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Chem.25, 623 (1971)\nNakajima A., Ohya-Nishiguchi H., Deguchi Y.: Bull. Chem. Soc. Jpn.45, 713 (1972)\nParmon V.N., Kokorin A.I., Zhidomirov G.M., Zamaraev K.I.: Mol. Phys.26, 1565 (1973)\nBuchachenko A.L., Vasserman A.M.: Stable Radicals. Moscow: Khimia 1973.\nBerliner L.J. (ed.): Spin Labeling: Theory and Applications. New York: Academic Press 1976.\nParmon V.N., Kokorin A.I., Zhidomirov G.M.: Russ. J. Struct. Chem.18, 104 (1977)\nParmon V.N., Kokorin A.I., Zhidomirov G.M.: Stable Biradicals. Moscow: Nauka 1980.\nParmon V.N., Zhidomirov G.M.: Mol. Phys.27, 367 (1974)\nParmon V.N., Kokorin A.I., Zamaraev K.I.: Izv. Akad. Nauk SSSR Ser. Khim.1976, 1776.\nVolodarsky L.B. (ed.): Imidazoline Nitroxides: Synthesis, Properties, Applications, vols. 1, 2. Boca Raton, Fla.: CRC Press 1988.\nHideg K., Hankovsky O.H. in: Spin Labeling: Theory and Applications. Biological Magnetic Resonance (Berliner L.J., Reuben J., eds.), vol. 8. New York: Plenum 1989.\nGrampp G., Rasmussen K., Kokorin A.I.: Appl. Magn. Reson.26, 245–252 (2004)\nKokorin A.I., Parmon V.N., Suskina V.I., Ivanov V.P., Rozantsev E.G., Zamaraev K.I.: Russ. J. Phys. Chem.48, 548 (1974)\nShapiro A.B., Goldfield M.G., Rozantsev E.G.: Tetrahedron Lett.24, 2183 (1973)\nPavlikov V.V., Shapiro A.B., Rozantsev E.G.: Izv. Akad. Nauk SSSR Ser. Khim.1980, 128.\nKokorin A.I., Pavlikov V.V., Shapiro A.B.: Proc. Acad. Sci. USSR Sect. Phys. Chem.253, 525 (1980)\nShapiro A.B., Novozhilova G.V., Rozantsev E.G.: Izv. Akad. Nauk SSSR Ser. Khim.1976, 452; Shapiro A.B., Novozhilova G.V., Dombrovsky V.A., Volodarsky L.B., Rozantsev E.G.: ibid. Izv. Akad. Nauk SSSR Ser. Khim.1976, 2124.\nKokorin A.I., Novozhilova G.V., Shapiro A.B.: Izv. Akad. Nauk SSSR Ser. Khim.1981, 286.\nGrigor’ev I.A., Dikanov S.A., Shchukin G.I., Volodarsky L.B., Tsvetkov Yu.D.: Zh. Strukt. Khim.23, 565 (1982)\nGrigor’ev I.A., Dikanov S.A., Gogolev A.Z., Volodarsky L.B.: Izv. Sib. Otd. Akad. Nauk SSSR Ser. Khim. Nauk1988, 95.\nRiddick J.A., Bunger W.B., Sakano K.T. in: Techniques of Chemistry, vol. II: Organic Solvents, Physical Chemistry and Methods of Purification. New York: Wiley 1986.\nMolin Yu.N., Salikhov K.M., Zamaraev K.I.: Spin Exchange. Berlin: Springer 1980.\nKokorin A.I., Parmon V.N., Shubin A.A.: Atlas of Anisotropic EPR Spectra of Nitroxide Biradicals. Moscow: Nauka 1984.\nAlster E., Silver B.L.: Mol. Phys.58, 977 (1986)\nLuckhurst G.R., Pedulli G.F.: Mol. Phys.18, 425 (1970)\nMetzner E.K., Libertini L.J., Calvin M.: J. Am. Chem. Soc.96, 6515 (1974)\nRozantsev E.G., Pavelko G.F., Buchachenko A.L., Neiman M.B.: Izv. Akad. Nauk SSSR Ser. Khim.1967, 2306.\nSysoeva I.A., Buchachenko A.L., Vasserman A.M., Vasileiskaya I.S., Muslin D.V.: Dokl. Akad. Nauk SSSR192, 1291 (1970)\nEaton G.R., Eaton S.S.: Biol. Magn. Reson.8, 339 (1989)\nRozantsev E.G., Ozhogina O.A., Rakhimov R.R., Prokof’ev A.I.: Mol. Phys.76, 1009 (1992)\nGrigor’ev I.A., Dikanov S.A. in: Imidazoline Nitroxides: Synthesis, Properties, Applications (Volodarsky L.B., ed.), vol. 1, pp. 77–150. Boca Raton, Fla.: CRC Press 1988.\nGrigor’ev I.A., Gogolev A.Z., Sagdeev R.Z., Volodarskii L.B.: Chem. Phys. Lett.100, 19 (1983)\nGrigor’ev I.A., Gogolev A.Z., Kirilyuk I.A., Volodarskii L.B., Sagdeev R.Z.: Izv. Akad. Nauk SSSR Ser. Khim.1988, 1029.\nGrigor’ev I.A., Volodarskii L.B., Gogolev A.Z., Sagdeev R.Z.: Chem. Phys. Lett.122, 46 (1985)\nCarrington A., McLachlan A.D.: Introduction to Magnetic Resonance with Applications to Chemistry and Chemical Physics. New York: Harper & Row 1967.\nKreilich R.W. in: NMR of Paramagnetic Molecules: Principles and Applications (La Mar G.N., Horrocks W., De W., Ir., Holm R.H., eds.). New York: Academic Press 1973.\nGulin V.I., Dikanov S.A., Martin V.V., Grigor’ev I.A., Volodarsky L.B.: Izv. Sib. Otd. Akad. Nauk SSSR Ser. Khim. Nauk1988, 99.\nGiroud A.M., Rassat A.: Bull. Soc. Chim. Fr.1979, 48.\nParmon V.N., Kokorin A.I., Zhidomirov G.M., Zamaraev K.I.: Mol. Phys.30, 695 (1975)\nDikanov S.A., Shchukin G.I., Grigor’ev I.A., Rukin S.I., Volodarsky L.B.: Izv. Akad. Nauk SSSR Ser. Khim.1985, 565.\nSankarapandi S., Rifkind J.M., Manoharan P.T.: Proc. Indian Acad. Sci. (Chem. Sci.)106, 1329 (1994)\nGrampp G., Landgraf S., Grigor’ev I.A., Shapiro A.B., Kokorin A.I.: Appl. Magn. Reson.19, 187 (2000)\nShastnev P.V., Salikhov K.M.: Teor. Eksp. Khim.9, 291 (1973)\nNedlin G.M.: Fiz. Tverd. Tela (Leningrad)15, 3048 (1973)\nBriere R., Lemaire H., Rassat A.: Bull Soc. Chim. Fr.1965, 3273.\nGriffith O.H., Dehlingert P.J., Van S.P.: J. Membr. Biol.15, 159 (1974)\nHayat H., Silver B.L.: J. Phys. Chem.77, 72 (1973)\nShapiro A.B., Parmon V.N., Pavlikov V.V., Rubtsov V.I., Rozantsev E.G.: Izv. Akad. Nauk SSSR Ser. Khim.1980, 449.\nKosower E.M.: J. Am. Chem. Soc.80, 3253 (1958); Kosower E.M.: An Introduction to Physical Organic Chemistry, part 2. New York: Wiley 1968.\nMilaeva E.R., Rubezhov A.Z., Prokof’ev A.I., Okhlobystin O.Yu.: Usp. Khim.51, 1638 (1982)\nLarionov S.V.: Zh. Strukt. Khim.23, 125 (1982)\nLarionov S.V. in: Imidazoline Nitroxides, vol. II, Applications (Volodarsky L.B., ed.), pp. 81–113. Boca Raton, Fla.: CRC Press 1988.\nMore K.M., Eaton G.R., Eaton S.S., Hankovszky O.H., Hideg K.: Inorg. Chem.28, 1734 (1989)\nBencini A., Gatteschi D.: EPR of Exchange Coupled Systems. Berlin: Springer 1990.\nOvcharenko V.I., Sagdeev R.Z.: Usp. Khim.68, 381 (1999)\nVanifatova N.G., Evstiferov M.V., Martin V.V., Petrukhin O.M., Volodarskii L.B., Zolotov Yu. A.: Zh. Anal. Khim.43, 435 (1988)\nNagy V.Yu., Petrukhin O.M., Zolotov Yu.A.: CRC Crit. Rev. Anal. Chem.17, 265 (1987); Nagy V.Yu. in: Imidazoline Nitroxides, vol. II, Applications (Volodarsky L.B., ed.), pp. 115–155. Boca Raton, Fla.: CRC Press 1988.\nVolodarskii L.B., Reznikov V.A., Ovcharenko V.I.: Synthetic Chemistry of Stable Nitroxides. 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Chekmenev, B.M. Goodson, Angew. Chem. 53, 7495–7498 (2014)\nA.S. Kiryutin, A.N. Pravdivtsev, K.L. Ivanov, Y.A. Grishin, H.M. Vieth, A.V. Yurkovskaya, J. Magn. Reson. 263, 79–91 (2016)\nR. Savka, H. Plenio, Dalton T 44, 891–893 (2015)",{"EN":684},"A number of Ir–N-heterocyclic carbene (Ir–NHC) complexes with asymmetric N-heterocyclic carbene (NHC) ligands have been prepared and examined for signal amplification by reversible exchange (SABRE). Pyridine was chosen as model compound for hyperpolarization experiments. This substrate was examined in a solvent mixture using several Ir–NHC complexes, which differ in their NHC ligands. The SABRE polarization was created at 6 mT and the 1H nuclear magnetic resonance signals were detected at 7 T. We show that asymmetric NHC ligands, because of their favorable chemistry, can adapt the SABRE active complexes to different chemical scenarios.",{"EN":686},"Substituent Influences on the NMR Signal Amplification of Ir Complexes with Heterocyclic Carbene Ligands",{"VOID":688},"10.1007\u002Fs00723-019-01115-x","https:\u002F\u002Flink.springer.com\u002Farticle\u002F10.1007\u002Fs00723-019-01115-x",[691,706,721,737,754,766,778,790,803,819,831],{"id":692,"sortIndex":379,"researcher":20,"roles":693,"affiliations":694,"properties":703},"b314d7a1-18dd-4468-be97-0a633f60845f",[227],[695],{"id":20,"sortIndex":21,"affiliation":696,"properties":20},{"id":697,"createTime":698,"updateTime":698,"relativeEntities":699,"slug":20,"properties":700,"entityType":41,"verifyStatus":19,"verifyTime":20,"verifyNote":20,"syncStatus":19,"languages":20,"translateLanguages":20,"viewCount":21},"a0864fc8-47b5-4401-976a-e6818a3885d5","2024-01-05T11:43:17.350+00:00",[],{"title":701},{"VI":702},"Medical Faculty, 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Phys. 111, 2873–2881 (2013)\nE. Bordignon, H. Brutlach, L. Urban, K. Hideg, A. Savitsky, A. Schnegg, P. Gast, M. Engelhard, E.J.J. Groenen, K. Möbius, H.J. Steinhoff, Appl. Magn. Reson. 37, 391–403 (2010)\nE. Bordignon, A.I. Nalepa, A. Savitsky, L. Braun, G. Jeschke, J. Phys. Chem. B. 119, 13797–13806 (2015)\nA. Nalepa, K. Möbius, M. Plato, W. Lubitz, A. Savitsky, Appl. Magn. Reson. 50, 1–16 (2019)\nT.I. Smirnova, T.G. Chadwick, M.A. Voinov, O. Poluektov, J. van Tol, A. Ozarowski, G. Schaaf, M.M. Ryan, V.A. Bankaitis, Biophys. J. 92, 3686–3695 (2007)\nP. Gast, R.T.L. Herbonnet, J. Klare, A. Nalepa, C. Rickert, D. Stellinga, L. Urban, K. Möbius, A. Savitsky, H.J. Steinhoff, E.J.J. Groenen, Phys. Chem. Chem. Phys. 16, 15910–15916 (2014)\nR. Owenius, M. Engström, M. Lindgren, M. Huber, J. Phys. Chem. A. 105, 10967–10977 (2001)\nZ. Rinkevicius, N.A. Murugan, J. Kongsted, K. Aidas, A.H. Steindal, H. Agren, J. Phys. Chem. B. 115, 4350–4358 (2011)\nZ. Rinkevicius, L. Telyatnyk, O. 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Orlando, Phys. Chem. Chem. Phys. 23, 4480–4485 (2021)",{"EN":889},"The hydrogen bond plays a key role in weak directional intermolecular interactions. It is operative in determining molecular conformation and aggregation, and controls the function of many chemical systems, ranging from inorganic, organic to biological molecules. Although an enormous amount of spectroscopic information has been collected about hydrogen-bond formation between molecules with closed-shell electronic configuration, the details of such interactions between open-shell radicals and closed-shell molecules are still rare. Here we report on an investigation of hydrogen-bonded complexes between pyrroline-type as well as piperidine-type neutral nitroxide radicals and an alcohol, i.e., 2-propanol. These nitroxide radicals are commonly used as EPR spin labels and probes. To obtain information on the geometry of the complexes and their electronic structure, multi-resonance EPR techniques at various microwave frequencies (X-, Q-, W-band, 244 GHz) have been employed in conjunction with DFT calculations. The planar five-membered ring system of the pyrroline-type nitroxide radical was found to form exclusively well-defined in-plane σ-type hydrogen-bonded complexes with one 2-propanol molecule in the first solvation shell in frozen solution. The measured hyperfine parameters of the hydrogen-bridge proton and the internal magnetic parameters describing the electron Zeeman and the electron-nuclear hyperfine and nuclear quadrupole interactions are in good agreement with values predicted by state-of-the-art DFT calculations. In contrast, multi-resonance EPR on the non-planar six-membered ring system of the piperidine-type nitroxide radical (TEMPOL) reveals a more complex situation, i.e., a mixture of a σ-type with, presumably, an out-of-plane π-type complex, both present in comparable fraction in frozen solution. For TEMPOL, the DFT calculations failed to predict magnetic interaction parameters that are in good agreement with experiment, apparently due to the considerable flexibility of the nitroxide and hydrogen-bonded complex. The detailed information about nitroxide\u002Fsolvent complexes is of particular importance for Dynamic Nuclear Polarization (DNP) and site-directed spin-labeling EPR studies that employ nitroxides as polarizing agents or spin labels, respectively.",{"EN":891},"Hydrogen-Bonded Complexes of Neutral Nitroxide Radicals with 2-Propanol Studied by Multifrequency EPR\u002FENDOR",{"VOID":893},"10.1007\u002Fs00723-021-01442-y","https:\u002F\u002Flink.springer.com\u002Farticle\u002F10.1007\u002Fs00723-021-01442-y",[896,911,926,938,953,968],{"id":897,"sortIndex":114,"researcher":20,"roles":898,"affiliations":899,"properties":908},"29f953af-aab8-42ca-bdd5-98631ba7f9fd",[227],[900],{"id":20,"sortIndex":21,"affiliation":901,"properties":20},{"id":902,"createTime":903,"updateTime":903,"relativeEntities":904,"slug":20,"properties":905,"entityType":41,"verifyStatus":19,"verifyTime":20,"verifyNote":20,"syncStatus":19,"languages":20,"translateLanguages":20,"viewCount":21},"f32a2432-5326-472e-9f1a-f4db1154d740","2024-01-28T21:15:22.172+00:00",[],{"title":906},{"VI":907},"Max-Planck-Institut für Chemische Energiekonversion, Mülheim (Ruhr), Germany",{"title":909},{"VI":910},"Wolfgang Lubitz",{"id":912,"sortIndex":21,"researcher":20,"roles":913,"affiliations":914,"properties":923},"dd35720b-5178-493e-9925-5d24091600c6",[227],[915],{"id":20,"sortIndex":21,"affiliation":916,"properties":20},{"id":917,"createTime":918,"updateTime":918,"relativeEntities":919,"slug":20,"properties":920,"entityType":41,"verifyStatus":19,"verifyTime":20,"verifyNote":20,"syncStatus":19,"languages":20,"translateLanguages":20,"viewCount":21},"7d07433d-98b7-41a3-8e93-23e3296da9c2","2024-01-17T05:57:04.413+00:00",[],{"title":921},{"VI":922},"Faculty of Physics, Technical University Dortmund, Dortmund, Germany",{"title":924},{"VI":925},"Anton Savitsky",{"id":927,"sortIndex":180,"researcher":20,"roles":928,"affiliations":929,"properties":935},"9b78ca2b-a669-4866-a778-85ed1585327c",[227],[930],{"id":20,"sortIndex":21,"affiliation":931,"properties":20},{"id":902,"createTime":903,"updateTime":903,"relativeEntities":932,"slug":20,"properties":933,"entityType":41,"verifyStatus":19,"verifyTime":20,"verifyNote":20,"syncStatus":19,"languages":20,"translateLanguages":20,"viewCount":21},[],{"title":934},{"VI":907},{"title":936},{"VI":937},"Anna Nalepa",{"id":939,"sortIndex":327,"researcher":20,"roles":940,"affiliations":941,"properties":950},"04241514-651c-4678-a9b5-9c800cee6827",[227],[942],{"id":20,"sortIndex":21,"affiliation":943,"properties":20},{"id":944,"createTime":945,"updateTime":945,"relativeEntities":946,"slug":20,"properties":947,"entityType":41,"verifyStatus":19,"verifyTime":20,"verifyNote":20,"syncStatus":19,"languages":20,"translateLanguages":20,"viewCount":21},"5b605a61-e4ff-48ba-b99a-3852fe20e0a1","2024-01-28T02:11:23.257+00:00",[],{"title":948},{"VI":949},"High Performance Computing Center Stuttgart (HLRS), Stuttgart, Germany",{"title":951},{"VI":952},"Taras 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J.F., Swartz H.M., Pals M.: J. Cell. Physiol.140, 505–511 (1989)\nHu H., Sosnovsky G., Swartz H.M.: Biochim. Biophys. Acta112, 161–166 (1992)\nGlockner J.F., Norby S.W., Swartz H.M.: Magn. Reson. Med.29, 12–18 (1992)\nKuppusamy P., Shankar R.A., Zweier J.L.: Phys. Med. Biol.43, 1837–1844 (1998)\nBaker J.E., Froncisz W., Kalyanaraman B.: Free Radic. Biol. Med.22, 109–115 (1997)\nInoue M., Utsumi H., Kirino Y.: Chem. Pharm. Bull. (Tokyo)42, 2346–2348 (1994)\nGallez B., Mäder K., Swartz H.M.: Magn. Reson. Med.36, 694–697 (1996)\nLai C.S., Hopwood L.E., Swartz H.M.: Exp. Cell Res.130, 437–442 (1980)\nEdgcomb M.R., Sirimanne S., Wilkinson B.J., Drouin P., Morse R.D.: Biochim. Biophys. Acta1463, 31–42 (2000)\nZhang R., Goldstein S., Samuni A.: Free Radic. Biol. Med26, 1245–1252 (1999)\nSpooner P.J.R., Veenhoff L.M., Watts A., Poolman B.: Biochemistry38, 9634–9639 (1999)\nSwartz H.M., Chen K., Hu H.P., Hideg, K.: Magn. Reson. Med.22, 372–377 (1991)\nSano H., Naruse M., Matsumoto K., Oi T., Utsumi H.: Free Radic. Biol. Med.28, 959–969 (2000)\nMäder K., Bacic G., Domb A., Elmalak O., Langer R., Swartz H.M.: J. Pharm. Sci.86, 126–134 (1997)\nOffer T., Mohsen M., Samuni A.: Free Radic. Biol. Med.25, 832–838 (1998)\nKrishna M.C., DeGraff W., Hankovszky O.H., Sar C.P., Kalai T., Jeko J., Russo A., Mitchell J.B., Hideg K.: J. Med. Chem.41, 3477–3492 (1998)\nShankar R.A., Hideg K., Zweier J.L., Kuppusamy P.: J. Pharmacol. Exp. Ther.292, 838–845 (2000)\nHahn S.M., Krishna M.C., DeLuc A.M., Coffin D., Mitchell J.B.: Free Radic Biol. Med.28, 953–958 (2000)\nDikalov S., Skatchkov M., Fink B., Bassenge E.: Nitric Oxide1, 423–431 (1997)\nDikalov S., Skatchkov M., Bassenge E.: Biochem. Biophys. Res. Commun.231, 701–704 (1997)\nMiura Y., Utsumi H., Kashiwagi M., Hamada A.: J. Biochem. (Tokyo)108, 516–518 (1990)\nLai C.S., Hopwood L.E., Hyde J.S., Lukiewicz S.: Proc. Natl. Acad. Sci. USA79, 1166–1170 (1982)\nSwartz H.: Adv. Exp. Med. Biol.345, 799–806 (1994)\nJames P.E., Grinberg O.Y., Michaels G., Swartz H.M.: J. Cell. Physiol.163, 241–247 (1995)\nKocherginsky N., Swartz H.M.: Nitroxide Spin Labels: Reactions in Biology and Chemistry. Boca Raton: CRC Press 1995.\nSentjure M., Pecar S., Chen K., Wu M., Swartz H.M.: Biochim. Biophys. Acta1073, 329–335 (1991)\nKroll C., Langner A., Borchert H.H.: Free Radic. Biol. Med.26, 850–857 (1999)\nSuzuki-Nishimura T., Swartz H.M.: Free Radic. Biol. Med.17, 473–479 (1994)\nChen K., Glockner J.F., Morse P.D. II, Swartz H.M.: Biochemistry28, 2496–2501 (1989)\nChen K., Morse P.D. II, Swartz H.M.: Biochim. Biophys. Acta943, 477–484 (1988)\nChen K., Swartz H.M.: Biochim. Biophys. Acta970, 270–277 (1988)\nMorse P.D. II, Ruuge E.K., Petro M.J., Swartz H.M.: Biochim. Biophys. Acta1034, 298–302 (1990)\nReid D.A., Bottle S.E., Micallef A.S.: Chem. Commun.17, 1907–1908 (1998)\nMicallef A.S., Bott R.C., Bottle S.E., Smith G., White J.M., Matsuda K., Iwamura H.: J. Chem. Soc. Perkin Trans.2, 65–71 (1999)\nMicallef A.S., Bottle S.E., Gillies D.G., Hughes D.S., Sutcliffe L.H.: J. Chem. Soc. Perkin Trans. (2001) in press.\nSwartz H.M., Sentjure M., Morse P.D. II: Biochim. Biophys. Acta888, 82–90 (1986)\nIannone A., Hu H., Tomasi A., Vannini V., Swartz H.M.: Biochim. Biophys. Acta991, 90–96 (1989)",{"EN":1026},"Nitroxides are widely used as biophysical probes to study molecular motion, intracellular oxygen, pH, transmembrane potential, and cellular redox metabolism, etc. They may be rapidly metabolized to hydroxylamines by cells, which limits their use in viable systems. In this study, we have characterized relevant properties in cells of several isoindoline nitroxides that have been prepared to have different physicochemical properties: 1,1,3,3-tetramethylisoindolin-2-yloxyl (TMIO) and its analogs 5-carboxy-1,1,3,3-tetramethylisoindolin-2-yloxyl (CTMIO), 5-(N,N,N-trimethylammonio)-1,1,3,3-tetramethyl isoindolin-2-yloxyl iodide (QATMIO) and 2-hydroxy-1,1,3,3-tetramethylisoindoline hydrochloride (TMIOH.HCI). The oxygen sensitivity and metabolic kinetics of these were compared in CHO cells under different oxygen tensions with 1-oxyl-2,2,6,6-tetramethyl-4-piperidione (Tempone) and 3-carboxyl-2,2,5,5-tetramethyl-pyrrolidine-1-oxyl (PCA). Cytotoxicity was evaluated by the measurement of oxygen consumption rates, trypan blue exclusion, and clone formation. TMIO and its analogues have a higher relative oxygen sensitivity than Tempone and PCA with the oxygen sensitivity in electron paramagnetic resonance (EPR) spectrometry in the order of: TMIO=TMIOH=CTMIO>QATMIO=Tempone\u003CPCA. The rates of metabolism of these nitroxides are moderate and depend on oxygen concentration, ring type, ring substituent, and membrane permeation. These nitroxides have low cytotoxicity. The results indicate that TMIO and its analogues are potentially useful for EPR studies of viable systems, especially for oximetry.",{"EN":1028},"Development of isoindoline nitroxides for EPR oximetry in viable systems",{"VOID":1030},"10.1007\u002FBF03166117","https:\u002F\u002Flink.springer.com\u002Farticle\u002F10.1007\u002FBF03166117",[1033,1048,1060,1075,1087,1099,1111],{"id":1034,"sortIndex":379,"researcher":20,"roles":1035,"affiliations":1036,"properties":1045},"4b4fb241-74db-4528-ab77-23197a86988b",[227],[1037],{"id":20,"sortIndex":21,"affiliation":1038,"properties":20},{"id":1039,"createTime":1040,"updateTime":1040,"relativeEntities":1041,"slug":20,"properties":1042,"entityType":41,"verifyStatus":19,"verifyTime":20,"verifyNote":20,"syncStatus":19,"languages":20,"translateLanguages":20,"viewCount":21},"b1f229ce-cf43-4ea6-8b9a-2236862fd6ae","2024-02-19T23:45:20.845+00:00",[],{"title":1043},{"VI":1044},"EPR Center, Department of Diagnostic Radiology, Dartmouth Medical School, Hanover, USA",{"title":1046},{"VI":1047},"O. 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Fraissard, O. Lapina (eds.), Explosives Detection Using Magnetic and Nuclear Resonance Techniques. Series: NATO Science for Peace and Security Series. Subseries: NATO Science for Peace and Security Series B: Physics and Biophysics (Springer, Berlin, 2009), p. 295. (ISBN: 978-90-481-3060-3)\nT. Apih, B. Rameev, G. Mozzhukhin, J. Barras (eds.), Magnetic Resonance Detection of Explosives and Illicit Materials. Series: NATO Science for Peace and Security Series B: Physics and Biophysics (Springer, Berlin, 2014). (X, 168 p. 84 illus., 50 illus. in color)\nG.V. Mozzhukhin, B.Z. Rameev, Nuclear quadrupole resonance, in Book Subsurface Sensing. ed. by A.S. Turk, A.K. Hocaoglu, A.A. Vertiy (Wiley-Interscience, Hoboken, 2011), pp. 429–450. (ISBN: 978-0-470-13388-0, Hardcover, 920 pages)\nJ. Barras, K. Althoefer, M. Rowe, I. Poplett, J. Smith, The emerging field of medicines authentication by nuclear quadrupole resonance spectroscopy. Appl. Magn. Reson. 43(4), 511–529 (2012)\nJ. Barras, A. Jakobsson, E. Gudmundson, M.D. Rowe, I.J.F. Poplett, J. Luznik, V. Jazbinsek, J. Pirnat, J. Seliger, Z. Trontelj, J.A.S. Smith, K. Althoefer, The emerging field of medicines authentication by nuclear quadrupole resonance spectroscopy, in Counterfeit Medicines Volume II: Detection, Identification and Analysis. ed. by P. Wang, A.I. Wertheimer (ILM Publications, Hertfordshire, 2012)\nG.V. Mozjoukhine, The two-frequency nuclear quadrupole resonance for explosives detection. Appl. Magn. Reson. 18, 527–535 (2000). https:\u002F\u002Fdoi.org\u002F10.1007\u002FBF03162299\nK.L. Sauer, B.H. Suits, A.N. Garroway, J.B. Miller, Three-frequency nuclear quadrupole resonance of spin-1 nuclei. Chem. Phys. Lett. 342(3–4), 362–368 (2001). https:\u002F\u002Fdoi.org\u002F10.1016\u002FS0009-2614(01)00602-9\nV.S. Grechishkin, G.V. Mozzhukhin, N.Y. Sinyavskii, E.V. Yurepina, Two-frequency saturation in pulsed NQR of 14N. Russian Phys. J. 31(8), 647–649 (1988)\nD.Y. Osokin, R.R. Khusnutdinov, Theory of two-frequency excitation in 14N NQR. Appl. Magn. Reson. 24(2), 145–156 (2003)\nD.Y. Osokin, R.R. Khusnutdinov, V.A. Shagalov, Two-frequency multiple-pulse sequences in nitrogen-14 NQR. Appl. Magn. Reson. 25(3), 513–521 (2004)\nG.V. Mozjoukhine, The two-frequency nuclear quadrupole resonance for explosives detection. Appl. Magn. Reson. 18(4), 527–535 (2012)\nD.Y. Osokin, R.R. Khusnutdinov, Two-frequency composite pulses in NQR. Appl. Magn. Reson. 30(1), 7–11 (2006)\nG.V. Mozzhukhin, B.Z. Rameev, R.R. Khusnutdinov, N. Doğan, B. Aktas, Three-frequency composite multipulse nuclear quadrupole resonance technique for explosive detection. Appl. Magn. Reson. 43(4), 547–556 (2013)\nG.V. Mozzhukhin, B.Z. Rameev, N. Doğan, B. Aktaş, The application of the two frequency composite pulses for NQR detection of nitrogen-based compounds. J. Supercond. Nov. Magn. 24(1), 653–658 (2012)\nL. Cardona, H. Itozaki, J. Jiménez, N. Vanegas, H. Sato-Akaba, Design of a radiofrequency transceiver coil for landmine detection in Colombia by nuclear quadrupole resonance. Heliyon 6(1), e03242 (2020). https:\u002F\u002Fdoi.org\u002F10.1016\u002Fj.heliyon.2020.e03242\nG.V. Mozzhukhin, A.V. Efremov, A.V. Bodnya, V.V. Fedotov, A two-spiral flat coil for detecting 14N NQR signals. Russian Phys. J. 48(9), 978–983 (2005)\nB.H. Suits, A.N. Garroway, J.B. Miller, Noise-immune coil for unshielded magnetic resonance measurements. J. Magn. Reson. 131(1), 154–158 (1998)\nB.H. Suits, A.N. Garroway, Optimizing surface coils and the self-shielded gradiometer. J. Appl. Phys. 94(6), 4170–4178 (2003). https:\u002F\u002Fdoi.org\u002F10.1063\u002F1.1601296\nJ. Shinohara, H. Sato-Akaba, H. Itozaki, Simulation of nuclear quadrupole resonance for sensor probe optimization. Solid State Nucl. Magn. Reson. 43–44, 22–6 (2012). https:\u002F\u002Fdoi.org\u002F10.1016\u002Fj.ssnmr.2012.02.004\nC.P. Slichter, Principles of Magnetic Resonance, 2nd edn. (Springer-Verlag, Berlin, 1980), p. 165\nG.V. Mozzhukhin, B.Z. Rameev, N. Dogan, B. Aktas, The two-frequency multipulse sequence in nuclear quadrupole resonance of N-14 nuclei, in Explosives Detection using Magnetic and Nuclear Resonance Techniques. Series: NATO Science for Peace and Security Series. Subseries: NATO Science for Peace and Security Series B: Physics and Biophysics. ed. by J. Fraissard, O. Lapina (Springer, Berlin, 2009), pp. 205–230\nG.V. Mozzhukhin, B.Z. Rameev, N. Dogan, B. Aktas, The application of the two-frequency composite pulses for NQR detection of nitrogen-based compounds. J. Supercond. Nov. Magn. 24, 653–658 (2011)\nJ.A.S. Smith, Nitrogen-14 quadrupole resonance detection of RDX and HMX based explosives. Eur. Conv. Secur. Detection 408, 288–292 (1995)\nA.N. Garroway, M.L. Buess, J.B. Miller, B.H. Suits, A.D. Hibbs, G.A. Barrall, R. Matthews, L.J. Burnett, IEEE Trans. Geosci. Remote Sens. 39(6), 1108 (2001)\nV.S. Grechishkin, Nuclear Quadrupole Interaction in Solids (Nauka, Moscow, 1973), p. 154\nG.V. Mozjoukhine (Mozzhukhin), Appl. Magn. Reson. 118, 527 (2000)\nScience for Peace and Security Programme, Last updated: 10 Jun. 2021 14:20, https:\u002F\u002Fwww.nato.int\u002Fcps\u002Fen\u002Fnatohq\u002Ftopics_85373.htm",{"EN":1169},"The experimental realization of the two-frequency 14N nuclear quadrupole resonance (NQR) technique with use of the gradiometer radiofrequency (RF) probe for applications in the remote detection of explosives and other substances has been proposed. The planar two-frequency gradiometer has been designed, modeled and manufactured. The regions, where the RF magnetic fields are nearly orthogonal to each other, have been determined by finite-element modeling studies. The two-frequency experiments have been carried out for the detection of hexahydro-1,3,5-trinitro-s-triazine C3H6N6O6 (RDX). The possibility of the combined use of the two-frequency 14N NQR technique and the gradiometer RF probe in practice for detection of explosives hidden under clothes or underground has been also discussed.",{"EN":1171},"Two-Frequency Planar Gradiometer for Distant NQR Detection of Explosives",{"VOID":1173},"10.1007\u002Fs00723-021-01430-2","https:\u002F\u002Flink.springer.com\u002F10.1007\u002Fs00723-021-01430-2",[1176,1191,1206,1230,1249],{"id":1177,"sortIndex":379,"researcher":20,"roles":1178,"affiliations":1179,"properties":1188},"803086c6-a3fa-4e1a-b1a0-86d1d5a17ac2",[227],[1180],{"id":20,"sortIndex":21,"affiliation":1181,"properties":20},{"id":1182,"createTime":1183,"updateTime":1183,"relativeEntities":1184,"slug":20,"properties":1185,"entityType":41,"verifyStatus":19,"verifyTime":20,"verifyNote":20,"syncStatus":19,"languages":20,"translateLanguages":20,"viewCount":21},"74280b31-0c43-42cf-8337-a011138376a7","2023-12-14T19:50:34.270+00:00",[],{"title":1186},{"VI":1187},"Zavoisky Physical-Technical Institute – Subdivision of the Federal Research Center “Kazan Scientific Center of Russian Academy of Sciences”,, Kazan\u002FTatarstan, Russian Federation",{"title":1189},{"VI":1190},"Y. 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Vaughan, M. Garwood, C.M. Collins, W. Liu, L. DelaBarre, G. Adriany, G.P. Andersen, H. Merkle, R. Goebel, M.B. Smith, K. Ugurbil, Magn. Reson. Med. 46, 24 (2001)\nP.-F. Van de Moortele, C. Akgun, G. Adriany, S. Moeller, J. Ritter, C.M. Collins, M.B. Smith, J.T. Vaughan, K. Ugurbil, Magn. Reson. Med. 54, 1503 (2005)\nC.M. Collins, W. Liu, W. Schreiber, Q.Y. Yang, M.B. Smith, J. Magn. Reson. Imag. 21, 192 (2005)\nN.I. Avdievich, H.P. Hetherington, A.M. Kuznetsov, J.W. Pan, J. Magn. Reson. Imag. 29, 461 (2009)\nA. Nabetani, G. McKinnon, T. Nakada, in Proceedings of the 14th annual meeting of ISMRM, Seattle, 2006, p. 2608\nG. Adriany, P.-F. Van de Moortele, F. Wiesinger, S. Moeller, J.P. Strupp, P. Andersen, C. Snyder, X. Zhang, W. Chen, K.P. Pruessmann, P. Boesiger, J.T. Vaughan, K. Ugurbil, Magn. Reson. Med. 53, 434 (2005)\nR.G. Pinkerton, E.A. Barberi, R.S. Menon, Magn. Reson. Med. 54, 499 (2005)\nG. Adriany, P.F. Van de Moortele, J. Ritter, S. Moeller, E.J. Auerbach, C. Akgun, C.J. Snyder, T. Vaughan, K. Ugurbil, Magn. Reson. Med. 59, 590 (2008)\nN.I. Avdievich, J.W. Pan, J.M. Baehring, D.D. Spencer, H.P. Hetherington, Magn. Reson. Med. 62, 17 (2009)\nW. Mao, M.B. Smith, C.M. Collins, Magn. Reson. Med. 56, 4–918 (2006)\nT.S. Ibrahim, L. Tang, J. Magn. Reson. Imag. 25, 6–1235 (2007)\nJ. Tropp, T. Schirmer, J. Magn. Reson. 151, 146 (2001)\nN.I. Avdievich, J.W. Pan, A.M. Kuznetsov, H.P. Hetherington, in Proceedings of the 17th annual meeting of ISMRM, Honolulu, 2009, p. 3002\nH.P. Hetherington, N.I. Avdievich, J.W. Pan, in Proceedings of the 18 th annual meeting of ISMRM, Stockholm, 2010, p. 3822\nN.I. Avdievich, J.W. Pan, H.P. Hetherington, in Proceedings of the 19th annual meeting of ISMRM, Montreal, 2011, p. 328\nN.I. Avdievich, J.W. Pan, H.P. Hetherington, in Proceedings of the 18th annual meeting of ISMRM, Stockholm, 2010, p. 1501\nN.I. Avdievich, H.P. Hetherington, J. Magn. Reson. 186, 341 (2007)\nQ.X. Yang, J. Wang, C.M. Collins, M.B. Smith, X. Zhang, K. Ugurbil, W. Chen, Magn. Reson. Med. 52, 1016 (2004)\nJ.T. Vaughan, H.P. Hetherington, J.O. Otu, J.W. Pan, G.M. Pohost, Magn. Reson. Med. 32, 206 (1994)\nM.D. Harpen, Magn. Reson. Med. 29, 5–713 (1993)\nM. Sucher, J. Fox, Handbook of microwave measurements (Interscience Publishers, Polytechnic Press of the Polytechnic Institute of Brooklyn\u002FNew York, 1963)\nJ.P. Strupp, E.J. Auerbach, A. Gozubuyuk, G. Adriany, K. Ugurbil, P.-F. Van De Moortele, in Proceedings of the 16th annual meeting of ISMRM, Toronto, 2008, p. 1135\nJ.W. Pan, D.B. Twieg, H.P. Hetherington, Magn. Reson. Med. 40, 363 (1998)\nH.P. Hetherington, N.I. Avdievich, J.W. Pan, in Proceedings of the 19th annual meeting of ISMRM, Montreal, 2011, p. 163\nH.P. Hetherington, N.I. Avdievich, A.M. Kuznetsov, J.W. Pan, Magn. Reson. Med. 63, 9 (2010)\nA.R. Rath, J. Magn. Reson. 86, 488 (1990)\nJ. Murphy-Boesch, R. Srinivasan, L. Carvajal, T.R. Brown, J. Magn. Reson. B 103, 103 (1994)\nG.X. Shen, J.F. Wu, F.E. Boada, K.R. Thulborn, Magn. Reson. Med. 41, 268 (1999)\nM.D. Schnall, V.H. Subramanian, J.S. Leigh, B. Chance, J. Magn. Reson. 65, 122 (1985)\nJ.R. Fitzsimmons, B.L. Beck, H.R. Brooker, Magn. Reson. Med. 30, 107 (1993)",{"EN":1313},"The paper describes technological advances in high-field (7 T) transceiver-phased arrays developed for magnetic resonance imaging of the human brain. The first part of this work describes an 8-element inductively decoupled split elliptical transceiver-phased array with selectable geometry, which provides an easy and efficient way of compensating for changes in mutual inductive coupling associated with difference in loading due to variability in head shape and size. The second part of the work describes a double-row 16-element (2 × 8) transceiver array to extend the homogeneous transmit B\n                        1 profile in the longitudinal direction. Multiplexing eight transmit channels between the two rows of the array provides homogeneous excitation over the entire volume. The final section describes design and construction of a double-tuned 31P\u002F1H 16-element (8 at each frequency) array. The array improves transmission efficiency and B\n                        1 homogeneity at 1H frequency in comparison with 31P\u002F1H quadrature transverse electromagnetic volume coil. For 31P studies, the array also improves transmission efficiency (38%), signal-to-noise ratio (SNR) for central brain locations (20%) and provides substantially greater SNR (up to 400%) for peripheral locations.",{"EN":1315},"Transceiver-Phased Arrays for Human Brain Studies at 7 T",{"VOID":1317},"10.1007\u002Fs00723-011-0280-y","https:\u002F\u002Flink.springer.com\u002Farticle\u002F10.1007\u002Fs00723-011-0280-y",[1320],{"id":1321,"sortIndex":21,"researcher":20,"roles":1322,"affiliations":1323,"properties":1332},"7771205b-4d7f-4f7e-b6b2-a66c1ce76e39",[227],[1324],{"id":20,"sortIndex":21,"affiliation":1325,"properties":20},{"id":1326,"createTime":1327,"updateTime":1327,"relativeEntities":1328,"slug":20,"properties":1329,"entityType":41,"verifyStatus":19,"verifyTime":20,"verifyNote":20,"syncStatus":19,"languages":20,"translateLanguages":20,"viewCount":21},"4e4dd07d-e919-45a4-8330-f7a543aabb62","2024-01-17T05:30:35.366+00:00",[],{"title":1330},{"VI":1331},"Department of Neurosurgery, Yale University, New Haven, USA",{"title":1333},{"VI":1334},"Nikolai I. 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Springer, Berlin (1992)\nBoldu, J.L., Gleason, R.J., Georgiev, M.: Phys. Rev. B 32, 7043–7047 (1985)\nDavies, J.J., Smith, S.R.P., Wertz, J.E.: Phys. Rev. 178, 608–612 (1969)\nRubio, J., Chen, Y., Abraham, M.M.: J. Chem. Phys. 64, 4804–4806 (1976)\nGroh, D.J., Pandey, R., Recio, J.M.: Phys. Rev. B 50, 14860–14866 (1994)\nLever, A.B.P.: Inorganic Electronic Spectroscopy. Elsevier, Amsterdam (1984)\nZheng, W.C., Wu, X.X.: J. Phys. Chem. Solids 66, 1701–1704 (2005)\nMacfarlane, R.M.: Phys. Rev. B 1, 989–1004 (1970)\nMacfarlane, R.M.: J. Chem. Phys. 47, 2066–2073 (1967)\nGriffith, J.S.: The Theory of Transition-Metal Ions. Cambridge University Press, London (1964)\nDu, M.L., Rudowicz, C.: Phys. Rev. B 46, 8974–8977 (1992)\nClementi, E., Raimondi, D.L.: J. Chem. Phys. 38, 2686–2689 (1963)\nClementi, E., Raimondi, D.L., Reinhardt, W.P.: J. Chem. Phys. 47, 1300–1307 (1967)\nZheng, W.C.: Physica B 215, 255–259 (1995)\nWeast, R.C. (ed.): CRC Handbook of Chemistry and Physics. CRC Press, Boca Raton, Fla. (1989)\nStokowski, S.E., Schawlow, A.L.: Phys. Rev. 178, 457–464 (1969)\nBryknar, Z., Trepakov, V., Potucek, Z., Tastrabik, L.: J. Lumin. 87–89, 605–607 (2000)\nWu, S.Y., Dong, H.N.: Z. Naturforsch. A 59, 689–693 (2004)\nTippins, H.H.: Phys. Rev. B 1, 126–135 (1970)\nYamase, T., Kobayashi, T., Kettel, S.F.A.: J. Electrochem. Soc. 143, 1678–1680 (1996)\nBlasse, G., de Korte, P.H.M.: J. Inorg. Nucl. Chem. 43, 1505–1506 (1981)\nNewman, D.J., Ng, B.: Rep. Prog. Phys. 52, 699–763 (1989)\nYu, W.L.: J. Phys.: Condens. Matter 6, 5105–5112 (1994)\nZheng, W.C., Zhou, Q., Wu, X.X., Mei, Y.: Spectrochim. Acta A 61, 1243–1246 (2005)\nYeom, T.H., Choh, S.H., Du, M.L., Tang, M.S.: Phys. Rev. B 53, 3415–3421 (1996)\nRudowicz, C., Zhou, Y.Y.: J. Magn. Magn. Mater. 111, 153–163 (1992)",{"EN":1381},"The electron paramagnetic resonance (EPR) parameters (g-factors g\n                        ‖, g\n                        ⊥ and zero-field splitting D) of two tetragonal 3d3 impurity centers M3d-VMg and M3d-Li+ (where M3d = Cr3+ or Mn4+, VMg is the Mg2+ vacancy) in M3d-doped MgO crystals are calculated from the high-order perturbation formulas including both the crystal-field (CF) and the charge-transfer (CT) mechanisms for 3d3 ions in the tetragonal symmetry. The calculated results are in reasonable agreement with the experimental values. From the calculations, it can be found that the relative importance of the CT mechanism for EPR parameters increases with increasing valence state of the 3d3 ion. So, for the high-valence 3d\n                  n\n                 ions in crystals, a reasonable explanation of EPR parameters should take into account both CF and CT mechanisms. The defect structures (characterized by the displacement ΔR of O2− in the intervening M3d and VMg or Li+ at the Mg2+ site) for these tetragonal impurity centers are obtained from the calculations. The results are consistent with the expectations based on the electrostatic interactions.",{"EN":1383},"Study of EPR parameters and defect structure for two tetragonal impurity centers in MgO:Cr3+ and MgO:Mn4+ crystals",{"VOID":1385},"10.1007\u002Fs00723-009-0181-5","https:\u002F\u002Flink.springer.com\u002Farticle\u002F10.1007\u002Fs00723-009-0181-5",[1388,1413,1435,1447],{"id":1389,"sortIndex":379,"researcher":20,"roles":1390,"affiliations":1391,"properties":1410},"a516129f-7cd9-4b35-82d2-e48d19f8c9fd",[227],[1392,1400],{"id":20,"sortIndex":21,"affiliation":1393,"properties":20},{"id":1394,"createTime":1395,"updateTime":1395,"relativeEntities":1396,"slug":20,"properties":1397,"entityType":41,"verifyStatus":19,"verifyTime":20,"verifyNote":20,"syncStatus":19,"languages":20,"translateLanguages":20,"viewCount":21},"18e5d2f4-131b-4999-a7b1-a0a67b7d1d17","2023-12-06T23:51:31.368+00:00",[],{"title":1398},{"VI":1399},"Department of Material Science, Sichuan University, Chengdu, People’s Republic of China",{"id":1401,"sortIndex":180,"affiliation":1402,"properties":1409},"a6448e75-debe-4e85-891a-94fae1506a5f",{"id":1403,"createTime":1404,"updateTime":1404,"relativeEntities":1405,"slug":20,"properties":1406,"entityType":41,"verifyStatus":19,"verifyTime":20,"verifyNote":20,"syncStatus":19,"languages":20,"translateLanguages":20,"viewCount":21},"1f83dcbb-c8bb-490d-83be-fe48f44b93fe","2023-12-12T05:20:45.631+00:00",[],{"title":1407},{"VI":1408},"International Center for Materials Physics, Chinese Academy of Sciences, Shenyang, People’s Republic of China",{},{"title":1411},{"VI":1412},"W. -C. Zheng",{"id":1414,"sortIndex":327,"researcher":20,"roles":1415,"affiliations":1416,"properties":1432},"5812e121-91d9-47da-bfcb-3b1dae384c4e",[227],[1417,1422],{"id":20,"sortIndex":21,"affiliation":1418,"properties":20},{"id":1394,"createTime":1395,"updateTime":1395,"relativeEntities":1419,"slug":20,"properties":1420,"entityType":41,"verifyStatus":19,"verifyTime":20,"verifyNote":20,"syncStatus":19,"languages":20,"translateLanguages":20,"viewCount":21},[],{"title":1421},{"VI":1399},{"id":1423,"sortIndex":180,"affiliation":1424,"properties":1431},"7f57abfe-329b-471c-a2e8-8bc5b1aac8d8",{"id":1425,"createTime":1426,"updateTime":1426,"relativeEntities":1427,"slug":20,"properties":1428,"entityType":41,"verifyStatus":19,"verifyTime":20,"verifyNote":20,"syncStatus":19,"languages":20,"translateLanguages":20,"viewCount":21},"7af4aaa0-d224-4162-8fc9-77efc226f302","2024-02-12T16:19:33.711+00:00",[],{"title":1429},{"VI":1430},"Department of Applied Physics, Chongqing Institute of Technology, Chongqing, People’s Republic of China",{},{"title":1433},{"VI":1434},"W. -L. Feng",{"id":1436,"sortIndex":180,"researcher":20,"roles":1437,"affiliations":1438,"properties":1444},"e68cc9de-40ae-496c-856b-3989963f8481",[227],[1439],{"id":20,"sortIndex":21,"affiliation":1440,"properties":20},{"id":1394,"createTime":1395,"updateTime":1395,"relativeEntities":1441,"slug":20,"properties":1442,"entityType":41,"verifyStatus":19,"verifyTime":20,"verifyNote":20,"syncStatus":19,"languages":20,"translateLanguages":20,"viewCount":21},[],{"title":1443},{"VI":1399},{"title":1445},{"VI":1446},"W. Fang",{"id":1448,"sortIndex":21,"researcher":20,"roles":1449,"affiliations":1450,"properties":1459},"f4913f96-c5ec-4897-8a6f-320bacd142c0",[227],[1451],{"id":20,"sortIndex":21,"affiliation":1452,"properties":20},{"id":1453,"createTime":1454,"updateTime":1454,"relativeEntities":1455,"slug":20,"properties":1456,"entityType":41,"verifyStatus":19,"verifyTime":20,"verifyNote":20,"syncStatus":19,"languages":20,"translateLanguages":20,"viewCount":21},"6b7b3262-3639-467f-9f1d-58654631ff1b","2024-01-30T06:00:23.344+00:00",[],{"title":1457},{"VI":1458},"Department of Physics, Civil Aviation Flight University of China, Guanghan, People’s Republic of China",{"title":1460},{"VI":1461},"Xiao-Xuan Wu",{"url":1386,"publisher":1463,"properties":1491},{"id":6,"createTime":7,"updateTime":8,"relativeEntities":1464,"slug":10,"properties":1465,"entityType":18,"verifyStatus":19,"verifyTime":20,"verifyNote":20,"syncStatus":19,"languages":20,"translateLanguages":20,"viewCount":21,"subjectFields":1469,"manageAffiliations":1470,"indexDatabases":1471,"url":97,"thumbnailPath":20,"statistic":1486,"gsStatistic":20,"type":203,"analyzePriority":20},[],{"issn":1466,"eissn":1467,"title":1468},{"VOID":13},{"VOID":15},{"EN":17},[],[],[1472,1479],{"id":79,"indexDatabase":1473,"url":92,"indexYears":93,"academicFieldIds":1478,"indexDatabaseRanking":96},{"id":81,"createTime":82,"updateTime":83,"relativeEntities":1474,"label":1475,"description":1476,"key":89,"publicationTags":1477,"standard":20},[],{"EN":86,"VI":86},{"EN":86,"VI":88},[91],[95],{"id":58,"indexDatabase":1480,"url":73,"indexYears":20,"academicFieldIds":1485,"indexDatabaseRanking":20},{"id":60,"createTime":61,"updateTime":62,"relativeEntities":1481,"label":1482,"description":1483,"key":69,"publicationTags":1484,"standard":20},[],{"EN":65,"VI":65},{"VI":67,"EN":68},[71,72],[75,76,77],{"impactFactor":21,"impactFactorByYear":1487,"i10Index":113,"i10IndexLast5Year":114,"totalPublication":115,"totalPublicationByYear":1488,"totalCitation":143,"totalCitationByYear":1489,"totalCitationPerPublication":170,"totalCitationPerPublicationByYear":1490,"hindexLast5Year":117,"hindex":117},{"2004":100,"2005":101,"2012":102,"2013":103,"2014":104,"2015":105,"2016":106,"2017":107,"2018":108,"2019":108,"2020":109,"2021":110,"2022":111,"2023":112},{"1990":117,"1991":118,"1992":119,"1993":120,"1994":121,"1995":122,"1996":123,"1997":124,"1998":125,"1999":126,"2000":127,"2001":128,"2002":129,"2003":128,"2004":130,"2005":131,"2006":132,"2007":121,"2008":133,"2009":134,"2010":133,"2011":133,"2012":135,"2013":136,"2014":137,"2015":135,"2016":137,"2017":135,"2018":138,"2019":139,"2020":134,"2021":140,"2022":141,"2023":142,"2024":54},{"1990":145,"1991":146,"1992":113,"1993":147,"1994":148,"1995":149,"1996":150,"1997":151,"1998":152,"1999":126,"2000":153,"2001":154,"2002":125,"2003":127,"2004":155,"2005":156,"2006":141,"2007":157,"2008":158,"2009":159,"2010":160,"2011":161,"2012":162,"2013":163,"2014":164,"2015":165,"2016":121,"2017":166,"2018":118,"2019":167,"2020":136,"2021":130,"2022":168,"2023":169},{"1990":172,"1991":173,"1992":174,"1993":175,"1994":114,"1995":176,"1996":177,"1997":178,"1998":179,"1999":180,"2000":181,"2001":182,"2002":183,"2003":184,"2004":185,"2005":186,"2006":182,"2007":187,"2008":188,"2009":189,"2010":190,"2011":191,"2012":192,"2013":193,"2014":194,"2015":195,"2016":196,"2017":197,"2018":198,"2019":199,"2020":200,"2021":201,"2022":202,"2023":108},{"volume":1492,"pages":1494},{"VOID":1493},"35",{"VOID":1495},"503-510","2009-05-15",2009,{"id":1499,"createTime":1500,"updateTime":1501,"relativeEntities":1502,"slug":1503,"properties":1504,"entityType":221,"verifyStatus":299,"verifyTime":1513,"verifyNote":300,"syncStatus":19,"languages":20,"translateLanguages":20,"viewCount":21,"primaryUrl":1514,"fullTextUrl":20,"authors":1515,"publicationType":240,"publisherRelationship":1606,"citationCount":20,"citationInfo":20,"publishDate":1640,"publishYear":1641,"citationAnalyzeStatus":19,"lastCitationAnalyze":20,"indexDatabases":20,"openAccess":20,"references":20,"isForceReanalyzing":277},"097571d7-3344-41d4-8832-896c17455135","2024-01-17T12:38:09.363+00:00","2024-12-13T23:57:19.959+00:00",[],"MAS-STMAS-and-DQMAS-NMR-Studies-of-the-Thermal-Transformation-of-Kaolinite",{"references":1505,"abstract":1507,"title":1509,"doi":1511},{"VOID":1506},"S.K. Giri, N.N. Das, G.C. Pradhan, Powder Technol. 214, 3 (2011)\nS. Ghosh, Z.Y. Wang, S. Kang, P.C. Bhowmik, B.S. Xing, Pedosphere 19, 1 (2009)\nC.Y. Chen, G.S. Lan, W.H. Tuan, J. Eur. Ceram. Soc. 20, 14–15 (2000)\nH.P. He, J.G. Guo, J.X. Zhu, P. Yuan, C. Hu, Spectrochim Acta A 60, 5 (2004)\nA.A. Ogacho, B.O. Aduda, F.W. Nyongesa, J. Mater. Sci. 38, 11 (2003)\nH. Schneider, J. Schreuer, B. Hildmann, J. Eur. Ceram. Soc. 28, 2 (2008)\nJ.C. Taylor, I. Hinczak, C.E. Matulis, Powder Diffr. 15, 1 (2000)\nO. Font, N. Moreno, X. Querol, M. Izquierdo, E. Alvarez, S. Diez, J. Elvira, D. Antenucci, H. Nugteren, F. Plana, A. Lopez, P. Coca, F.G. Pena, Fuel 89, 10 (2010)\nD. Iuga, C. Morais, Z.H. Gan, D.R. Neuville, L. Cormier, D. Massiot, J. Am. Chem. Soc. 127, 33 (2005)\nA.R. Grimmer, H. Zanni, P. Sozzani (Eds.), Springer Verlag Berlin (1998)\nJ. Skibsted, C. Hall, Cement Concrete Res. 38, 2 (2008)\nJ.H. Baltisberger, Z. Xu, J.F. Stebbins, S.H. Wang, A. Pines, J. Am. Chem. Soc. 118, 30 (1996)\nK. Glock, O. Hirsch, P. Rehak, B. Thomas, C. Jager, J. Non-Cryst. Solids 232, 113 (1998)\nJ. Klinowski, S.W. Carr, S.E. Tarling, P. Barnes, Nature 330, 6143 (1987)\nS.M. DePaul, M. Ernst, J.S. Shore, J.F. Stebbins, A. Pines, J. Phys. Chem. B 101, 16 (1997)\nK. Kanehashi, K. Saito, Energy Fuel 18, 6 (2004)\nP. Burchill, O.W. Howarth, B.J. Sword, Fuel 70, 3 (1991)\nL. Frydman, J.S. Harwood, J. Am. Chem. Soc. 117, 19 (1995)\nS. Antonijevic, S.E. Ashbrook, S. Biedasek, R.I. Walton, S. Wimperis, H.X. Yang, J. Am. Chem. Soc. 128, 24 (2006)\nZ.H. Gan, J. Am. Chem. Soc. 122, 13 (2000)\nT. Takahashi, S. Kashiwakura, K. Kanehashi, T. Nagasaka, Energy Fuel 23, 1178 (2009)\nJ.P. Amoureux, A. Flambard, L. Delevoye, L. Montagne, Chem. Commun. 27, 3472 (2005)\nS. Ganapathy, L. Delevoye, J.P. Arnoureux, P.K. Madhu, Magn. Reson. Chem. 46, 10 (2008)\nT. Takahashi, K. Kanehashi, Y. Shimoikeda, T. Nemoto, K. Saito, J. Magn. Reson. 198, 2 (2009)\nJ. Trebosc, J.P. Amoureux, Z.H. Gan, Solid State Nucl. Magn. Reson. 31, 1 (2007)\nM.A. Bernstein, L.A. Trimble, Magn. Reson. Chem. 32, 2 (1994)\nI. de Boer, L. Bosman, J. Raap, H. Oschkinat, H.J.M. de Groot, J. Magn. Reson. 157, 2 (2002)\nS.P. Brown, H.W. Spiess, Chem. Rev. 101, 12 (2001)\nN. Malicki, G. Mali, A.A. Quoineaud, P. Bourges, L.J. Simon, F. Thibault-Starzyk, C. Fernandez, Micropor. Mesopor. Mat. 129, 1–2 (2010)\nX.C. Lin, K. Ideta, J. Miyawaki, Y. Nishiyama, I. Mochida, S.H. Yoon, Magn. Reson. Chem. 50, 4 (2012)\nS. Lee, Y.J. Kim, H.S. Moon, J. Am. Ceram. Soc. 86, 1 (2003)\nX.C. Lin, K. Ideta, J. Miyawaki, H. Takebe, S.H. Yoon, I. Mochida, Energy Fuel 26, 4 (2012)\nJ. Schneider, M.A. Cincotto, H. Panepucci, Cement Concrete Res. 31, 7 (2001)\nS.D. Wang, K.L. Scrivener, Cement Concrete Res. 33, 5 (2003)\nJ.H. Kwak, J.Z. Hu, D.H. Kim, J. Szanyi, C.H.F. Peden, J. Catal. 251, 1 (2007)\nJ.K. João Rocha, Phys. Chem. Miner. 17, 2 (1990)\nM. Pernpointner, L. Visscher, J. Chem. Phys. 114, 23 (2001)\nP. Mcmillan, B. Piriou, J. Non-Cryst. Solids 55, 2 (1983)\nM.J. Toplis, D.B. Dingwell, T. Lenci, Geochim. Cosmochim. Acta 61, 13 (1997)\nB.O. Mysen, D. Virgo, C.M. Scarfe, Am. Miner. 65, 690–710 (1980)\nB.O. Mysen, D. Virgo, I. Kushiro, Am. Miner. 66, 678–701 (1981)\nJ.F. Stebbins, Z. Xu, Nature 390, 6655 (1997)\nW. Loewenstein, Am. Miner. 39, 92–96 (1954)",{"EN":1508},"Thermal transformations of kaolinite at different temperatures were monitored using X-ray diffraction (XRD), high-resolution solid-state nuclear magnetic resonance  (800 MHz for 1H Larmor frequency) with single-pulse magic-angle spinning, double-quantum filter satellite-transition magic-angle spinning, and double-quantum homo-nuclear correlation under magic-angle spinning experiments. Results show that combined experiments clearly manifest the transitions of silicon and aluminum structures at different thermal treatment stages; and moreover, high magnetic field offers higher sensitivity and resolution, hereby the slim resonances are obtained successfully at less stringent conditions. The dehydroxylation process of kaolinite causes the presence of short-range order in metakaolinite, which is absence of XRD reflections. Particularly, the features of metakaolinite with high concentration of defects are found with dispersive aluminum coordinations; and further, the distorted tetrahedral aluminum is detected in kaolinite-derived mullite because of the locally disorganized structure. The framework structure of kaolinite-derived mullite is considered to be primarily formed by the tetrahedral aluminum bonding with octahedral aluminum. 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