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J. 154, 107–114 (2009)\nFefelov, V.F., Gorbunov, V.A., Myshlyavtsev, A.V., Myshlyavtseva, M.D.: Thermodynamics of lattice gas models of multisite adsorption. In: Morales-Rodriguez, R. (ed.) Thermodynamics–fundamentals and its application in science chapter 15, pp. 389–416. In Tech, Rijeka (2012)\nFefelov, V.F., Gorbunov, V.A., Myshlyavtsev, A.V., Myshlyavtseva, M.D.: Model of homonuclear dimer adsorption in terms of two possible molecule orientations with respect to surface: square lattice. Phys. Rev. 82, 041602 (2010a)\nFefelov, V.F., Gorbunov, V.A., Myshlyavtsev, A.V., Myshlyavtseva, M.D., Evseeva, S.I.: The simplest model of adsorption of molecules with different orientations in adlayer on the stepped surface. Appl. Surf. Sci. 256, 5298–5304 (2010b)\nFefelov, V.F., Gorbunov, V.A., Myshlyavtsev, A.V., Myshlyavtseva, M.D.: The simplest model of multisite adsorption of molecules with different orientation in Adlayer. Nanotech Conference and Expo 2010: Nanotech Conference Technical Proceedings, Anaheim, 2 July 649–652 (2010c)\nFrenkel, Y.I., Kontorova, T.: On the theory of plastic deformation and doubling. Zh. Eksp. Teor. Fiz. 8, 1340 (1938). In Russian\nGonzalez, E.J., Ramirez-Pastor, A.J., Pereyra, V.D.: Adsorption of dimers molecules on triangular and honeycomb lattices. Langmuir 17, 6974–6980 (2001)\nPieranski, P., Sotta, P., Rohe, D., Imperor-Clerc, M.: Devil’s staircase–type faceting of a cubic lyotropic liquid crystal. Phys. Rev. Lett. 84, 2409–2412 (2000)\nSelke, W., Fisher, M.E.: Monte Carlo study of the spatially modulated phase in an Ising model. Phys. Rev. 20, 257–265 (1979)\nShibata, N., Ishii, C., Ueda, K.: Devil’s staircase in Kondo semimetals at low temperatures. Phys. Rev. 52, 10232–10238 (1995)\nWang, X.Y., Taylor, P.L.: Devil’s staircase, critical thickness, and propagating fingers in antiferroelectric liquid crystals. Phys. Rev. Lett. 76, 640–643 (1996)\nYe, Y., Sun, W., Wang, Y., Shao, X., Xu, X., Cheng, F., Li, J., Wu, K.: A unified model: self-assembly of trimesic acid on gold. J. Phys. Chem. 111, 10138–10141 (2007)",{"EN":216},"We have constructed the simple two-dimensional adsorption model with short range non-competing interactions which demonstrates devil’s staircase of phase transitions. The main factor which leads to the appearance of infinite amount of ordered structures in our model is two competing forms of adsorption. 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Pharmaceut. Sci., 5, 199–204 (2002).\nFrancotte, E., P. Richert, M. Mazzotti, and M. Morbidellim, “Simulated Moving Bed Chromatographic Resolution of a Chiral Antitussive,” J. Chromatogr. A, 796, 239–248 (1998).\nGu, X.Q., B. Fryirs, and L.E. Mather, “High-Performance Liquid Chromatographic Separation and Nanogram Quantitation of Bupivacaine Enantiomers in Blood,” J. Chromatogr. B, 719, 135–140 (1998).\nGuiochon, G., S.G. Shirazi, and A.M. Katti, Fundamentals of Preparative and Nonlinear Chromatography, Academic Press, Boston, MA, 1994.\nMa, Z. and N.-H.L. Wang, “Standing Wave Analysis of SMB Chromatography: Linear Systems,” AIChE J., 1997, 43, 2488–2508 (1997).\nMiller, L., C. Orihuela, R. Fronek, and J. Murphy, “Preparative Chromatographic Resolution of Enantiomers using Polar Organic Solvents with Polysaccharide Chiral Stationary Phases,” J. Chromatogr. A, 865, 211–226 (1999).\nMigliorini, C., M. Mazzotti, G. Zenoni, and M. Morbidelli, “Shortcut Experimental Method for Designing Chiral SMB Separations,” AIChE J., 48, 69–77 (2002).\nMiyabe, K. and G. Guiochon, “A Study of Mass Transfer Kinetics in an Enantiomeric Separation System Using a Polimeric Imprinted Stationary Phase,” Biotechnol. Prog., 16, 617–627 (2000).\nMiyabe, K. and G. Guiochon, “Kinetic Study of the Concentration Dependence of the Mass Transfer Rate Coefficient in Anion-Exchange Chromatography of Bovine Serum Albumin,” Biotechnol. Prog., 15, 740–752 (1999).\nPais, L.S., J.M. Loureiro, and A.E. Rodrigues, “Chiral Separation by SMB Chromatography,” Sep. Purif. Technol., 20, 67–77 (2000).\nRuthven, D.M., Principles of Adsorption and Adsorption Process, Wiley, New York, 1984.\nSantos, M.A.G., V. Veredas, I.J. Silva Junior, C.R.D. Correia, L.T. Furlan, and C.C. Santana, “Simulated Moving-Bed Adsorption for Separation of Racemic Mixtures,” Braz. J. of Chem. Eng., 21, 127–136 (2004).\nSilva Jr., I.J., M.A.G. Santos, V. Veredas, and C.C. Santana, “Experimental Determination of Chromatographic Separation Parameters of Ketamine Enantiomers on MCTA,” Sep. Purif. Technol., 43, 103–110 (2005).\nSchulte, M., R. Ditz, R.M. Devant, J.N. Kinkel, and F. Charton, “Comparison of the Specific Productivity of Different Chiral Stationary Phases Used for Simulated Moving-Bed Chromatography,” J. Chromatogr. A, 769, 93–100 (1997).\nTanaka, P.P., R.O. Souza, M.F.O. Salvalaggio, and M.A.A. Tanaka, “Comparative Study of 0.5% Bupivacaine Versus 0.5% Bupivacaine Enantiomeric Mixture (S75-R25) in Epidural Anesthesia for Orthopedic Surgery,” Rev. Brasil. Anestesiol., 53, 331–337 (2003).\nXie, Y., B. Hritzko, Y.C. Chin, and N.-H.L. Wang, “Separation of FTC-Ester Enantiomers Using a Simulated Moving Bed,” Ind. Eng. Chem. Res., 42, 4066–4067 (2003).\nYu, H.W. and C.-B. Ching, “Modeling, Simulation and Operation Performance of a Simulated Moving Bed for Enantioseparation of Fluoxetine on New β-Cyclodextrin Columns,” Adsorption, 9, 213–223 (2003).\nWang, X. and C.-B. Ching, “Chiral Separation and Modeling of the Three-Chiral-Center β-blocker Drug Nadolol by Simulated Moving Bed Chromatography,” J. Chromatogr. A, 1035, 167–176 (2004).\nWang, X. and C.-B. Ching, “Kinetic and Equilibrium Study of the Separation of Three Chiral Center Drug, Nadolol, by HPLC on a Novel Perphenyl Carbamoylated β-Cyclodextrin Bonded Chiral Stationary Phase,” Sep. Sci. Technol., 37, 2567–2586 (2002).\nWankat, P.C. Rate-Controlled Separations, Chapman & Hall, London, 1994.\nWilson, E.J. and C.J. Geankoplis, “Liquid Mass Transfer at Very Low Reynolds Numbers in Packed Beds,” Ind. Eng. Chem Fund., 5, 9–14 (1966).",{"EN":351},"Bupivacaine is an amide type local anesthetic widely used in surgery and obstetrics because of its sustained peripheral and central nerve blockade. R-(+)-bupivacaine is more toxic to the central nervous and the cardiovascular systems than S-(−)-bupivacaine. To obtain S-(−)-bupivacaine with high degree of purity using a continuous simulated moving bed (SMB) unity, equilibrium and mass transfer parameters under dilute conditions were obtained by pulse experiments using 0,0′-bis[4-terc-butyl-benzoyl]-N,N′-diallyl-L-tartar diamide immobilized in silica (Kromasil® CHI-TBB). The linear equilibrium constants were found to be 2.12 and 2.91 for R-(+)-and S-(−)-bupivacaine, respectively. Axial dispersion coefficients were found to be practically the same for both enantiomers. A fast kinetic of mass transfer was observed. The internal resistance to the mass transfer controls all the mass transfer process in this chiral column and the pore diffusion coefficients were of the order 10−7cm2\u002Fs. The equilibrium and mass transfer parameters will be employed in future simulation and design of operating conditions of SMB unity.",{"EN":353},"Chromatographic Separation of Bupivacaine Enantiomers by HPLC: Parameters Estimation of Equilibrium and Mass Transfer Under Linear Conditions",{"VOID":355},"10.1007\u002Fs10450-005-4903-1","https:\u002F\u002Flink.springer.com\u002Farticle\u002F10.1007\u002Fs10450-005-4903-1",[358,373,385,397],{"id":359,"sortIndex":258,"researcher":19,"roles":360,"affiliations":361,"properties":370},"51ca066d-47a4-4276-9fa5-0fee9a1940be",[230],[362],{"id":19,"sortIndex":20,"affiliation":363,"properties":19},{"id":364,"createTime":365,"updateTime":365,"relativeEntities":366,"slug":19,"properties":367,"entityType":55,"verifyStatus":18,"verifyTime":19,"verifyNote":19,"syncStatus":18,"languages":19,"translateLanguages":19,"viewCount":20},"66909643-208e-428e-83c8-8820eec1fc46","2023-12-29T23:58:24.579+00:00",[],{"title":368},{"VI":369},"Laboratory of Bioseparations, Department of Biotechnological Process, School of Chemical Engineering, State University of Campinas, Campinas, Brazil",{"title":371},{"VI":372},"Marcos José Souza Carpes",{"id":374,"sortIndex":20,"researcher":19,"roles":375,"affiliations":376,"properties":382},"a7377f47-807d-400f-b637-cd7beb85cce0",[230],[377],{"id":19,"sortIndex":20,"affiliation":378,"properties":19},{"id":364,"createTime":365,"updateTime":365,"relativeEntities":379,"slug":19,"properties":380,"entityType":55,"verifyStatus":18,"verifyTime":19,"verifyNote":19,"syncStatus":18,"languages":19,"translateLanguages":19,"viewCount":20},[],{"title":381},{"VI":369},{"title":383},{"VI":384},"Ivanildo José Da 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M., Piotrowska, A.: Performance analysis of Joule-Thomson cryocooler supplied with gas mixture. Cryocoolers 17, 397–406 (2012)\nLee, J., Lee, K., Jeong, S.: Experimental study of a mixed refrigerant Joule-Thomson cryocooler using a commercial air-conditioning scroll compressor. Cryogenics 55–56, 47–52 (2013)\nLewis, R., Wang, Y., Bradley, P.E., Huber, M.L., Radebaugh, R., Lee, Y.C.: Experimental investigation of low-pressure refrigerant mixtures for micro cryogenic coolers. Cryogenics 54, 37–43 (2013)\nNarasimhan, N.L., Venkatarathnam, G.: A method for estimating the composition of the mixture to be charged to get the desired composition in the circulating in a single stage JT refrigerator operating with mixtures. Cryogenics 50, 93–101 (2010)\nPassow, K.L., Skye, H.M., Nellis, G.F., Klein, S.A.: Experimental verification of a precooled mixed gas Joule-Thomson cryoprobe model. Adv. Cryog. Eng. 57, 1198–1205 (2012)\nPrakash, M.J., Prasad, M., Rastogi, S.C., Akkimaradi, B.S., Gupta, P.P., Narayanamurthy, H., Srinivasan, K.: Development of a laboratory model of activated charcoal-nitrogen adsorption cryocooler. Cryogenics 40, 481–488 (2000)\nRao, R.R., Prasad, M., Srinivasan, K.: Optimum operating conditions for an adsorption cryocooler: a case of activated carbon + nitrogen system. Cryogenics. 45, 193–197 (2005)\nTzabar, N.: Mixed-refrigerant Joule-Thomson (MR JT) mini-cryocoolers. Adv. Cryog. Eng. 59, 148–154 (2014a)\nTzabar, N.: Binary mixed-refrigerants for steady cooling temperatures between 80 K and 150 K with Joule-Thomson cryocoolers. Cryogenics 64, 70–76 (2014b)\nTzabar, N., Grossman, G.: Nitrogen, methane, and ethane sorption on activated carbon. Cryogenics 51, 499–508 (2011)\nTzabar, N., Grossman, G.: Analysis of an activated-carbon sorption compressor operating with gas mixtures. Cryogenics 52, 491–499 (2012)\nTzabar, N., Lapp, Z.: Experimental investigation on mixed-refrigerant for closed-cycle Joule-Thomson cryocoolers. Adv. Cryog. Eng. 55, 1121–1128 (2010)\nTzabar, N., ter Brake, H.J.M.: Adsorption isotherms and Sips models of nitrogen, methane, ethane, and propane on commercial activated carbons and polyvinylidene chloride. Adsorption 22, 901–914 (2016)\nTzabar, N., Holland, H.J., Vermeer, C.H., ter Brake, H.J.M.: Modeling the adsorption of mixed gases based on pure gas adsorption properties. Mat. Sci. Eng. (2015). https:\u002F\u002Fdoi.org\u002F10.1088\u002F1757-899X\u002F101\u002F1\u002F012169\nWu, Y., Zalewski, D.R., ter Brake, H.J.M.: Optimization of the working fluid for a sorption-based Joule-Thomson cooler. Adv. Cryog. Eng. 57, 1789–1796 (2012)",{"EN":455},"Sorption-based compressors are thermally driven and because of the absence of moving parts they are vibration free, and have the potential for long life. Sorption-based compressors have been reported to operate Joule–Thomson (JT) cryogenic coolers with pure working fluids. However, using mixed refrigerants instead of pure refrigerants is attractive since that would dramatically improve the system coefficient of performance. Our on-going research aims to develop an efficient JT sorption cryocooler, operating with mixed refrigerants, and is focused on studying the characteristics of the sorption compressor cycle. This paper presents the results of an advanced numerical analysis, which is based on a previous model, and its experimental verification. The analysis relates to the ideal cycle of a sorption compressor operating with a gas mixture. Obviously, dynamics and kinetics play a major rule in a real sorption compressor cycle. However, since there are no reported gas-mixture sorption compressors and the existing experience in this field is poor, a preliminary ideal cycle analysis is considered. Satisfying agreement between the numerical and experimental results is obtained and the processes in the sorption cycle are discussed. The outcomes of the current study are the basis for the next phase in which a sorption compressor prototype will be built operating with gas mixtures.",{"EN":457},"Analysis of ideal sorption compressor cycles operating with gas mixtures",{"VOID":459},"10.1007\u002Fs10450-018-9937-2","https:\u002F\u002Flink.springer.com\u002Farticle\u002F10.1007\u002Fs10450-018-9937-2",[462,477],{"id":463,"sortIndex":263,"researcher":19,"roles":464,"affiliations":465,"properties":474},"048466a6-72b0-4a31-9a75-8c131832c616",[230],[466],{"id":19,"sortIndex":20,"affiliation":467,"properties":19},{"id":468,"createTime":469,"updateTime":469,"relativeEntities":470,"slug":19,"properties":471,"entityType":55,"verifyStatus":18,"verifyTime":19,"verifyNote":19,"syncStatus":18,"languages":19,"translateLanguages":19,"viewCount":20},"d4b8171d-2584-4ccb-926a-6d55dd5aa52c","2024-01-03T18:04:55.895+00:00",[],{"title":472},{"VI":473},"Energy, Materials and Systems, Faculty of Science and Technology, University of Twente, Enschede, The Netherlands",{"title":475},{"VI":476},"H. J. M. ter Brake",{"id":478,"sortIndex":20,"researcher":19,"roles":479,"affiliations":480,"properties":496},"e0188097-ceae-4134-bfb8-3e33e6579bec",[230],[481,488],{"id":482,"sortIndex":263,"affiliation":483,"properties":487},"b59e097b-0c3c-4511-81da-5c67eb5b396b",{"id":468,"createTime":469,"updateTime":469,"relativeEntities":484,"slug":19,"properties":485,"entityType":55,"verifyStatus":18,"verifyTime":19,"verifyNote":19,"syncStatus":18,"languages":19,"translateLanguages":19,"viewCount":20},[],{"title":486},{"VI":473},{},{"id":19,"sortIndex":20,"affiliation":489,"properties":19},{"id":490,"createTime":491,"updateTime":491,"relativeEntities":492,"slug":19,"properties":493,"entityType":55,"verifyStatus":18,"verifyTime":19,"verifyNote":19,"syncStatus":18,"languages":19,"translateLanguages":19,"viewCount":20},"7f5ab8f2-6d2a-496a-a0b1-266370b6bbb0","2024-01-03T18:04:55.886+00:00",[],{"title":494},{"VI":495},"Department of Mechanical Engineering, Faculty of Engineering, Ariel University, Ariel, Israel",{"title":497},{"VI":498},"N. Tzabar",{"url":460,"publisher":500,"properties":528},{"id":6,"createTime":7,"updateTime":8,"relativeEntities":501,"slug":10,"properties":502,"entityType":17,"verifyStatus":18,"verifyTime":19,"verifyNote":19,"syncStatus":18,"languages":19,"translateLanguages":19,"viewCount":20,"subjectFields":506,"manageAffiliations":507,"indexDatabases":508,"url":110,"thumbnailPath":19,"statistic":523,"gsStatistic":19,"type":201,"analyzePriority":19},[],{"issn":503,"eissn":504,"title":505},{"VOID":13},{"VOID":15},{"EN":10},[],[],[509,516],{"id":90,"indexDatabase":510,"url":103,"indexYears":104,"academicFieldIds":515,"indexDatabaseRanking":109},{"id":92,"createTime":93,"updateTime":94,"relativeEntities":511,"label":512,"description":513,"key":100,"publicationTags":514,"standard":19},[],{"EN":97,"VI":97},{"EN":97,"VI":99},[102],[106,107,108],{"id":70,"indexDatabase":517,"url":85,"indexYears":19,"academicFieldIds":522,"indexDatabaseRanking":19},{"id":72,"createTime":73,"updateTime":74,"relativeEntities":518,"label":519,"description":520,"key":81,"publicationTags":521,"standard":19},[],{"EN":77,"VI":77},{"VI":79,"EN":80},[83,84],[87,88],{"impactFactor":20,"impactFactorByYear":524,"i10Index":123,"i10IndexLast5Year":124,"totalPublication":125,"totalPublicationByYear":525,"totalCitation":151,"totalCitationByYear":526,"totalCitationPerPublication":175,"totalCitationPerPublicationByYear":527,"hindexLast5Year":200,"hindex":200},{"2012":113,"2013":114,"2014":115,"2015":116,"2016":117,"2017":118,"2018":119,"2019":119,"2020":120,"2021":116,"2022":121,"2023":122},{"1995":127,"1996":128,"1997":129,"1998":130,"1999":131,"2000":132,"2001":127,"2002":132,"2003":133,"2004":129,"2005":134,"2006":130,"2007":135,"2008":136,"2009":137,"2010":138,"2011":139,"2012":136,"2013":140,"2014":141,"2015":135,"2016":142,"2017":143,"2018":144,"2019":145,"2020":146,"2021":147,"2022":148,"2023":149,"2024":150},{"1995":153,"1996":130,"1997":154,"2004":155,"2005":156,"2006":157,"2007":158,"2008":159,"2009":160,"2010":161,"2011":162,"2012":163,"2013":164,"2014":165,"2015":166,"2016":167,"2017":168,"2018":169,"2019":170,"2020":171,"2021":172,"2022":173,"2023":174},{"1995":177,"1996":178,"1997":179,"2004":180,"2005":181,"2006":182,"2007":183,"2008":184,"2009":185,"2010":186,"2011":187,"2012":188,"2013":189,"2014":190,"2015":191,"2016":192,"2017":193,"2018":194,"2019":195,"2020":196,"2021":197,"2022":198,"2023":199},{"volume":529,"pages":531},{"VOID":530},"24",{"VOID":532},"325-332","2018-02-26",2018,{"id":536,"createTime":537,"updateTime":538,"relativeEntities":539,"slug":540,"properties":541,"entityType":221,"verifyStatus":222,"verifyTime":538,"verifyNote":223,"syncStatus":18,"languages":19,"translateLanguages":19,"viewCount":20,"primaryUrl":550,"fullTextUrl":19,"authors":551,"publicationType":305,"publisherRelationship":603,"citationCount":19,"citationInfo":19,"publishDate":636,"publishYear":444,"citationAnalyzeStatus":18,"lastCitationAnalyze":19,"indexDatabases":19,"openAccess":19,"references":19,"isForceReanalyzing":342},"108c12de-cf96-4a94-895a-0cdd194ae316","2023-12-27T09:24:46.646+00:00","2024-12-15T23:53:49.077+00:00",[],"Adsorption-of-Pure-Gases-and-Mixtures-on-Porous-Solids-up-to-High-Pressures",{"references":542,"abstract":544,"title":546,"doi":548},{"VOID":543},"Beutekamp S., Adsorption von Gasgemischen bis zu Drücken von 15MPa, Ph D thesis, Center of Non-Classical Chemistry, Leipzig, University of Leipzig, Germany, 2002.\nDo D.D., Adsorption and Kinetics, Imperial College Press, London, UK, 1999.\nDreisbach F., R. Staudt, and J.U. Keller, High Pressure Adsorption Data of Methane, Nitrogen, Carbon Dioxide andtheir Binary and Ternary Mixtures on Activated Carbon, Adsorption, 5, 215–227 (1999).\nGibbs J.W., On the Equilibrium of Heterogeneous Substances, American Journal of Sciences and Arts, 16, 441–458 (1878).\nHarting P., J. Germanus, and S. Beutekamp, Ermittlung von Partialbeladungen bei der Gemischadsorption von Gasen biszu höheren Drücken. In: Staudt, R. (Hrsg.): Technische Sorptionsprozesse. VDI Fortschrittberichte, Reihe3, Nr. 554, VDI Verlag, Düsseldorf 1998.\nHerbst A. and P. Harting, Thermodynamic Description of Excess Isotherms in High-Pressure Adsorption of Methane, Argonand Nitrogen, Adsorption, 8, 111–123 (2002).\nHonigberg, M.G., Chemical Equilibrium and Velocity of Reactions at High Pressures (in Russian), Publisher “Chimija”, Moscow, pp. 117–119.(1969).\nKeller J.U., F. Dreisbach, H. Rave, R. Staudt, and M. Tomalla, Measurement and Correlation of Gas Mixture Adsorption Equilibria of Natural Gas Compounds on Microporous Sorbens, I. Experimental Methods, Adsorption, 5, 199–214 (1999).\nLe Van D., Adsorption processes and modelling: present and future, F. Meunier (Hrsg.): Proc. 6th Int. Conf. on Fund. of Adsorption, Elsevier, Paris 1998.\nMarkham E.C. and A.F. Benton, The Adsorption of Gas Mixtures by Silica, J. Am. Chem. Soc., 53 (1)497–507 (1931).\nMyers A.L. and J.M. Prausnitz, Thermodynamics of Mixed Gas Adsorption, AICh E Journal, 11 (1)121–127.(1965).\nMyers A.L., J.A. Calles and G. Calleja, Comparison of Molecular Simulation of Adsorption with Experiment, Adsorption, 3, (2) 107–115 (1997).\nRouquerol F., J. Rouquerol, and K.S.W. Sing, Adsorption by Powders and Porous Solids—Principles, Methodology and Applications. Academic Press, London, 1999.\nSuzuki M., (Ed); Proc. 4th Int. Conf. on Fund. of Adsorption, Kyoto, May 1992, Kodanska Ltd., Tokyo, 1993.\nStaudt R., G. Saller, M. Tomalla, and J.U. Keller, A Note on Gravimetric Measurements of Gas-Adsorption Equilibria.Ber. Bunsenges. Phys. Chem. Bd.97(1) 98–105 (1993).\nStaudt R., Analytische und experimentelle Untersuchung von Adsorptionsgleichgewichten von reinen Gasen und Gasgemischen an Aktivkohlen und Zeolithen, Dissertation, Fachbereich Maschinentechnik, Universität Siegen, 1994.\nStaudt R., S. Bohn, F. Dreisbach and J.U. Keller, Gravimetric and Volumetric Measurement of Helium Adsorption Equilibriaon different Porous Solids, Proc. of the Characterization of Porous Solids, IV Conference, Bath., 1996, B.McEnaney et al. (Eds.), London: Royal Society of Chemistry, 1997.\nTalu O., Needs, status, techniques and problems with binary gas adsorption experiments, Adv. Colloid Interface Sci., 76\u002F77, 227–269 (1998).\nvan Ness H.C., Adsorption of Gases on Solids, I & EC Fundamentals, 8(3) 464–473 (1969).",{"EN":545},"Physisorption equilibria of multicomponent gases on microporous solids like zeolites or activated carbons are considered. An overview about adsorption measurements of pure gases H2, He, O2, N2, Ar, CO2, CO, CH4, C2H4 and C2H6 and some of their mixtures in the pressure range vacuum \u003C p \u003C 50 MPa at different temperatures 10∘C–70∘C were investigated. Also a thermodynamic formalism based on a modified van Ness method and on a new 3 parameter Isotherm equation (3-PIG) to describe the excess amount adsorbed was developed. Results are shown and discussed.",{"EN":547},"Adsorption of Pure Gases and Mixtures on Porous Solids up to High Pressures",{"VOID":549},"10.1007\u002Fs10450-005-5402-0","https:\u002F\u002Flink.springer.com\u002Farticle\u002F10.1007\u002Fs10450-005-5402-0",[552,567,579,591],{"id":553,"sortIndex":20,"researcher":19,"roles":554,"affiliations":555,"properties":564},"5c31c174-c461-44dc-831f-014ae6ace890",[230],[556],{"id":19,"sortIndex":20,"affiliation":557,"properties":19},{"id":558,"createTime":559,"updateTime":559,"relativeEntities":560,"slug":19,"properties":561,"entityType":55,"verifyStatus":18,"verifyTime":19,"verifyNote":19,"syncStatus":18,"languages":19,"translateLanguages":19,"viewCount":20},"4449491b-f089-4806-9b93-6cc39800dc21","2023-12-27T09:24:46.708+00:00",[],{"title":562},{"VI":563},"Center of Non-Classical Chemistry, the University of Leipzig, Leipzig, Germany",{"title":565},{"VI":566},"Reiner Staudt",{"id":568,"sortIndex":245,"researcher":19,"roles":569,"affiliations":570,"properties":576},"c82123f3-284c-40c9-a872-c53429f62c9b",[230],[571],{"id":19,"sortIndex":20,"affiliation":572,"properties":19},{"id":558,"createTime":559,"updateTime":559,"relativeEntities":573,"slug":19,"properties":574,"entityType":55,"verifyStatus":18,"verifyTime":19,"verifyNote":19,"syncStatus":18,"languages":19,"translateLanguages":19,"viewCount":20},[],{"title":575},{"VI":563},{"title":577},{"VI":578},"Peter 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R.K., Schwarz, J.A.: Analysis of high pressure adsorption of gases on activated carbon by potential theory. Carbon 26, 873–887 (1988)\nAmankwah, K.A.G., Schwarz, J.A.: A modified approach for estimating pseudo-vapor pressures in the application of the Dubinin-Astakhov equation. Carbon 33(9), 1313–1319 (1995)\nBae, J.-S., Bhatia, S.K.: High-pressure adsorption of methane and carbon dioxide on coal. Energy & Fuels 20, 2599–2607 (2006)\nBatos-Neto, M., Torres, A.E.B., Azevedo, D.C.S., Cavalcante, C.L., Jr.: A theoretical and experimental study of charge and discharge cycles in a storage vessel for adsorbed natural gas. Adsorption 11, 147–157 (2005)\nBénard, P., Chahine, R.: Modeling of high-pressure adsorption isotherms above the critical temperature on microporous adsorbents: application to methane. Langmuir 13, 808–813 (1997)\nBénard, P., Chahine, R.: Modeling of adsorption storage of hydrogen on activated carbons. Int. J. Hydrog. Energy 26, 849–855 (2001)\nCruz, P., Santos, J.C., Magalhães, F.D., Mendes, A.: Cyclic adsorption separation processes: analysis strategy and optimization procedure. Che. Eng. Sci. 58, 3143–3158 (2003)\nCzerny, A.M., Bénard, P., Chahine, R.: Adsorption of nitrogen on granular activated carbon: experiment and modeling. Langmuir 21, 2871–2875 (2005)\nDastgheib, S.A., Karanfil, T.: The effect of the physical and chemical characteristics of activated carbons on the adsorption energy and affinity coefficient of Dubinin equation. J. Colloid Interface Sci. 292, 312–321 (2005)\nDreisbach, F., Lösch, H.W., Harting, P.: Highest pressure adsorption equilibria data: measurement with magnetic suspension balance and analysis with a new adsorbent\u002Fadsorbate-volume. Adsorption 8, 95–109 (2002)\nDubinin, M.M.: The potential theory of adsorption of gases and vapors for adsorbents with energetically nonuniform surfaces. Chem. Rev. 60, 235–241 (1960)\nDubinin, M.M.: Physical adsorption of gases and vapors in micropores. In: Cadenhead, D.A., Danielli, J.F., Rosenberg, M.D. (eds.) Progress in Membrane and Surface Science, vol. 9, chap. 1, pp. 1–70. Academic Press, New York (1975)\nHimeno, S., Komatsu, T., Fujita, S.: High-pressure adsorption equilibria of methane and carbon dioxide on several activated carbons. J. Chem. Eng. Data 50, 369–376 (2005)\nLemmon, E.W., Peskin, A.P., McLinden, M.O., Friend, D.G.: NIST12 Thermodynamic and Transport Properties of Pure Fluids—NIST Standard Reference Database 12, Version 5.0. US Secretary of Commerce, Washington (2000)\nMota, J.P.B., Rodrigues, A.E., Saatdjian, E., Tondeur, D.: Dynamics of natural gas adsorption storage systems employing activated carbon. Carbon 35(9), 1259–1270 (1997)\nMurata, K., El-Merraoui, M., Kaneko, K.: A new determination method of absolute adsorption isotherm of supercritical gases under high pressure with a special relevance to density-functional theory study. J. Chem. Phys. 114(9), 4196–4205 (2001)\nMurata, K., Miyawaki, J., Kaneko, K.: A simple determination method of absolute adsorbed amount for high pressure gas adsorption. Carbon 40, 425–428 (2002)\nMyers, A.L., Monson, P.A.: Adsorption in porous materials at high pressure: theory and experiment. Langmuir 18(26), 10261–10273 (2002)\nOzawa, S., Kusumi, S., Ogino, Y.: Physical adsorption of gases at high pressure IV. An improvement of the Dubinin-Astakhov adsorption equation. J. Colloid Interface Sci. 56(1), 83–91 (1976)\nPoirier, E., Chahine, R., Bénard, P., Lafi, L., Dorval-Douville, G., Chandonia, P.A.: Hydrogen adsorption measurements and modeling on metal-organic frameworks and single-walled carbon nanotubes. Langmuir 22(21), 8784–8789 (2006)\nRichard, M.-A., Bénard, P., Chahine, R.: Gas adsorption process in activated carbon over a wide temperature range above the critical point. Part 2: conservation of mass and energy. Adsorption (2009, in press)\nSalem, M.M.K., Braeuer, P., Szombathely, M.V., Heuchel, M., Harting, P., Quitzch, K., Jaroniec, M.: Thermodynamics of high-pressure adsorption of argon, nitrogen, and methane on microporous adsorbents. Langmuir 14(12), 3376–3389 (1998)\nSircar, S.: Gibbsian surface excess for gas adsorption—revisited. Ind. Eng. Chem. Res. 38(10), 3670–3682 (1999)\nTalu, O., Myers, A.L.: Molecular simulation of adsorption: Gibbs dividing surface and comparison with experiment. AIChE J. 47(5), 1160–1168 (2001)\nTeng, Y., Wang, R.Z., Wu, J.Y.: Study of the fundamentals of adsorption systems. Appl. Therm. Eng. 17(4), 327–338 (1997)\nZhang, S.-Y., Talu, O., Hayhurst, D.T.: High-pressure adsorption of methane in NaX, MgX, CaX, SrX, and BaX. J. Phys. Chem. 95, 1722–1726 (1991)",{"VI":647,"EN":648},"Các mô phỏng về hiệu ứng nhiệt trong quá trình hấp phụ là công cụ quý giá cho việc thiết kế các hệ thống dựa trên hấp phụ hiệu quả như lưu trữ khí, tách khí và máy bơm nhiệt dựa trên hấp phụ. Một biểu diễn phân tích của dữ liệu hấp phụ đã đo được trong khoảng áp suất và nhiệt độ hoạt động rộng là cần thiết để tính toán các phương trình bảo toàn khối lượng và năng lượng đầy đủ. Trong Phần 1, mô hình Dubinin-Astakhov (D-A) được điều chỉnh để mô hình hóa các đẳng nhiệt hấp phụ của hydro, nitơ và methane trên than hoạt tính ở áp suất cao và nhiệt độ siêu tới hạn, với giả định thể tích hấp phụ vi mô không đổi. Mô hình hấp phụ loại D-A năm tham số được chứng minh là phù hợp với dữ liệu thực nghiệm cho hydro (30 đến 293 K, lên tới 6 MPa), nitơ (93 đến 298 K, lên tới 6 MPa) và đối với methane (243 đến 333 K, lên tới 9 MPa). Chất lượng của sự phù hợp của nhiều đẳng nhiệt hấp phụ thực nghiệm là xuất sắc trong khoảng nhiệt độ và áp suất lớn liên quan. Các tham số của mô hình cũng có thể được xác định chỉ từ các đẳng nhiệt hydro ở 77 K và 298 K mà không làm giảm nhiều chất lượng của sự phù hợp.","Simulations of the thermal effects during adsorption cycles are valuable tools for the design of efficient adsorption-based systems such as gas storage, gas separation and adsorption-based heat pumps. An analytical representation of the measured adsorption data over the wide operating pressure and temperature swing of the system is necessary for the calculation of complete mass and energy conservation equations. In Part 1, the Dubinin-Astakhov (D-A) model is adapted to model hydrogen, nitrogen, and methane adsorption isotherms on activated carbon at high pressures and supercritical temperatures assuming a constant microporous adsorption volume. The five parameter D-A type adsorption model is shown to fit the experimental data for hydrogen (30 to 293 K, up to 6 MPa), nitrogen (93 to 298 K, up to 6 MPa), and for methane (243 to 333 K, up to 9 MPa). The quality of the fit of the multiple experimental adsorption isotherms is excellent over the large temperature and pressure ranges involved. The model’s parameters could be determined as well from only the 77 K and 298 K hydrogen isotherms without much reducing the quality of the fit.",{"VI":650,"EN":651},"Quá trình hấp phụ khí trên than hoạt tính ở khoảng nhiệt độ rộng trên điểm tới hạn. Phần 1: Mô hình Dubinin-Astakhov đã được chỉnh sửa","Gas adsorption process in activated carbon over a wide temperature range above the critical point. 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Ö. Özbelge, and T. Doğu, “Use of General Purpose Adsorption Isotherms for Heavy Metal-Clay Mineral Interactions,” J. Colloid Interface Sci., 198, 130–140 (1998).\nAtun, G., G. Hisarlı, and M. Tunçay, “Adsorption of Safranine-O on Hydrophilic and Hydrophobic Glass Surfaces,” Coll. Surf., 143, 27–33 (1998).\nBajpai, A.K. and R. Sachdeva, “Adsorption of Casein onto Alkali Treated Bentonite,” J. Appl. Polym. Sci., 78, 1656–1663 (2000).\nBorovec, Z., “The Adsorption of Uranyl Species by Fine Clay,” Chemical Geology, 32,45–48 (1981).\nBrooks, S.P.J. and B.J. Lampi, “Problems Associated with Measuring Phytate in Infant Cereals,” J. Agric. Food Chem., 49, 564–569 (2001).\nCarrado, K.A. and L. Xu, “ın Situ Synthesis of Polymer-Clay Nanocomposites from Silcate Gels,” Chem. Matter., 10, 1440–1445 (1998).\nCelis, R., M.C. Hermosin, and J. Cornejo, “Heavy Metal Adsorption by Functionalized Clays,” Environ Sci. Technol., 34, 4593–4599 (2000).\nCeyhan, Ö., H. Güler, and R. Güler, “Adsorption Mechanisms of Phenol and Methylphenols on Organoclays,” Ads. Sci. Technol., 17, 469–477 (1999).\nChisholm-Brause, C., S.D. Conradson, C.T. Buscher, P.G. Eller, and D.E. Morris, “Speciation of Uranyl Sorbed at Multiple Binding Sites on Montmorillonite,” Geochim. Cosmochim. Acta., 58, 3625–3631 (1994).\nDai, S., Y.S. Shin, C.E. Barnes, and L.M. Toth, “Enhancement of Uranyl Adsorption Capacity and Selectivity on Silica Sol-Gel Glasses Via Molecular Imprinting,” Chem. Mater., 9, 2521–2525 (1997).\nDe Boland, A.R., G.B. Garner, and B.L. O'Dell, “Identification and Properties of “Phytate” in Cereal Grains and Oilseed Products,” J. Agric. Food. Chem., 23, 1186–1189 (1975).\nDomb, A.J., E.G. Cravalho, and R. Langer, “The Synthesis of Poly(hydroxamic Acid) from Poly(acrylamide),” J. Polym. Sci. Poly. Chem., 26, 2623–2630 (1988).\nEligwe, C.A., N.B. Okolue, C.O. Nwambu, and C.I.A. Nwoko, “Adsorption Thermodynamics and Kinetics of Mercury(II), Cadmium( II) and Lead(II) on Lignite,” Chem. Eng. Technol., 22,45–49 (1999).\nFrossard, E., M. Bucher, F. Machler, A. Mozafar, and R. Hurrell, “Potential for Increasing the Content and Bioavailability of Fe, Zn and Ca in Plants for Human Nutrition,” J. Sci. Food Agric., 80, 861–879 (2000).\nGiles, C.H., T.H. MacEwan, S.N. Nakhwa, and D. Smith, “Studies in Adsorption. Part XI. A System of Classification of Solution Adsorption Isotherms, and Its Use in Diagnosis of Adsorption Mechanisms and in Measurement of Spesific Surface Areas of Solids,” J. Chem. Soc., 3973–3993 (1960).\nGreenwood, N.N. and A. Earnshaw, Chemistry of The Elements, Butterworth-Heinemann Ltd., Cambridge, 1995.\nGrim, R.E., Clay Minerology, Mc Graw Hill, New York, 1968.\nGüven, O. and P. Akkas, “Enhancement of Uranyl Ion Uptake by Prestructuring of Acyrlamide—Maleic Acid Hydrogels,” J. Appl. Polym. Sci., 78, 284–289 (2000).\nHaderlein, S.B., K.W. Weissmahr, and R.P. Schwarzenbach, “Specific Adsorption of Nitroaromatic Explosives and Pesticides to Clay Minerals,” Environ Sci. Technol., 30, 612–622 (1996).\nJin, W. and S. Zhu, “Study of Adsorption Equilibrium and Dynamics of Benzene, Toluene, and Xylene on Zeolite NaY,” Chem. Eng. Technol., 23, 151–156 (2000).\nLagadic, I.L., M.K. Mitchell, and B.D. Payne, “Highly Effective Adsorption of Heavy Metal Ion by a Thiol-Functionalized Magnesium Phyllosilicate Clay,” Environ Sci. Technol., 35, 984–990 (2001).\nLagaly, G., “Introduction: From Clay Mineral-Polymer Interactions to Clay Mineral-Polymer Nanocomposites,” Appl. Clay. Sci., 15, 1–9 (1999).\nLoewus, F.A. and M.W. Loewus, “Myo-Inositol: Its Biosynthesis and Metabolizm,” Ann. Rev. Plant Physiol., 34, 137–161 (1983).\nLuckham, P.F. and S. Rossi, “The Colloidal and Rheological Properties of Bentonite Suspensions,” Adv. Colloid Interface Sci., 82, 43–92 (1999).\nLurie, Ju., Handbook of Analytical Chemistry, Mir Publishers, Moscow, 1975.\nMiller, J.C. and J.N. Miller, Statistics for Analytical Chemistry, John Wiley & Sons, New York, 1989.\nO'Neill, I.K., M. Sargent, and M.L. Trimble, “Determination of Phytate in Foods by Phosphorus-31 Fourier Transform Nuclear Magnetic Resonance Spectrometry,” Anal. Chem., 52, 1288–1291 (1980).\nPanayotova, M., “Kinetics of Heavy Metal Ions Removal from Wastewater by Natural Zeolite in the Presence of Calcium and Magnesium,” J. Environ. Protec. Eco., 3, 350–355 (2000).\nPefferkorn, E., “Polyacrylamide at Solid\u002FLiquid Interfaces,” J. Coll. and Inter. Sci., 216, 197–220 (1999).\nRauf, N. and S.S. Tahir, “Thermodynamics of Fe(II) and Mn(II) Adsorption onto Bentonite from Aqueous Solutions,” J. Chem. Therm., 32, 651–658 (2000).\nShi, H., T. Lan, and J. Pinnavaia, “Interfacial Effects on the Reinforcement Properties of Polymer-Organoclay Nanocomposites,” Chem. Mater., 8, 1584–1587 (1996).\nSingh, V.K. and P.N. Tiwari, “Removal and Recovery of Chromium(VI) from Industrial Waste Water,” J. Chem. Tech. Biotechnol., 69, 376–382 (1997).\nStarodoubtsev, S.G., N.A. Churochkina, and A.R. Khokhlov, “Hydrogel Composites of Neutral and Slightly Charged Poy-( acrylamide) Gels with Incorporated Bentonite. Interaction with Salt and Ionic Surfactants,” Langmuir., 16, 1529–1534 (2000).\nTheng, B.K.G., The Chemistry of Clay-Organic Reactions, John Wiley & Sons, New York, 1974.\nTsao, G.T., Y. Zheng, J. Lu, and C.S. Gong, “Adsorption of Heavy Metal Ions by Immobilized Phytic Acid,” Appl. Bichem. Biotechnol., 63–65, 731–741 (1997).\nVan der Maas, J.H., Basic Infrared Spectroscopy, Heyden & Son Ltd., London, 1972.\nVohra, P., G.A. Gray, and F.H. Kratzer, “Phytic Acid-Metal Complexes,” Proc. Soc. Exp. Biol. Med., 120, 447–449 (1965).",{"EN":1008},"Composite of polyacrylamide-bentonite (PAA-B) was prepared by direct polymerisation of PAA in a suspension of bentonite (B). Adsorption and thermodynamic features of phytic acid (Phy) adsorption onto B, PAA and PAA-B, and those of Fe3+, Zn2+, UO2\n2+ adsorption onto PAA-B and its modification by Phy (PAA-B-Phy) have been investigated. The reusability, storagability, ion selectivity and recoverability of sorbed ions with 1 M HCl have also been considered. The chemical and physical structure of adsorbents has been characterised by means of FT-IR and XRD. All adsorption isotherms for Phy and the ions were L-type of the Giles classification except, the one which is S type for adsorption of Phy onto PAA. The maximum adsorption capacities for the ions adsorbed were in order of UO2\n2+ > Fe3+ > Zn2+ for PAA-B and Zn2+ > Fe3+ > UO2\n2+ for PAA-B-Phy. Langmuir equilibrium constants for the adsorption of ions onto PAA-B-Phy were significantly higher than those found for PAA-B; the magnitude of increase for UO2\n2+ was about 100. The thermodynamic parameters indicated that adsorption reactions are spontaneous in terms of adsorption free enthalpy. The chemical structure of PAA-B-Phy was not changed at the end of the studies of reusability and storagability. The composite was selective for UO2\n2+ of the ions of interest. The composite of PAA-B and its modification by Phy have been used for the first time in this investigation. 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