\u002Fb>\u002F\u003Cb>b\u003C\u002Fb> được kết nối tại điểm nối 6–5. Một ảnh hưởng mạnh mẽ của các hiệu ứng độ cao cục bộ và độ cao π‐vòng đối với sự thay đổi hóa học NMR của các proton methine trong cầu được quan sát thấy: các sự thay đổi hóa học của các proton nằm trên vòng ngũ giác trong \u003Cb>2a\u003C\u002Fb>\u002F\u003Cb>b\u003C\u002Fb> và trên vòng lục giác trong \u003Cb>3a\u003C\u002Fb>\u002F\u003Cb>b\u003C\u002Fb> khác nhau với Δδ = 3,47 và 3,45 ppm, tương ứng. Phân tích các sự thay đổi hóa học \u003Csup>13\u003C\u002Fsup>C-NMR của các nguyên tử C đầu cầu và các hằng số liên kết \u003Csup>1\u003C\u002Fsup>\u003Ci>J\u003C\u002Fi>(C,H) cho các nguyên tử cầu methano cho thấy một cách thuyết phục rằng các cấu trúc cầu vòng 6-5 \u003Cb>2a\u003C\u002Fb>\u002F\u003Cb>2b\u003C\u002Fb> và \u003Cb>3a\u003C\u002Fb>\u002F\u003Cb>3b\u003C\u002Fb> là π-homoaromatic (‘liên kết transannular mở’) và các cấu trúc cầu vòng 6-6 \u003Cb>1a\u003C\u002Fb>\u002F\u003Cb>b\u003C\u002Fb> là π-homoaromatic (‘liên kết transannular đóng’). Các phổ hấp thụ điện tử cho thấy π-homoconjugation trong \u003Cb>2a\u003C\u002Fb>\u002F\u003Cb>b\u003C\u002Fb> và \u003Cb>3a\u003C\u002Fb>\u002F\u003Cb>b\u003C\u002Fb> đại diện cho sự rối loạn điện tử nhỏ hơn nhiều của chromophore C\u003Csub>60\u003C\u002Fsub> nguyên gốc so với σ-homoconjugation trong \u003Cb>1a\u003C\u002Fb>\u002F\u003Cb>b\u003C\u002Fb>. Kết quả của nghiên cứu này cho thấy một liên kết ấn tượng giữa hóa học của các annulene cầu methano và các fullerenes cầu methano.",{"EN":2891,"VI":2892},"Improved Purification of C\u003Csub>60\u003C\u002Fsub> and Formation of σ‐ and π‐Homoaromatic methano‐bridged fullerenes by reaction with alkyl diazoacetates","Cải tiến việc tinh chế C\u003Csub>60\u003C\u002Fsub> và hình thành các fullerenes cầu methano σ- và π-homoaromatic thông qua phản ứng với các alkyl diazoacetates",{"VI":993},{"VOID":2895},"10.1002\u002Fhlca.19930760310",[31],[30],"https:\u002F\u002Fonlinelibrary.wiley.com\u002Fdoi\u002F10.1002\u002Fhlca.19930760310",[2900,2919,2934],{"id":2901,"sortIndex":32,"researcher":28,"roles":2902,"affiliations":2903,"properties":2912,"displayName":2916,"givenName":28,"familyName":28},"c7f5b11f-527b-4a71-aec6-8e647e58bf0b",[],[2904],{"id":2905,"sortIndex":32,"affiliation":2906,"properties":28},"1710beac-b8fb-446d-8711-430bd3f2953c",{"id":2905,"createTime":28,"updateTime":28,"relativeEntities":2907,"slug":28,"properties":2908,"entityType":28,"verifyStatus":28,"verifyTime":28,"verifyNote":28,"languages":28,"translateLanguages":28,"viewCount":28,"url":28,"parentIds":2911,"statistic":28},[],{"title":2909},{"EN":2910},"Laboratorium für Organische Chemie, ETH‐Zentrum, Universitätstrasse 16, CH–8092 Zürich",[],{"orcid":2913,"title":2915,"openalex":2917},{"VOID":2914},"https:\u002F\u002Forcid.org\u002F0000-0002-4079-332X",{"EN":2916},"Lyle 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N.Houk I.Chao unpublished results.",{},{"id":28,"text":3234,"url":28,"identifiers":3235},"10.1002\u002F9780470147245.ch1",{"doi":3234},{"id":28,"text":3237,"url":28,"identifiers":3238},"10.1021\u002Fja01081a045",{"doi":3237},{"id":28,"text":3240,"url":28,"identifiers":3241},"10.1016\u002FS0040-4039(01)98370-4",{"doi":3240},{"id":28,"text":3243,"url":28,"identifiers":3244},"10.1016\u002FS0040-4039(00)96970-3",{"doi":3243},{"id":28,"text":3246,"url":28,"identifiers":3247},"Regitz M., 1973, Org. Synth. Coll., 179",{},{"id":28,"text":3249,"url":28,"identifiers":3250},"10.1126\u002Fscience.254.5039.1768",{"doi":3249},{"id":3252,"createTime":3253,"updateTime":3254,"relativeEntities":3255,"slug":3256,"properties":3257,"entityType":996,"verifyStatus":26,"verifyTime":3271,"verifyNote":997,"languages":3272,"translateLanguages":3273,"viewCount":32,"primaryUrl":3274,"fullTextUrl":28,"authors":3275,"publicationType":1019,"publisherRelationship":3326,"citationCount":459,"citationInfo":3391,"publishDate":3394,"publishYear":3392,"citationAnalyzeStatus":884,"lastCitationAnalyze":28,"indexDatabases":3395,"openAccess":28,"references":3396,"isForceReanalyzing":1189},"de507ed6-4b60-4705-b225-29e4d5fc1e93","2024-10-15T12:32:31.996+00:00","2025-02-25T01:55:31.646+00:00",[],"Carbocyclische-Verbindungen-aus-Monosacchariden-I-Umsetzungen-in-der-glucosereihe",{"openalex":3258,"mag":3260,"abstract":3262,"title":3265,"keywords":3268,"doi":3269},{"VOID":3259},"W2000644628",{"VOID":3261},"2000644628",{"EN":3263,"VI":3264},"\u003Cjats:p>\u003Cjats:bold>Carbocyclic Compounds from Monosaccharides. 1. Transformations in the Glucose Series\u003C\u002Fjats:bold>\u003C\u002Fjats:p>\u003Cjats:p>A method for the preparation of pentasubstituted cyclopentanes from monosaccharides is presented, involving two crucial steps, viz. the reductive fragmentation of 5‐bromo‐5‐deoxyglucosides (such as \u003Cjats:bold>10, 17\u003C\u002Fjats:bold> and \u003Cjats:bold>23\u003C\u002Fjats:bold>, see \u003Cjats:italic>Scheme 3\u003C\u002Fjats:italic>) with Zn or butyl lithium yielding 5,6‐dideoxy‐hex‐5‐enoses (such as \u003Cjats:bold>11\u003C\u002Fjats:bold> and \u003Cjats:bold>24\u003C\u002Fjats:bold>, see \u003Cjats:italic>Schemes 3\u003C\u002Fjats:italic> and \u003Cjats:italic>4\u003C\u002Fjats:italic>), and the subsequent cyclization of these hexenoses with \u003Cjats:italic>N\u003C\u002Fjats:italic>‐methyl‐ or \u003Cjats:italic>N\u003C\u002Fjats:italic>‐(alkoxyalkyl)hydroxylamines (\u003Cjats:italic>via\u003C\u002Fjats:italic> the corresponding nitrones) to form cyclopentano‐isoxazolidines (see \u003Cjats:italic>Scheme 2\u003C\u002Fjats:italic>). Thus, the glucosides \u003Cjats:bold>17\u003C\u002Fjats:bold> and \u003Cjats:bold>23\u003C\u002Fjats:bold> were converted diastereoselectively and in good yields into the cyclopentano‐isoxazolidines \u003Cjats:bold>27\u003C\u002Fjats:bold> and \u003Cjats:bold>45\u003C\u002Fjats:bold> (\u003Cjats:italic>Schemes 5\u003C\u002Fjats:italic> and \u003Cjats:italic>7\u003C\u002Fjats:italic>), which were characterized by their transformation into various derivatives. \u003Cjats:bold>27\u003C\u002Fjats:bold> and \u003Cjats:bold>45\u003C\u002Fjats:bold> were correlated through the common derivative \u003Cjats:bold>62\u003C\u002Fjats:bold>. The configuration of the cyclization products were established by pyrolysis of the \u003Cjats:italic>N\u003C\u002Fjats:italic>‐oxide \u003Cjats:bold>65\u003C\u002Fjats:bold> to the enol ether \u003Cjats:bold>67\u003C\u002Fjats:bold> (\u003Cjats:italic>Scheme 10\u003C\u002Fjats:italic>).\u003C\u002Fjats:p>","\u003Cjats:p>\u003Cjats:bold>Các hợp chất cacbocylic từ monosaccharide. 1. Chuyển đổi trong chuỗi glucose\u003C\u002Fjats:bold>\u003C\u002Fjats:p>\u003Cjats:p>Chúng tôi trình bày một phương pháp chuẩn bị cyclopentane pentasubstituted từ monosaccharide, bao gồm hai bước quan trọng, cụ thể là phân mảnh khử của 5‐bromo‐5‐deoxyglucosides (chẳng hạn như \u003Cjats:bold>10, 17\u003C\u002Fjats:bold> và \u003Cjats:bold>23\u003C\u002Fjats:bold>, xem \u003Cjats:italic>Hình 3\u003C\u002Fjats:italic>) bằng Zn hoặc butyl lithium, tạo ra 5,6‐dideoxy‐hex‐5‐enoses (như \u003Cjats:bold>11\u003C\u002Fjats:bold> và \u003Cjats:bold>24\u003C\u002Fjats:bold>, xem \u003Cjats:italic>Hình 3\u003C\u002Fjats:italic> và \u003Cjats:italic>4\u003C\u002Fjats:italic>), và sau đó là cyclization của các hexenose này với \u003Cjats:italic>N\u003C\u002Fjats:italic>‐methyl‐ hoặc \u003Cjats:italic>N\u003C\u002Fjats:italic>‐(alkoxyalkyl)hydroxylamines (\u003Cjats:italic>qua\u003C\u002Fjats:italic> các nitron tương ứng) để tạo thành cyclopentano‐isoxazolidines (xem \u003Cjats:italic>Hình 2\u003C\u002Fjats:italic>). Như vậy, các glucoside \u003Cjats:bold>17\u003C\u002Fjats:bold> và \u003Cjats:bold>23\u003C\u002Fjats:bold> đã được chuyển đổi chọn lọc diastereo và với năng suất tốt thành các cyclopentano‐isoxazolidines \u003Cjats:bold>27\u003C\u002Fjats:bold> và \u003Cjats:bold>45\u003C\u002Fjats:bold> (\u003Cjats:italic>Hình 5\u003C\u002Fjats:italic> và \u003Cjats:italic>7\u003C\u002Fjats:italic>), mà đã được phân tích đặc trưng qua việc chuyển đổi thành các dẫn xuất khác nhau. \u003Cjats:bold>27\u003C\u002Fjats:bold> và \u003Cjats:bold>45\u003C\u002Fjats:bold> đã được liên quan thông qua dẫn xuất chung \u003Cjats:bold>62\u003C\u002Fjats:bold>. Cấu hình của các sản phẩm cyclization đã được xác lập thông qua quá trình nhiệt phân \u003Cjats:italic>N\u003C\u002Fjats:italic>-oxide \u003Cjats:bold>65\u003C\u002Fjats:bold> thành enol ether \u003Cjats:bold>67\u003C\u002Fjats:bold> (\u003Cjats:italic>Hình 10\u003C\u002Fjats:italic>).\u003C\u002Fjats:p>",{"EN":3266,"VI":3267},"Carbocyclische Verbindungen aus Monosacchariden. I. Umsetzungen in der glucosereihe","Các hợp chất cacbocylic từ monosaccharide. 1. Chuyển đổi trong chuỗi glucose",{"VI":993},{"VOID":3270},"10.1002\u002Fhlca.19790620629","2024-10-15T12:32:31.995+00:00",[31],[30],"https:\u002F\u002Fonlinelibrary.wiley.com\u002Fdoi\u002F10.1002\u002Fhlca.19790620629",[3276,3303],{"id":3277,"sortIndex":32,"researcher":28,"roles":3278,"affiliations":3279,"properties":3296,"displayName":3300,"givenName":28,"familyName":28},"05305074-2bf3-4f75-9688-d1a8ea5fbef8",[],[3280,3288],{"id":3281,"sortIndex":32,"affiliation":3282,"properties":28},"bfd83a5b-ba9e-43c5-ac2e-4ab4b827801e",{"id":3281,"createTime":28,"updateTime":28,"relativeEntities":3283,"slug":28,"properties":3284,"entityType":28,"verifyStatus":28,"verifyTime":28,"verifyNote":28,"languages":28,"translateLanguages":28,"viewCount":28,"url":28,"parentIds":3287,"statistic":28},[],{"title":3285},{"EN":3286},"Institut für Organische Chemie der Universität, Pérolles, CH-1705 Freiburg i. 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A., 1977, Topics in Antibiotic Chemistry, 1ff",{},{"id":28,"text":3407,"url":28,"identifiers":3408},"10.1021\u002Fcr60236a003",{"doi":3407},{"id":28,"text":3410,"url":28,"identifiers":3411},"10.7164\u002Fantibiotics.24.59",{"doi":3410},{"id":28,"text":3413,"url":28,"identifiers":3414},"Kishi T., Chem. Commun., 1967, 852",{},{"id":28,"text":3416,"url":28,"identifiers":3417},"10.1002\u002Fjlac.19324960105",{"doi":3416},{"id":28,"text":3419,"url":28,"identifiers":3420},"F.Stadler Diss. Wien1962.",{},{"id":28,"text":3422,"url":28,"identifiers":3423},"Angyal S. J., J. chem. Soc., 1958, 375",{},{"id":28,"text":3425,"url":28,"identifiers":3426},"10.1021\u002Fja01184a053",{"doi":3425},{"id":28,"text":3428,"url":28,"identifiers":3429},"10.1002\u002Fange.19640760204",{"doi":3428},{"id":28,"text":3431,"url":28,"identifiers":3432},"10.1016\u002FS0008-6215(00)85876-0",{"doi":3431},{"id":28,"text":3434,"url":28,"identifiers":3435},"10.1071\u002FCH9651973",{"doi":3434},{"id":28,"text":3437,"url":28,"identifiers":3438},"10.1021\u002Fjo00961a007",{"doi":3437},{"id":28,"text":3440,"url":28,"identifiers":3441},"10.1021\u002Fja01160a084",{"doi":3440},{"id":28,"text":3443,"url":28,"identifiers":3444},"10.1016\u002FS0008-6215(00)83175-4",{"doi":3443},{"id":28,"text":3446,"url":28,"identifiers":3447},"10.1351\u002Fpac197850111363",{"doi":3446},{"id":28,"text":3449,"url":28,"identifiers":3450},"10.1002\u002Fange.19710830907",{"doi":3449},{"id":28,"text":3452,"url":28,"identifiers":3453},"10.1021\u002Fja00422a053",{"doi":3452},{"id":28,"text":3455,"url":28,"identifiers":3456},"10.1021\u002Fja00446a055",{"doi":3455},{"id":28,"text":3458,"url":28,"identifiers":3459},"10.1021\u002Fja00494a045",{"doi":3458},{"id":28,"text":3461,"url":28,"identifiers":3462},"10.1021\u002Fjo00956a036",{"doi":3461},{"id":28,"text":3464,"url":28,"identifiers":3465},"10.7164\u002Fantibiotics.31.1007",{"doi":3464},{"id":28,"text":3467,"url":28,"identifiers":3468},"10.1002\u002Fcber.19590920120",{"doi":3467},{"id":28,"text":3470,"url":28,"identifiers":3471},"10.1002\u002Fhlca.19630460410",{"doi":3470},{"id":28,"text":3473,"url":28,"identifiers":3474},"F. G.Cocu Diss. No 1577 Genf1972.",{},{"id":28,"text":3476,"url":28,"identifiers":3477},"10.1002\u002Fange.19750871706",{"doi":3476},{"id":28,"text":3479,"url":28,"identifiers":3480},"10.1002\u002Fange.19750871707",{"doi":3479},{"id":28,"text":3482,"url":28,"identifiers":3483},"10.1002\u002Fcber.19570901114",{"doi":3482},{"id":28,"text":3485,"url":28,"identifiers":3486},"Yur'ev Y. K., 1961, Chem. Abstr., 55, 24573",{},{"id":28,"text":3488,"url":28,"identifiers":3489},"10.1021\u002Fjo00941a023",{"doi":3488},{"id":28,"text":3491,"url":28,"identifiers":3492},"10.1021\u002Fjo01271a049",{"doi":3491},{"id":28,"text":3494,"url":28,"identifiers":3495},"10.1002\u002Fcber.19640970218",{"doi":3494},{"id":28,"text":3497,"url":28,"identifiers":3498},"10.1002\u002Fcber.19671000813",{"doi":3497},{"id":28,"text":3500,"url":28,"identifiers":3501},"10.1021\u002Fja00865a034",{"doi":3500},{"id":28,"text":3503,"url":28,"identifiers":3504},"10.1021\u002Fja00897a046",{"doi":3503},{"id":28,"text":3506,"url":28,"identifiers":3507},"McCrindle R., J. chem. Soc., 1960, 1560",{},{"id":28,"text":3509,"url":28,"identifiers":3510},"10.1139\u002Fv76-123",{"doi":3509},{"id":28,"text":3512,"url":28,"identifiers":3513},"10.1021\u002Fja01039a042",{"doi":3512},{"id":28,"text":3515,"url":28,"identifiers":3516},"M.Schlosserin Houben‐Weyl «Methoden der org. Chemie» Bd. 5\u002F1b.",{},{"id":28,"text":3518,"url":28,"identifiers":3519},"10.1002\u002Fange.19690811502",{"doi":3518},{"id":28,"text":3521,"url":28,"identifiers":3522},"10.1351\u002Fpac197749081105",{"doi":3521},{"id":28,"text":3524,"url":28,"identifiers":3525},"10.3891\u002Facta.chem.scand.20-2423",{"doi":3524},{"id":28,"text":3527,"url":28,"identifiers":3528},"10.1139\u002Fv76-243",{"doi":3527},{"id":28,"text":3530,"url":28,"identifiers":3531},"10.1016\u002FS0008-6215(00)80000-2",{"doi":3530},{"id":28,"text":3533,"url":28,"identifiers":3534},"10.1248\u002Fcpb.26.484",{"doi":3533},{"id":28,"text":3536,"url":28,"identifiers":3537},"10.1002\u002Fange.19760880502",{"doi":3536},{"id":28,"text":3539,"url":28,"identifiers":3540},"Oppolzer W., 1977, Angew. Chemie, 89, 10, 10.1002\u002Fange.19770890105",{"doi":3541},"10.1002\u002Fange.19770890105",{"id":28,"text":3543,"url":28,"identifiers":3544},"10.1021\u002Fjo01256a059",{"doi":3543},{"id":28,"text":3546,"url":28,"identifiers":3547},"10.1021\u002Fjo01038a046",{"doi":3546},{"id":28,"text":3549,"url":28,"identifiers":3550},"10.1002\u002Fcber.19120450168",{"doi":3549},{"id":28,"text":3552,"url":28,"identifiers":3553},"10.1021\u002Fja00813a021",{"doi":3552},{"id":28,"text":3555,"url":28,"identifiers":3556},"Rieke R. D., Chem. Commun., 1973, 269",{},{"id":28,"text":3558,"url":28,"identifiers":3559},"10.1002\u002Fjlac.19244400102",{"doi":3558},{"id":28,"text":3561,"url":28,"identifiers":3562},"10.1016\u002FS0008-6215(00)83718-0",{"doi":3561},{"id":28,"text":3564,"url":28,"identifiers":3565},"10.1139\u002Fv69-194",{"doi":3564},{"id":28,"text":3567,"url":28,"identifiers":3568},"Schroeder L., J. chem. Soc. 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